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HomeMy WebLinkAboutWater Quality Data 201641.111-++.1 s+.+a+:+.ll?lij r • ANALYTICAL REPORT Ju ly 11. 2016 --------------· ----- EnCana Oil & Gas -Parachute, CO Sample Delivery Group : Samples Received Project Number: Description: Site: Report To : L84 4 405 06/30/2016 High Mesa WTF GarCo HIGH MESA WTF Brett Middleton 143 Diamond Avenue Parachute, CO 81635 Entire Report Reviewed By: ~ ~~~ Shane Gambill Technical Service Representative Results relate only ID the items lcstcd 01 cahbr«ted und arc reported as rounded vulues. This lest repolt ~all not be reproduced, except In full. without written approval of the laboratory Where applrcable. sampling conducted by ESC rs performed per guidance provided in laboralory standard operating proccdu1cs: 060302, 060303, and 060304 TABLE OF CONTENTS 'Cp Cover Page 2Tc : Table of Contents 3 Ss: Sample Summary 4 Cn: Case Narrative 5 Sr: Sample Results 20160628-HIME PIT W L844405-0 1 20160628-HIME PIT MI D l 844405-02 20160628-HIME PIT NE L844405-03 20160628-HIME PIT SE L844405-04 6GI: Glossary of Terms 1 Al: Accreditations & Locations 8 Sc: Chain of Custody ACCOUNT: EoCenn Oil & Gas • Pnrachute. CO PROJECT SDG: l84440 5 ' ON E LAB . NATIONWIDE • DATE/TIME· 01111n6 10:02 1 2 3 5 6 6 8 10 12 t 4 15 16 ~ • EJ EJ ~. a ~ E] PAGE 2 of t7 SAMPLE SUMMARY Collected by 20160628-HIME PIT W L844405-01 GW Chris Hines t.lethod Batch Dllutlon Pmparation dale/lime Giavimetric Analysis by Method 2540 C·2011 WG885818 07/05n6 08:39 Metals (ICP) by Methoo 60108 WG885472 10 01103n6 20 20 Metals (ICP) by Method 60109 WG885472 5 07/03n6 20 20 Volatile Organic Compounds (GC) by Method RSKt75 WG885857 1 07/051161112 Volatile Organic Compounds (GCIMS) by Melhod 826 (18 WG886485 lOO 07/071t6 00 51 Wet Chemistry by Method 2320 B-2011 WG886222 07107/16 09 57 Wet Chemistry by Melhoo 350 1 WG886594 07/0811612 04 Wet Chemistry by Methoo 450052 0-2011 WG884957 07/0V16 08:29 Wet Chemistry by Melhoo 9040C WG88485t 0710111610·37 Wet Chemistry by Method 9050A WG884955 07/0V1612 47 Wet Ch emistry by Method 9056A WG884839 t 06/3ons 19 35 Wet Chom stry by Method 9056A WG884839 50 0 06/30116 t9 St Wet Ch~m stry by Method 9056A WG885863 07/05116 2341 Collected by 20160628-HIME PIT MID L844405-02 GW Cluls Hines Method Batch Dilution Preparnlion date/time GrnvimetrlC Analy;is by Methoo 2540 C-2011 WG885818 1 07/05/16 08 39 Metals (ICP) by Method 60108 WG885472 10 07/03/16 20 20 Metals (ICP) by Method 60109 WG885472 5 07/03/16 20 20 Volatile Organic Compounds (GC) by Method RSK175 WG885857 07/05n61114 Volatile Organic Compounds (GC/MS) by Method 82608 WG886485 07/07/16 Ol"tt Wet Chemistry by Method 2320 8·2011 WG886222 0710711610 •05 Wet Chemistry by Method 350 1 WG886594 07/08116 12 06 Wet Chemistry by Method 450052 D·201t WG884957 07/0V16 08:29 Wet Chemistry by Method 9040C WG884851 07/0V1610:37 Wet Chemistry by Method 9050A WG884955 07/0V161247 Wei Chemistry by Method 9056A WG884839 I 06130116 20 07 Wet Chemistry by Method 9056A WG884839 500 06130116 20 24 Wet Chemislry by Method 9056A WG886709 07/08/1615·27 Collected by 20160628·HIME PIT NE L844405-03 GW Chris Hines Method Batch Dilution Preparation dale/lime Gravimetric Analysis by Melhod 2540 C-2011 WG885818 1 07105116 08:39 Metals (ICP) by Method 60108 WG885472 5 01103n5 20·20 Volatile Orgamc Compounds (GC) by Method RSK175 WG885857 07/05n611:16 Vol<thte Organic Compounds (GC/MS) by Method 82608 WG886485 07/07/16 01 30 Wel Chemistry by Method 2320 B-2011 WG886222 07107/16 10 14 Wet Chemistry by Method 350.1 WG886594 07108/16 12 :08 Wet Chemistry by Method 450052 0·2011 WG8849S7 07/01116 08 30 Wet Chemistry by Method 9040C WG88485t 07/01116 10:37 Wet Chemistry by Method 9050A WG8B4955 07/0VtG t2 47 Wet Chemistry by Method 9056A WG884839 06130/16 20 40 Wet Chemistry by Method 9056A WG884839 lOO 06130/16 20 57 Wet Chemistry by Method 9056A WG886709 07/0811615. 57 ACCOUNT: PROJECT: SDG: EnCana Olt & Ga~ -Parachute. CO LB44405 ONE LAB NATIONWIDE • Collected dale/time 06128116 08 t5 Analysts dale/lim e 07/05n6 09:36 01106n6 10 54 07/06116 08:03 07/0511611 12 07/07/t6 00 .5t 07/07/l6 09 :57 07/08116 t2·04 07/01/t6 08 29 07/0tlt610•37 07/01/t612 47 06/3011619 ·35 06/30116 19 51 07105116 23:41 Collected d<tte/lime 06128116 08 20 Analysis date/time 07/05/t6 09 36 07/06/t6 11:46 07/06116 08•06 07/05116 ll;t4 07/07/16 Ot:n 07/07116 10:05 07/08116 12:06 07/0tl16 08:29 07/01116 10:37 07101f1612:47 06130116 20:07 06130116 20:24 07/08116 15:27 Collected datrltimc 06/28/16 08:25 Analysis dale/lime 07/05116 09:36 07/061161143 07/051161116 07/07116 01 30 07/07116 10 14 0710811612 08 07/01116 08:30 07/0111610 37 07/01/16 12"47 06/30116 2040 06130116 20 57 07/08116 15 57 DATE/TIME; 0711111610:02 Receiv~d da1C/Ume 06/30116 09:00 Analy;t JM LTB LTB MJ JHH MCG DR AMC KK MAJ SAM SAM SAM Received date/time 06/30116 09:00 Aoo lyst JM LTB LTB MJ JHH M ~G DR AM C KK MAJ SAM SAM SAM Received dJle/llme 06130116 09 00 Analyst JM LTB MJ JHH MCG DR AMC KK MAJ SAM SAM SAM ~ ~ • ~ ~ EJ EJ EJ PAGE : 3 of t7 SAMPLE SUMMARY Collce1cd by 20160628-HIME PIT SE L844405-04 GW ChriS Hines tlcthod Batch OUutlon Preparation dale/time Gravimetric Analysis by Method 2540 C-2011 WG885818 1 07/05116 08:39 Metals (ICP) by Method 60106 WG885472 5 07/03116 20:20 Volatile Organic Compounds (GC) by Method RSK175 WG885857 07/0511611:22 Volatile Organic Compounds (GC/MS) by Method 82606 WG886485 07107/16 01 so Wet Chemistry by Method 2320 8·2011 WG886222 07107/16 10 22 Wet Chemistry by Method 350 1 WG886594 07/08/16 12·14 Wet Chemistry by Method 4SOOS2 D·2lll1 \VG884957 07101/16 08 30 Wet Chemistry by Method 9040C WG884851 07101/16 10 37 Wet Chemistry by Method 90SOA WG884955 1 07/0111612 47 Wet Chemistry by Melhod 9056A WG884839 1 06/30116 21:46 Wet Chemistry by Method 9056A WG884839 100 06130116 22"02 ACCOUNT. PROJECT SDG. EnCana Oil & Gas· Parnchute. CO LB44405 ONE LAB . NATIONWIDE • Collem.d date/time 06/28/t6 08 30 Analysis dalcllime 07/05/16 09 36 07/06/16 08 09 07/05/16 11 22 01101116 01 ·so 07/07/1610 :22 07/08/161214 07/01116 08"30 07/01/16 10 37 07/0111612 47 06/30/16 2146 06130/16 22 02 DATE/TIME. 07n11161002 Received diltc/li~c 06/30/16 09 00 Analyst JM LTB MJ JHH MCG OR AMC KK MAJ SAM SAM B ~ • B EJ El ~ [g PAGE 4 o f17 CASE NARRATIVE ONE LAB . NATIONWIDE • All MDL (LOD) and RDL (LOO) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed In this case narrative, a non-conformance form or properly qualified within the sample results By my digital signature below, I affi rm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been dentlfied by the laboratory, and no Information or data have been knowingly withheld that would affect the quality of the data . Sha ne Gambill Tech nical Serv i ce Re p resen t at ive Sample Hand li ng a nd ReceiVi ng The following samples were prepared and/or analyzed past recommended holding time. Concentrations should be considered minimum values . ESC Sample ID Project Sample ID L844405-01 20160628-HIME PIT W L844405-02 20160628-HIME PIT MID L844405·03 20160628-HIME PIT NE L844405-04 2016062B ·HIME PIT SE ACCOUNT : PROJECT: EnCana Oil & Gas. Parachute CO Method 9056A 9040C 9040C.9056A 9056A 9040C 9056A 9040C SDG LB44405 DATE/TIME· 07/11116 10:02 PAGE· Sof 17 20160628-HIME PIT W SAMPLE RESULTS -01 ONE LAB NATIONWIDE • Collect ed da t e/Il en e 06/28116 08 15 l844405 Grav imetri c Analys is b y Method 2 540 C-2011 B Result ~ ROL Dilution Analysis 8a.1 ch Anulyte m~·1 mit~ date /ti me ~ Dissolved Solids 12700 10 0 07/0512016 09 36 VIG8858t8 Wet Chemistry by Met hod 2320 B-2011 ~ Result ~ RDL Diluti on Analysis Bat ch Analyte mg/I mg/I dal e/I me ~ Alkalinlty 890 200 07/0712016 09:57 WG886222 Alkallni1y .Blca1bona1e 890 200 07/0 7/2016 09:57 WG886222 • Alkalinily,Carbonale ND 200 07/0 7/2016 09 57 WG886222 Wet Chemistry by Method 350.1 EJ Resull ~ RDL DUutlon Analysts lralch Analyte M[lf' mg/I date/time EJ Am 'llO!lfil N•lroqcn 137 0 250 07/08/201612 :04 YlG886594 Wet Chemistry by Method 450052 D-2011 EJ R~11 ~ RDl Dilution Analysis Olltdl Analyte mg/l mg/I dale/lime Sulfide 0642 00500 07/01/2016 08'29 \YG884957 Wet Chemistry by Method 9040C Re5ull ~ Dilution Analysis B~lch Analytc ~u date /time pH 768 07/01/2016 10 37 WG884851 Sample NMratlve: 9040C l844405 -01 WG884851 7 68 al 8 9c Wet Chemistry by Method 9050A Result ~ Dilution Analysis Botch Anall'le umhoslcm dale I time Sp!!C ific Conductance 30500 07/0U2016 12·47 WG8 84955 Wet Chemistry by Method 9056A Result ~ RDL Dilution Analysis Batch •nolyte mg,1 mg/I date/time Bromrd l!' 79 .S 100 06130/2016 19:35 WG8848l 9 Chloride 11000 500 500 06130/2016 19 51 WG884839 Fluoride ND 0.100 07/05/2016 23:41 WG885863 Nitrate ilS (NJ ND 0.100 06130/201619:35 WG884839 Nilriteils{NJ ND 0.100 06130/2016 19:35 WG884839 Sullale 640 500 06/30/2016 19:35 WG884839 Metals (ICP) b y Met hod 60108 Result ~ RDL Dlutlon Analysis Batch An~lyte n>g.1 mg/I date/ lime Arscnlc,Olssolved ND 00500 5 0710612016 08 03 WG885472 Barlum,Dlssolved 36 7 0.0250 5 07/06/2016 08:03 WG885472 Cadmium.Dissolved ND 0.0100 5 07/06/2016 08:03 YIG885472 Calcium Dissolved 207 5.00 5 07/0612016 08:03 WG885472 Chromium Dissolved ND 00500 !> 0110612016 08·03 WG885472 Copper ,Dissolved ND 0.0500 5 07/06/2016 08:03 WG885472 Iron.Dissolved ND 0 500 s 07/06/2016 OB 03 WG885472 ACCOUNT PROJECT SOG: DATE/TIME. PAGE EnCana OU & Gas· Parachule. CO L844405 o7nV16 10:02 60117 20160628-HIME PIT W SAMPLE RES UL TS -01 Cotle c l @d da t e/llme : 06/28116 08 :15 L844405 Metals (ICP) by Method 60108 Result ~ RDL Dilullon Analysis Analyte mg/I mg/1 date/t me Lead.Dissolved ND 0.0250 5 07/0612016 08:03 Magn;;s um.Dissolved 25.9 5 00 5 07/06/2016 08:03 Manganese .OJssolved 0.286 0.0500 5 07/0612016 08:03 PoU!ss .im Dissolved 471 5 00 5 07/061201 6 08:03 Selen um Dissolved ND 0.0500 5 07/0612016 08:03 Silver ,D issolved ND O.o250 5 07/0612016 08:03 Sodium.Dissolved 6580 10.0 10 0710612016 10:54 Volatile Organic Compounds (GC) by Method RSK175 l!ewli ~ RDL Dilution Analysis Analyte mgn mg/1 date/tiflll! Methane 0 552 00100 07/05/2016 11 :12 Ethane t+D 0.0130 07105/2016 11:12 Ethene hD 0.0130 0710512016 11:12 Propane hD 0.0190 0710512016 11:12 Volatile Organic Compounds (GC/MS) by Method 82608 Resull ~ RDL Dilution Analysis Anolyte m ~/1 mg/1 date /tim e Benz ene 0 704 0100 100 07/07/2016 00 :51 Toluen e 212 0.500 100 07/0712016 00:51 Ethylbenzen e ND 0.100 100 07/0712016 00 :51 Tola! Xylenes 1.73 0.300 100 07/07/2016 00 :51 Methyl tcit -butyl eth ;:r ND 0100 100 07/07/2016 00 :51 (SJ Toluene-dB 107 90.0-115 07/0712016 00:51 (SJ D.bro mofluorcmNhane 107 790-111 07/0711016 00.51 (SJ 4-Bromonuorcbenzene 100 80.1-120 07/0712016 00.51 ACCOUNT: PROJECT: SOG: EnCana Oll & Gas· Parnchu1e, CO LB44405 Batch WG885472 WG885472 WG885472 WG885472 WG885472 WG885472 WG885472 Batch WG885857 WG885857 WG885857 WG885857 Batch WG886485 WG886485 WG886485 WG886485 WG886485 WG886485 WG886485 WG886485 ONE LAB , NATIONWIDE. • DATE/TIME : 07111/16 10:02 EJ ~ ~ EJ • ~ EJ EJ PAGE· 7 of17 20160628-HIME PIT MID SAMPLE RES UL TS -02 ONE LAB NATIONWIDE • Collecttd d•t 1t /llme : 0 $/28116 08 20 l84440S Gravimetric Analysis by Method 2540 C-2011 ~ ReslJll ~ ROL DJutlon Analysis B41Ch Ana~,.00 mDI! mg~ date/ lime ~ Dissolved Solids 1080 0 10 0 07/05/2016 09:36 \11GB85818 Wet Chemistry by Method 2320 B-2011 ~ Result ~ RDl Diiution Analysts Batch Analyte mg/I mg/I dcllc/timc ~ Alkollnily 682 20.0 0710712016 10:05 WG886222 Alkallnily.BicmboncJtc 614 20.0 07/0 7/2016 10:05 WG886222 • Alkalinily,Cmbonale 67 B 20 0 0110112016 m·os WG886222 Wet Chemistry by Method 350.1 ~ Result ~ RDl Diiution Anilfysls 8.'ltch Analyte mg.~ mg/I date/time EJ Ammonia Nillogen NO 0 250 07/081201612 06 VIG886594 Wet Chemistry by Method 450052 D-2011 EJ RMu• ~ RDL Dilu tion Analysts &ten Anal'f1e mg/I mg/I date/time Sulfdc 0.0660 d2 00500 0710112016 08 :29 WG884957 Wet Chemistry by Method 9040C Result ~ Diiution Analysis Bat ch Anal~e SU date/ l me pH 8.62 07/011201610:37 WG88 4!14.i1 Somple Narrative; 904JC L84440S-02 WG884851 8 62 at 8 lt Wet Chemistry by Method 9050A Result ~ Dilution Analys is Batch Analyte umM !.ICIT' elate /time Specific Conductance 281 00 07/011201612 47 WG88495S Wet Chemistry by Method 9056A Result ~ RDl Dllutlon Aoolysls Batch Analytc mg/I mg/I date/time B·o mldc 69.8 100 06130/2016 20:07 WG8848 l9 Chloride 10300 SOD 500 06130/2016 20 24 WG884839 Fluoride 1.30 0100 071081201615:27 WG886709 Nltrolecls (NJ ND 0100 06/3012016 20:07 WG884839 Nitrite a~ (NJ ND 0100 06/30i2016 20 ·01 WG884839 Sulfate 111 5.00 06130/2016 20 ·01 WG884839 Metals (ICP) by Method 60108 Result ~ RDl Dilution Analysts Batch Analyte mg/I mgn datc/tlmr Arscnlc.D ssolvcd NO 0.0500 5 07/061201 6 08 06 WG885472 Barium.Dissolved 351 0.0250 5 07/06/2016 OB 06 WG885472 Cadmium.Dissolved ND 00100 5 07/06/2016 08 06 WG885472 Calcium.Dissolved 39 5 ! 5.00 5 07/06/2016 08:06 WG885472 Chromium.Dissolved ND 00500 5 07/06/2016 08 06 WG885472 Copper.Dissolved ND 0.0500 5 07/06/2016 08:06 WG885472 Iron. Dissolved NO 0.500 s 07/06/2016 08:06 WG885472 ACCOUNT PROJECT. SOG; OATE/T1'4E PAGE EnCan!l OM & Gas · Parachute CO LB4440S 0711111610:02 Bof17 20160628-HIME PI T MI D SAMPLE RES UL TS -02 Collected da t e /t ime ; 06/28116 08 :20 Metals (ICP} by Method 60108 Result ~ RDL Analyte mg/I mg/I Lead,Dlssolved ND 00250 Magnesium.Dissolved 22 7 500 Manganese Dissolved ND 0.0500 Potassium, Dissolved 42 7 500 Selenium Dissolved ND 00500 Silver.Dissolved ND 00250 Sodium.Dissolved 6110 100 Volatile Organic Compounds (GC) by Method RSK175 Result Qualifier RDL Analyte mg/I mg/I Meth;me 00594 00100 Ethane ND 0.0130 Ethene ND 0.0130 Propane ND 0.0190 Volatile Organic Compounds (GC/MS) by Method 82608 Result 2!!2!!!!fil ROL Analyte mg/I mg/I Benzene ND O.OOIOO Toluene ND 0.00500 Ethylbenzene ND O.OOIOO Total Xylenes ND 0.00300 Methyl tert-butyl eth er ND 0.00100 (S) Toluene-dB 108 90.0-115 (S) Dibromoffuo1om ethan t' 109 790-121 (S) 4-Bromonuorobenzene 103 801-120 ACCOUNT: FR OJIECT: EnCana Oil & Gas· Pmachute, CO L844405 Dilution 5 5 5 5 5 5 10 Diiution OlluUon Analysts date ft 11\C' 07/0612016 08:06 07/0612016 08:06 07/0612016 08:06 07/0612016 08:06 07/06/2016 08:06 07/06/2016 08:06 07/06/2016 1146 Analysis date/time 07/05120161114 07/051201611:14 07/05/201611-14 07/051201611-14 Analysts d ate I !Im a 07/07/2016 01"11 07/07/2016 01:11 07/07/2016 01:11 07107/20!6 0111 07/07/20!6 0111 07/0712016 01:11 07/0712016 01.11 07/0712016 01.11 SDG l844405 Batch WG885472 WG885472 WG885472 WG885472 WG885472 WG885472 WG885472 Batch WGBBS857 WGBB5857 WG885857 WG885857 Batch WG886485 WG886485 WG886485 WG886485 WGB86485 WG886485 WGB86485 WGB86485 ONE LAB . NATIONWIDE. • ---- DATE/TIME: 07111116 10 02 ~ j2rc I ~ EJ • El EJ EJ PAGE: 9of17 20160628-HIME PIT NE SAMPLE RES UL TS -03 I • ONE LAB NATIONWIDE . Coll ec t ed date/t ime 061281 16 08 •25 L84 44 0 S Gravimetric Analysis by Method 2540 C-2011 EJ Result ~ ROL Ollutlon Analysis Batch Al\i!fyte mg/I !r.<}1 date/time ~ Dissolved Solids 12200 10 0 0710512016 09•36 YIG885818 Wet Chemistry by Method 2320 B-2011 ~ Res ult ~ ROL Dilution Analysis Batch Analyt e mgn mg/I date/tim ~ EJ Al kali nity 417 20 .0 07/07/2016 10 14 WG886222 Al kalln ily,Blcarbonate 383 20 .0 07107/2016 10 14 WG886222 • Al kalini ty , Carbonate 33 9 20 0 07/071201610 t4 WG 886222 Wet Chemistry by Method 350.1 El Result ~ ROL Dilution Analy sis Bal.di A."ll!l'fl e mon mg/I dateltme EJ AmmonLi Nitrogen NO 0250 07f081201612 08 WG886594 Wet Chemistry by Method 450052 D-2011 ~ Result ~ ROL Dluton Analysis B41tch Annfylt! rr~ mg/I date/lime Sulb NO 0.0500 07101/2016 08:30 WG88<t957 Wet Chemistry by Method 9040C Result ~ Dilution Analysis Bolcll An.ll~e SU date/time pH 8 74 07101/201610 37 WG884851 Sample Narrative: 9040C l8444 0S-03 WG884851 8 74 at 9 2c Wet Chemistry by Method 9050A Result ~ Dilution Analysis Batch Analyl e um hos/cm dateflimt> Specific Conductance 21400 07fOV201612'47 WG884955 Wet Chemistry by Method 9056A Result ~ ROL Dilution Analysis Batch Analyte mgn mg/I date/lime Bromide 58 4 1.00 I 06/30/2016 20:40 WG884839 Chloride 7490 100 100 06130/2016 20:57 WG884839 Fluoride 0 733 0100 07/08/2016 15 57 WG886709 Nitrate as (NI NO 0100 06130/2016 20:40 WG884839 Nitrite as (N) NO 0100 06130/2016 20 :40 WG884839 Sulfate 100 5 00 06130/2016 20 40 WG884839 Metals (ICP) by Method 60108 Result Oua~fier ROL OUution Analysis Bntch An~e mg.II mg/I date/tim e A1senlc.O ssolvcd NO 00500 s 07/0612016114 3 WG885472 Barium.Dissolved 49 2 0.0250 5 07106/20161143 WG885472 Cadmium.Dissolved NO 00100 s 07/06/2016 11 43 V/(;885472 Calclum.Dlssolved 501 5.00 5 07/06/201611 :43 WG885472 Chromium .Dissolv ed NO 00500 s 07106/201611:43 WG885472 Copper.Dissolved NO 0.0500 s 071061201611:43 WG885472 lion,Oissolved NO 0500 5 07/06/2016 11 43 WG885472 ACCOUNT: PROJECT. SDG: DATE/TIME PAGE· EnConil 011 & Gas • Parachute. CO L844405 071111161002 10 of17 2 0160628-HI ME PIT NE SAMPLE RESULTS -03 Collected datf/l lme : 06 /28 /16 08 .25 L8444 0 5 Metals (ICP) by Method 60108 Result ~ RDL Dllutlon Allillysls Analyte m :.-~ mgn date/time lead.Dissolved ND 00250 5 07/061201611:43 Mag oosium,Dissolvcd 17 2 5.00 5 07/061'201611:43 Manganesc.Dlssolved NO 00500 5 071061201611:43 Potassium.Dissolved 44 7 5.00 5 071061201611:43 Selen um Dlssolvecl ND 00500 5 071061201611:43 Silver .Olssolvecl ND 0.0250 5 0710612016 11:43 Socllum,DJssolved 4570 5.00 5 0710612016 11:43 Volatlle Organic Compounds (GC) by Method RSK175 Result ~ RDL Diiution Analysis lln.'llyte mgn mgn elate/time ._.ethanP 0 116 00100 07/05/201611'16 Ethane ND 00130 07/05/2016 1116 Ethenc ND 0 0130 07105/2016 11'16 Propane ND 00\90 07/05120161116 Volatile Organic Compounds (GC/MS) by Method 82608 Result ~ ROL Dilution Anolysts AMJyte crg/l mgn date/time Benzene ND 0 00100 07/07/20l6 01:30 Toluene ND 000500 07/07/2016 01:30 Ethylbcnzene ND 0.00100 0710712016 01'30 Totill Xylenes ND 0.00300 07/07/2016 01:30 Methyl tcrt·butyl ether ND 0 00100 07/07/2016 ot:30 (SJ Toluene-dB 107 90.0·115 0710712016 01:30 (SJ Dibromonvoromethane 108 79.0-121 07/0712016 01:30 {SJ 4-Bromonuorobenrene 102 80M20 07/0712016 01.30 ACCOUNT : PROJECT SDG: EnCana 011 & Gas • Pa111ctlutc. CO LB44405 Batch WG885472 WG885472 WG885472 WG885472 WG885472 WG885472 WG885472 Batch WG8858 57 WG885857 WG885857 WG885857 Batch WG886485 WG886485 WG886485 WG886485 WG886485 WG886485 WG886485 WG88648S ONE LAB NATIONWIDE • DATE/TIME 07n1r1610:02 EJ ~ El ~ • EJ El EJ PAGE: 11 of17 20160628-HIME PIT SE SAMPLE RESULTS -04 ONE LAB NATIONWID E • Co llect ed dale/time: 06/28/16 08 :30 l 8 444 0S Gravimetric Analysis by Method 2540 C-2011 B R~lt ~ RDL Diiution Ana lysis ll<l lth Anlllyte l"I~ mgJ1 date I time ~ Dissolved Solids 9660 10 0 07/05/2016 09"36 WG885818 Wet Chemistry by Method 2320 B-2011 ~ Result ~ ROL Dilutlon Analysis Batch Analyte mgn mg/I dat cl tme B Alkalinity 438 20 0 07/07/201610:22 WG886222 Alkalinity.Bicarbonate 342 200 07/07/2016 10:2 2 WG886222 • Alkalimly,Cmbonate 9S 7 200 07/07/2016 10. 22 WG886222 Wet Chemistry by Method 350.1 ~ Resull ~ RDL Dilution Analysts Bcllc'I Analyte "'91 mg/I dale/lime EJ Amm onlil Nitrogl!~ M> 0 250 07/08/201612 •14 WG886594 Wet Chemistry by Method 450052 D-2011 ~ ResvJt ~ RD L Dilution Analysis BB!ch Analyte mgn mg/I date /lime Sulfide 0.0710 0.0500 07/0V2016 08:30 WG884957 Wet Chemistry by Method 9040C Result ~ Dtluton Analysis B.ikh Analyte SU date/time pH 9.04 07/011201610 37 WG884851 Slllllple Narrative: 904 0C l844405-04 WG884851 9 04 at 8 !k Wet Chemistry by Method 9050A Result ~ Dlluton An alysis Ba tch Annlj11e umhos/cm date / time Specific Conductance 18600 07/0V2016 12;47 WG884955 Wet Chemistry by Method 9056A Result ~ RD L 0 lullon Analysis Batch Al!alyte mg/I mg/I date/time Bromide 47 8 100 1 06/30/2016 21 46 WG884839 Chloride 6380 100 100 06/30/2016 22:02 WG884839 Fluoride 0498 0100 06/30/2016 2146 WG884839 Nllrate as (N) ND 0100 06/30/2016 21'46 WG884839 Nrt111e as(N) ND 0100 06/30/2016 2146 WG884839 Sulfate 20 5 500 06/30/2016 2146 WG884839 Metals (ICP) by Method 60108 Result ~ RDL Dilution Analysis Balch Analvte mg/I mgn d.)tc /tim e Arscnlc,Olssolved ND 0.0500 5 07/0612016 08 09 WG885472 B111lum.Dlssolved 41 .4 0.0250 5 07/06/2016 08:09 WG885472 Cadmium Dissolved ND 0.0100 s 07/0612016 08 09 WG885472 Caklum.Olssolved 34 4 ~ 5.00 s 07106/2016 08 :09 WG885472 Chromium Dissolved ND 00500 !:. 07106/2016 OB 09 WG885472 Copper.Dissolved ND 0.0500 s 07/06/2016 OB 09 WG885472 lron,Ols~olvcd NO 0.500 5 07/06/2016 08 09 WG885472 ~CCOUNT PROJECT: SDG: DATE/TIME: PAGE EnCana 011 & Gas· Parochute, CO L844405 07nV16 I0·02 12of17 20160628-HIME PIT SE SAMPLE RES UL TS -04 Collected date/time · 06/2 B/16 08 :30 Metals (ICP) by Method 60108 Result Qualifier RDL Alla1yte ir!J.ll mg/I lead.Dissolved ND 0.0250 t4agncsium.D ssolved 14 4 500 Manganese.Dissolved ND 0.0500 Potasslum,Dissolwd 26 5 500 Selenium,Dlssolved ND 00500 Silver.Dissolv~·d ND 0 0250 Sodium Dlssolvt;d 3630 5.00 Volatile Organic Compounds (GC) by Method RSK175 R~u11 2!!2!!!!2! RDL Analyte mg/I mg/I Methane 0109 0.0100 Ethane ~D 0.0130 Ethenc ND 0.0130 Propane ND 00190 Volatile Organic Compounds (GC/MS) by Method 82608 Result Qualifier RDL .rtll~e 111gn mg/I -------- Bcnzcn o ND 0 00100 Toluene ND 000500 Ethylbenzene ND 000100 Total Xylenes ND 000300 Methyl ten·butyl cth m ND 0.00100 (S) Toluene-dB 106 90.(J..1/5 (S) Oibromof/uoromelhane 107 79 ()..121 (S) 4·8romofluorobenzene 101 80.1-120 ACCOUNT: PROJECT· EnCana Oil & Gas -Parachute, CO l84440S Dilution 5 5 5 5 5 5 5 Dilution Dilution Analysis dMe/time 07/06/2016 08:09 01m612016 os·o9 0110612016 oa·o9 07/0612016 08:09 07/06/2016 08:09 07I06 .'201 £ 08:09 07/06/2016 08•09 Analysis date/lime 07/05/2016 11:22 07/05/2016 11:22 07/05/2016 11 22 07/05/2016 11:22 Analysts datl'itime 07/07/2016 01 :50 07/0712016 01:50 0710712016 01 :50 07/0712016 01:50 0710712016 01:50 07/0712016 Ot.·50 07/0712016 01:50 07/0712016 01:50 SDG. l844405 Batch WG885472 WG885472 WG885472 WG885472 WG885472 WG885472 WG885472 Batch WG885857 WG885857 WG885857 WG885857 Balch WG886485 WG886485 WG886485 WG886485 WG886485 WG886485 WG886485 WG886485 ONE LAB . NATIONWIDE. • ~ l i Tc I ~ ~ • EJ EJ ~ ----------- DATE/TIME · 07mn6I002 PAGE; 13of 11 GLOSSARY OF TERMS ONE LAB NATIONWIDE. • Abbreviations and Definitions SDG RDL ND (S) Qualifier B JS ACCOUNT: EnCana O~ & Gas· Pnmchutc. CO Sample Delivery Group. Reported Detection Limit. Not detected at the Reporting Limit (or MDL where applicable) Surrogate (Surrogate Standard)-Analytes added lo every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate. used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected In all environmental media Description The same analyte is found in the associated blank The sample matrix Interfered with the ability to make any accurate determination: spike value Is low. PROJECT. SDG: L84440S DATEfTIME. 0 7'11;1& 10'()2 PAGE' 14of17 ACCREDITATIONS & LOCAT I O NS ONE LAB . NATIONWIDE • ESC Lab Sciences ls lhe cnly envuonme~tal laboratcry accredlledlcert1r1ed to sup:ort your wcr( nal1onW1de from one local1on One phone call, cne pcirt of cortact, one l1bcralory. No o··er tab Is as accessible or prepared to handle your needs throughout the couniry. Our cap<M;l!y and capab1hty flDm our single locauon laboratory Is comparable to the collecttve totals of lhe network laboratories In our industry The most slgn1hcant ecnef1t lo our "ooc lcca~on· design Is the design or our labomtc:y campus The r.:cdcl Is ccnduc1v~ to accelerated produ ~tiv1:y, decreasing turn-around time, and p1cvenung cmss contamlna!ion, thus protecting sample lnteguty. Our focus on premium qualrty and prompt service allows u~ to be YOUR LAB OF CHOICE.. • Nlot all certifications held by the labo1atory arc applicable to the 1csutts repelled In the anached repo1t. State Accred itations Alabama 40660 Alaska UST-080 Arizona AZ0612 Arkansas 88 -0469 California 01157CA Colorado TN00003 Connetlcut PH -0197 Florida E87487 Georgia NELAP Georgia 1 923 Idaho TN00003 Illinois 200008 Indiana C-TN 01 Iowa 364 Kansas E-10277 Kentucky r 90010 Kentucky 1 16 Louisiana Al30792 Maine TN0002 Maryland 324 Massachusetts M-TN003 Michigan 9958 Minnesota 047-999 ·395 Mississippi TN00003 Missouri 340 Montana CERT0086 Nebraska NE ·OS -15 -05 Third Party & Federal Accreditations A2LA -ISO 17025 A2LA -ISO 17025 ~ Canada EPA -Crypto 1461 Ot 1461 02 1461 01 TN00003 Nevada New Hampshire New Jersey -NELAP New Mex ico New York North Carol tna North Carolina t North Caro li na 1 North Dakota Oh o-VAP Oklahoma Oregon Pennsylvan ia R ~ode lsla r d South Caro ~na South Dakota Tennessee " Texas Texas ' Utah Vermont Vi rgin a Washington West Virg inia Wl 5consln Wyom rng Al HA DOD USDA 100789 1461 01 s 67674 ' 011nkmg Water 1 Underground Storage Tank~ 1 Aquatic Tc. <nv ' ChemlcaUM1croblological ' Mo.d •·• Amed1tat1on no! appltcable Our Locations TN ·03 -2002 -34 2975 TN002 TN00003 11742 Env375 DW2 1704 41 R-14 0 Cl0069 9915 TN200002 68 02979 221 84004 n/a 2006 T 104704245 07 TX LAB0152 6157585858 VT2006 109 C1915 233 9980939910 A2lA ESC Lab Sciences has s1xty-fo~r client suppcl! centeis that provi de sam:t e pickup and/or th e delivery or sa.,.phng supplies. If you wolJl d I •e as1111an:e from ooe or ou1 support o[hces please coetact our main clllci. ESC Lab Sciences JM!rforms all testing al our central laboratory. ACCOUNT: PROJECT: EnCana 011 & Gas · Parachute, CO SDG: L844405 DATE/TIME 07111116 1002 PAGE 150117 Encana·ou & Gas-Parachute, co 143 Dramond Avenue Parachute, CO 81635 BilnnB 1nfonnatlon: Accounts Payable 143 Diamond Avenue Parachute, CO 81635 Report to: 1 ;;~~;~~~~:~~~---. --I Brett Middleton Project JI fV'k.s,q City/State tJTf ~R{.D Desaiptlon: J /. )./ Collected: I Client Project II Phone: 97~285-2653 Uib Project If ENCANACO-NPR Fax: 97~625-4636 P.O.# Tr ' I Rush? flab MUST Be Notified) Date Results Needed _ s.me Day --··-··-·--.. 2Clln' _Not Day ··---·--·--···lllm' E~ll?_No X_Yes _T_ D'Y ·---··-·---~ I FAX? _No _Yes No. _Three l>av -·-·-·-----25" of Sample ID Comp/G~b Matrbl • Depth Date nme l:ntrs ' l20160628·HIME PIT W t1<.118 GW t-2"6--/t 0815 ' l}9- 20160628-HIME PIT MIO i£MB I GW ' 08~0 I 10 20160628-HIME PIT NE IL P.11B GW O'?aS-10 20160628-HIME PIT SE I. A.AA GW J /}R3n 10 I . Ana)Pls I Container I Pttservatlve l°'•ln or Cimody Pase_ of_ i • i I l I .I I I -ESC ~ ; 0 XJ ... ~ ~ %1 Q. 0 z Q z . ::c • w e "' Q. Q. c...'L Q u g Q ::c ::c E :c N E • I .0 m 0 11'1 E 0 C) Xl N an ,... < z N :c ~ e ~ • ' 0 .!!J ""' ll.i: 0 I nl Q. ...J ..,. I ~ Q ~ I f6 ., ::c ~ e iii N i ~· ; ~ Ill N -rl " ~ o . 0 "' m -::-.,. ::c ~ ~ c I a> z x x x x x x x x x x x x x x )( )( x x x x ~ ... u ~ < 0 z i w Q. Q 0 ::c IS e z 0 -? &n N ::c .D l"1 .a ~ "' E ~ E ~ E "' -N z 0 '°"I ~ ..,. w 11'1 9 ~ "' ... ..... ' ·¥ -' -~ :::> ::c "' CL x x x x x x x x x -x 'X x L•A•ll S •C •l •IP;•N•C•C•9 VOUA ~All er e1<1QlC:C U06S ... _lld II _...,llj57UJ ,._, 11HSl-S151 -ll00-7'7-511St • hr6U-~ • l# L015 Acctnum: ENCANACO Temptate,n13507 Prelasin:,PS58630 TSR: HI· Jamd Wllfls PB: Shipped Via ~ ~ .. ,~ ...... ..,,.., -e;I ,, D t\\J \J-)t>-l(o pH Temp ___ _ utt4 s t9"3'\ \ '-\, aB Matrix: SS · Soll GW • GroundW3ter WW · Wastewater OW· Drinking Water OT· Other ___ _ emarks:NITRATE ONLY HAS A 48-HOUR HOLD TIME. issolved Metals= As, Ba, Cd, Cr, Cu, Pb, Ag, Ca, Fe, K, Mg, Mn, Na, Se. Time: /()."30 Time: ,I Received by: 2~ ... Flow Other ___ _ Samples returned via: 0 UPS a FedEx a Courier a Te!"'?: d .(' Date. _)a..\.~ -C Bottles RecefYed: l...\.'O llme· ~ ar:C9o ~ ~o-l (, Wold 11 Condition: CDC Seal Intact: pHO\ed:ed. LI flab use oil~ -1 .) ~w y N NA .• NO:: Jeremx W. Watkins ESC Lab Sciences Non-Conformance Form Logfn#:~S Client: ENCANACO Date: 6/30/16 Non-conformance (check a :>pUcable ttemsJ -sample, Integrity Chain of Custody Clarification -- Parameter(s} past holding Evaluated ljy: Jeremy -- x time Lo1dn Clarifit"41tion Needed If Broken Container: ·--_ __J Improper temperature Chain of custodv Is incomoletc Insufficient oacklnit material around container Improper container Please specify Metals requested Insufficient packing material Inside type cooler Improper preservation Please specify TCLP requested. lmoroocr handling bv carrier (FedEx I UPS I Courie Received additional samples not listed on coc. Sample was Insufficient sample volume. frozen Sample Is blphasic. Sample ids on containers do not match Ids on coc Container lid not Intact .. Vials received with headspace. Trip Blank not received . lfno Chain of<!ustody: - Broken container Client did not ·x· analysis. Received by: lC Broken container. Chai n ofC ustodv is missi nl! Datefflme: lC sufficient sample remains Temp./Cont Rec./pH ; Carrier: Tracltinl!# Lown Comments: 1. Received 1-40ml ylal broken for HIME PIT w. 3 Remains 2. NITRATE and NITRITE received Out of Hold Client Informed bv: Ca11X Email Vol<ie Mail .Time: 1130 TSR Initials: IW Client Contact: Chris Hine s Login Instructions: 1. Proceed with remaining In-tact vials. Enough remain for the analyses. 2. Add one hour to collection time to account for the time difference. Samples were collected on Mountain Time and are being analyzed on Central Time. Analyze ASAP and qualify accordingly. This E-mail and any attached files nre confidential, and may be copyright protected. If you are not the addressee, any dissemination of this communication Is strictly prohibited. If you have received this message In error, please contact the sender immediately nnd delete/destroy all Information received .' ' J • ~ I