HomeMy WebLinkAbout1.07 General Application Materials_Part8Client Sample ID :
Lab Sample ID :
Date Collected :
Date Received :
Date Prepared :
Date Analyzed :
Percent Moisture :
P3C6HSI
0l-6007-0lA
tU0U200t
tt/02t2001
tt/0612001
ty09l200t
28.51
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Project ID : Unocal Parachute
Lab Work Order : 01-6007
Sample Matrix : Soil
Lab File ID : GCMSIl08\3001030.D
Method Blank : MB-10506
Prep Factor : 333.11125976056
Effective Dilution : 6.99
Method: SW8270C 827OC Hazardous Substance List Units:us/Ks
Analyte cAs #Concentration RL POL
Acenaphthene
Acenaphthylene
Anthracene
Benzo(b&k)fl uoranthene
Benzo(a)anthracene
83-32-9
208-96-8
120-12-7
205-99-2+k
56-55-3
1600
2500
3900
7100
3900
12000
1 2000
12000
23000
1 2000
I
Benzo(a)pyrene
Benzo(g,h,i)perylene
Benzoic acid
Benzyl alcohol
Bis(2-chlo roethyl)ether
50-32-8
191-24-2
65-85-0
100-51-6
111-44-4
4100
4000
1 3000
3600
3500
Bis(2-chloroeth oxy)meth ane
Dichlorodiisopropyl ether
Bis(2-ethylhexyl)phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
1 800
4500
4900
4600
4600
12000
12000
12000
12000
12000
111-91-1
1 08-60-1
117-81-7
I 01-55-3
85-68-7
4-Chloroanlline
4-Chlo ro-3-m ethylph enol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
4400
5000
2400
3000
3500
12000
12000
I 2000
12000
12000
106-47-8
59-50-7
91-58-7
95-57-8
7005-72-3
Chrysene
Dibenz(a, h)anthracene
Dibenzofuran
DFn-butylphthalate
1,2-Dichlorobenzene
3900
4500
2600
4300
31 00
12000
12000
12000
12000
12000
218-01-9
53-70-3
132-64-9
84-74-2
95-50-1
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3, 3' -Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
541-73-1
106-46-7
91-94-1
120-83-2
84-66-2
4400
31 00
14000
31 00
3600
12000
1 2000
23000
12000
12000
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-methylphen ol
2,4-Dinitrophenol
2,4-Dinitrotoluene
1 05-67-9
1 31-1 1-3
534-52-1
51-28-5
121-14-2
6600
4000
8700
12000
3200
12000
12000
12000
23000
12000
I
2,6-Dinitrotoluene
Di-n-octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
606-20-2
117-84-0
206-44-O
86-73-7
118-74-1
5600
41 00
4000
2400
2100
12000
12000
12000
12000
1 2000
Hexachlorobutadiene 87-68-3 3900 '12000
U - Not Detected atlhe Reporting Limit (RL)
J - Analyte detected below Practical Quantitation Limit (PQL)
E - Extrapolated value. See rerun at dilution.
B - Anallte detected in the associated Method Blank
il-
S - Spike Recovery outside accepted recovery limits
| - Compound detecte.d above regulatory limit.
X - Poor surrogate recovery due to high dilution.
/<
Qunlifiers:
ffi"tyrt Approved I 1/09/2001 2:59 PM
I 12000
12000
23000
12000
12000
I
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Sample ID :
Lab Sample ID :
Date Collected :
Date Received :
Date Prepared :
Date Analyzed :
Percent Moisfure :
P3C6HSI
0l-6007-01A
tr/01/2001
1710212001
tU06l200r
tU09/2001
28.51
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSI108\3001030.D
Method Blank : MB-10506
Prep Factor : 333.1 1125916056
Effective Dilution : 6.99
Method: SW8270C 827OC Hazardous Substance List Units: pS/KS
Analyte CAS #Concentration RL POL
H exachlorocyclo pentadiene
Hexachloroethane
lndeno( 1,2, 3-cd)pyrene
lsophorone
77-47-4
67-72-1
1 93-39-5
78-59-1
31 00
3300
41 00
2300
1 2000
12000
12000
12000
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline
2200
7700
5300
2600
4300
12000
12000
12000
12000
12000
91-57-6
95-48-7
106-44-5
91-20-3
88-74-4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
51 00
4100
2600
3200
9300
12000
12000
12000
12000
12000
N-Nitrosodiph enylamin e
N-Nitrosodipro pylamin e
Pentachlorophenol
Phenanthrene
Phenol
4000
2200
7300
2600
2900
12000
12000
12000
12000
12000
86-30-6
621-64-7
87-86-5
85-01-8
1 08-95-2
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2900
3700
5600
4700
12000
12000
12000
12000
129-00-0
120-82-1
95-95-4
88-06-2
Surrogate Recovery
2-Fluorophenol
Phenol-d6
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-d14
124o/o
o%
117%
99%
560/o
104%
QC LimitsI - 119
11 - 115
18 - 120
26 - 115
7-129
7-125
SX
SX
X
X
X
X
I
U - Not Detected atthe Reporting Limit (RL)
J - Analyte detected below Practical Quantitation Limit (PQL)
E - Extrapolated value. See rerun al dilution.
B - Andvte detected in the associated Melhod Blankb
S - Spike Recovery outside accepted recovery limits
* - Compound detected above rogulatory limit.
X - Poor surrogate recovery due to high dilution.
/?,e/Q
e.qtifiers:
Analyst Approved 1l/09/2001 2:59PM
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-602t
Client Sample ID : P3C6GL3
Lab Sample ID : 0l-6007-024
Date Collected : ll/0112001
Date Received : ll/02/2001
Date Prepared z ll/0612001
Date Analyzed : lll07/2001
Percent Moisture : 12.'71
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab Fite ID : GCMSIl0T\1301006.D
Method Blank : MB-10506
Prep Factor : 33.178500331785
Effective Dilution : l.14
Method: SW8270C 827OC Hazardous Substance List Units: pg/Kg
Analyte CAS #Concentration RL POL
Acenaphthene
Acenaphthylene
Anthracene
Benzo(b&k)fl uoranthene
Benzo(a)anthracene
26
40
63
120
64
190
190
190
380
190
83-32-9
208-96-8
120-12-7
205-99-2+k
56-55-3
Benzo(a)pyrene
Benzo(g,h,i)perylene
Benzoic acid
Benzyl alcohol
Bis(2-chloroethyl)ether
50-32-8
191-24-2
65-85-0
100-51-6
111-44-4
67
66
210
59
57
190
190
380
190
190
Bis(2-chloroethoxy)methane
Dlchlorodiisopropyl ether
Bis(2-ethyl h exyl ) p hth alate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
29
73
81
75
75
190
190
190
190
190
111-91-1
1 08-60-1
117-81-7
1 01-55-3
85-68-7
190
190
190
190
190
4-Chloroaniline
4-C hloro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
10647-8
59-50-7
91-58-7
95-57-8
7005-72-3
71
82
39
48
56
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
218-01-9
53-70-3
132-64-9
84-74-2
95-50-1
64
t5
43
70
50
190
190
190
190
190
'l ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
3, 3' -Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
72
51
230
50
58
190
190
380
190
190
541-73-1
106-46-7
91-94-1
120-83-2
84-66-2
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
110
65
140
200
53
190
190
190
380
190
1 05-67-9
131-11-3
534-52-1
51-28-5
121-14-2
2,6-Dinitrotoluene
Di-n-octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
606-20-2
117-84-0
20644-O
86-73-7
118-74-1
92
66
66
39
34
190
190
190
190
190
Hexachlorobutadiene 87-68-3 64 190
U - Not Detected al the RepoAing Limit (RL)
J - Analyte dstectod below Practical Quantitation Limit (PQL)
E - Extrapolaled value. See rerun al dilution.
B - Andyte detect€d inilre associated Method Blank
S - Spike Recovery outside accepted recovery limits
t - Compound delected above regulatory limit.
X - Not Applicable.
il*
Quqlifters:
Analyst 1 U042001 9:3i AM
\
Chrysene
Dibenz(a, h)anthracene
Dibenzofuran
Di-n-butylphthalate
1 ,2-Dichlorobenzene
,oa/<
'A[proved
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Sample ID : P3C6GL3
Lab Sample ID : 0l-6007-02A
DateCollected : ll/01/2001
Date Received : ll/02/2001
Date Prepared : 11106/2001
Date Analyzed : lll07l200l
Percent Moisture : 12.77
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSI107\1301006.D
Method Blank : MB-10506
Prep Factor : 33.178500331785
Effective Dilution : 1.14
Method: SW8270C 8270C Hazardous Substance List Units: pg/KS
Analyte cAs #Concentration RL PQL
H exachlorocyclopentadiene
Hexachloroethane
lndeno( 1,2,3-cd)pyrene
lsophorone
51
53
67
38
190
190
190
190
77-47-4
67-72-1
'193-39-5
78-59-1
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline
91-57-6
95-48-7
10644-5
91-20-3
88-744
1
36
30
87
43
70
190
190
190
190
190
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
83
67
42
52
150
190
190
190
190
190
N-Nitrosodiph enylamine
N-Nitrosodipropylamine
Pentachlorophenol
Phenanthrene
Phenol
66
36
120
43
47
190
190
190
190
190
86-30-6
621-64-7
87-86-5
85-01-8
'108-95-2
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1 29-00-0
120-82-1
95-95-4
88-06-2
47
61
92
76
190
190
190
190
Surrogate Recovery
2-Fluorophenol
Phenol-d6
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-d14
60o/o
71%
65o/o
65%
58o/o
83%
QC Limits
9 - 119
11 - 115
18 - 120
26 - 115
7-129
7-125
U - Not Detected a1lhe Reporting Limit (RL)
J - Analyte detected below Prac'tical Quartilation Limil (PQL)
E - E:<fapolafed value. See rerun at dilution.
B - Analyte detectcd inthe associated Method Blank
S - Spiko Recovery outside accepted recovery limits
| - Compound detected above regulalory limit.
X - Not fuplicable.
F
Qualiflers:
Analyst Approved l1/0U2001 9: ji AM
-t
I
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Sample ID : P3Cl2GL5
Lab Sample ID : 016007-03A
Date Collected : l1/01/2001
Date Received : lll02l200l
Date Prepared : ll/06/2001
Date Analyzed : lll07/2007
Percent Moisture : 12.91
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSIl0T\1401007.D
Method Blank : MB-10506
PrepFactor :33.3333333333333
Effective Dilution : l.14
Method: SW8270C 827OC Hazardous Substance List Units: pS/Kg
Analyte CAS #Concentration RL POL
Acenaphthene
Acenaphthylene
Anthracene
Benzo( b&k)lluoranthene
Benzo(a)anthracene
26
41
64
120
65
190
190
190
380
190
83-32-9
208-96-8
120-12-7
205-99-2+k
56-55-3
190
190
380
190
190
Benzo(a)pyrene
Benzo(g,h,i)perylene
Benzoic acid
Benzyl alcohol
Bis(2-chloroethyl)ether
50-32-8
191-24-2
65-85-0
100-51-6
111-444
67
66
t10
60
58
2
Bis(2-chloroethoxy)meth ane
Dichlorodiisopropyl ether
Bis(2-ethylhexyl)phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
29
74
81
75
75
190
190
190
190
190
111-91-1
108-60-1
117-81-7
101-55-3
85-68-7
4-Chloroaniline
4-Chloro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chloropt enylphenyl ether
'106-47-8
59-50-7
91-58-7
95-57-8
7005-72-3
72
83
39
49
57
190
190
190
190
190
Chrysene
Dibenz(a, h )anthracene
Dibenzofuran
Di-n-butylphthalate
1,2-Dichlorobenzene
65
73
43
70
51
190
190
190
190
190
218-01-9
53-70-3
132-64-9
84-74-2
95-50-1
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3' -Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
541-73-1
106-46-7
91-94-1
120-83-2
84-66-2
73
51
230
50
59
190
190
380
190
190
2,4-Dimeth9phenol
Dimethylphthalate
4,6-Dinitro-2-methylph enol
2,4-Dinitrophenol
2,4-Dinitrotoluene
10567-9
131-11-3
534-52-1
51-28-5
121-14-2
110
66
140
200
53
190
190
190
380
190
2,6-Dinitrotoluene
Di-n-octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
606-20-2
117-84-0
20644-0
86-73-7
118-74-1
92
67
oo
39
35
190
190
190
190
190
Hexachlorobutadiene 87-68-3 65 190
U - Not Detec&d atthe Reporting Limit (RL)
J - An lyte det€€ted bolow Praaical Quarnftation Limil (PQL)
E - E:<trapolated value. See rerun at dilution.
B - Andyt€ dstected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
* - Compound detected above regulatory limit.
X - Not Applicable.
,EAKtL
Q ''liffers:
Analyst Approved 1 l/08/2001 9:33 AM
\
t
I
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client $ample ID :
Lab Sample ID :
Date Collected :
Date Received :
Date Prepared :
Date Analyzed :
Percent Moisture:
P3CI2GL5
0l-6007-03A
lt/0r/2001
tu02t200t
tt/06t2001
ty0'112001
12.91
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSI107\1401007.D
Method Blank : MB-10506
Prep Factor : 33.3333333333333
Effective Dilution : 1.14
Method: SW8270C 8270C Hazardous Substance List Units: rc/Kg
Analyte CAS #Concentration RL PQL
Hexachlo rocyclo pentadiene
Hexachloroethane
lndeno( 1,2, 3-cd)pyrene
lsophorone
77474
67-72-1
1 93-39-5
78-59-1
51
53
68
38
190
190
190
190
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline
9'1-57-6
95-48-7
1 06-44-5
91-20-3
88-744
37
'130
87
43
71
190
190
'190
190
190
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
99-09-2
100-01€
98-95-3
88-75-5
100-02-7
84
67
42
52
150
190
190
190
190
190
N-Nitrosodiphenylamine
N-Nitrosodipropylamine
Pentachlorophenol
Phenanthrene
Phenol
86-30-6
621-64-7
87-86-5
85-01-8
1 08-95-2
66
50
20
43
47
1
190
190
190
190
190
Pyrene
1,2,4-Trichlorobenzene
2, 4, 5-Trichlo ro ph en ol
2,4,6-Trichlorophen ol
129-00-0
120-82-1
95-95-4
88-06-2
47
61
92
77
190
190
190
190
Surrogate Recovery
2-Fluorophenol
Phenol-d6
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-d14
52%
60o/o
56%
63o/o
67o/o
76o/o
QC Limits
9 - 119
11 - 115
18 - 120
26 - 115
7-129
7-125
U - Not Dctected atthe Reporting Limit (RL)
J - Analyt€ dctected below Practical Quantitation Limit (PQL)
E - Extrapolated value. Seo rerun at dilution
B - Analvte detectcd in the associarcd Method Blark
tb
S - Spike Recovery outside accepted rccovery limits
* - Compound detected above regulatory limit.
X - Not Applicabie.
Quqlilier:s:
Analyst Approved 1 l/08/2001 9:33 AM
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Sample ID : P3Cl lHS2
Lab Sample ID : 0l-6007-04A
DateCollected : ll/01/2001
Date Received : lll02l200l
Date Prepared : 11106/2001
Date Analyzed : ll/09/200l
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSll0S\3101031.D
Method Blank : MB-10506
PrepFactor :333.333333333333
Effective Dilution : 6.08Percent Moisture : 17.85
Method: SW8270C 8270C Hazardous Substance List Units: pg/Kg
Analyte CAS #Concentration RL POL
Acenaphthene
Acenaphthylene
Anthracene
Benzo(b&k)fl uoranthene
Benzo(a)anthracene
1 400
2200
3400
6200
3400
1 0000
1 0000
1 0000
20000
1 0000
83-32-9
208-96-8
120-12-7
205-99-2+k
56-55-3
Benzo(a)pyrene
Benzo(g,h,i)perylene
Benzoic acid
Benzyl alcohol
3600
3500
1 1000
3200
3100
1 0000
1 0000
20000
1 0000
1 0000Bis(2-chloro ethyl)ether
50-32-8
191-24-2
65-85-0
100-51-6
111-44-4
Bis(2-chloroeth oxy)methan e
Dichlorodiisopropyl ether
Bis(2-ethylheryl)phth alate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
1 500
3900
4300
4000
4000
1 0000
1 0000
1 0000
1 0000
'10000
111-91-1
1 08-60-1
117-81-7
1 01 -55-3
85-68-7
4-Chloroaniline
4-Chloro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl ether
Chrysene
Dibenz(a, h)anthracene
Dibenzofuran
Di-n-butylphthalate
1,2-Dichlorobenzene
3400
3900
2300
3700
2700
't0000
1 0000
1 0000
1 0000
1 0000
106-47-8
59-50-7
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
84-74-2
95-50-'t
3800
4400
2100
2600
3000
1 0000
1 0000
'10000
1 0000
1 0000
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3' -Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
541-73-1
106-46-7
91-94-1
120-83-2
84-66-2
3900
2700
12000
2700
31 00
1 0000
1 0000
20000
1 0000
1 0000
2,4-Dimethylphenol
Dimethylphthalate
4, 6-Dinitro-2-m ethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
5800
3500
7600
11000
2800
1 0000
1 0000
1 0000
20000
1 0000
1 05-67-9
1 31-1 'l -3
534-52-1
51-28-5
121-14-2
2,6-Dinitrotoluene
Di-n-octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
4900
3500
3500
2100
1 800
1 0000
1 0000
1 0000
1 0000
1 0000
606-20-2
117-84-O
20644-0
86-73-7
118-74-1
Hexachlorobutadiene 87-68-3 3400 1 0000
U - Not Detected at the Reporting Limit (RL)
J - Analyte detected below Practical Quantilation Limit (PQL)
E - Extrapolated value. See rerun at dilution.
B - Analle detected in the associaled Method Blank
.h_ t,'
S - Spike Recovery outside accepted recovery limits
| - Compound detected above regulatory limit.
X - Poor surrogate recovery due to high dilution.
IPA,K
Qualifiers:
Analyst Approved 11/09/2001 3:10PM
I
\
I
I
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Sample ID : P3CllHS2
Lab Sample ID : 01-6007-04A
Date Collected : lll0ll200l
Date Received : lll02l200l
Date Prepared : 7110612001
Date Analyzed : 1110912001
Percent Moisture : 17.85
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSll08\3101031.D
Method Blank : MB-10506
PrepFactor :333.333333333333
Effective Dilution : 6.08
Method: SW8270C 8270C Hazardous Substance List Units: pg/Kg
Analyte CAS #Concentration RL PQL
H exachlorocyclopentadiene
Hexachloroethane
lndeno( 1,2,3-cd)pyrene
lsophorone
77-474
67-72-1
1 93-39-5
78-59-1
2700
2800
3600
2000
1 0000
1 0000
1 0000
1 0000
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline
1 900
6700
4600
2300
3800
1 0000
1 0000
1 0000
1 0000
1 0000
91-57-6
95-48-7
1 06-44-5
91-20-3
88-74-4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
4400
3600
2200
2800
81 00
1 0000
'10000
1 0000
1 0000
1 0000
N-Nitrosodiphenylamine
N-Nitrosodipropylamin e
Pentachlorophenol
Phenanthrene
Phenol
3500
1 900
6300
2300
2500
1 0000
1 0000
1 0000
1 0000
1 0000
86-30-6
621-64-7
87-86-5
85-0 1 -8
1 08-95-2
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
129-00-0
120-82-1
95-95-4
88-06-2
2500
3200
4900
41 00
1 0000
1 0000
1 0000
1 0000,6-Trichlo enol
Surrogate
2-Fluorophenol
Phenol-d6
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-d14
1O2o/o
0o/o
98%
97o/o
47%
98%
X
SX
X
X
X
X
QC LimitsI - '119
11 - 115
18 - 120
26 - 115
7-129
7-125
U - Not Detected at rhe Reporting Limit (RL)
J - Anelyte detecled below Practical Quanlilalion Limit (PQL)
E - Extrapolated value. See rErun at dilution.
B - Analyte detected inlhe associaled Metrod Blank
h
S - Spike Recovery outside accepted recovery limits
* - Compound detected above regulatory limit.
X - Poor surrogale recovery due to high dilution.
nbK
Qrrelifis13;
Analyst Approved 11/09/2001 3:l0PM
I
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Sample ID : P3CllGL8
Lab Sample ID : 0l-6007-054
DateCollected : ll/01/2001
Date Received : ll/02/2001
Date Prepared : ll/0612001
Date Analyzed : lll07l200l
Percent Moisture : 13.02
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSI107\1601009.D
Method Blank : MB-10506
Prep Factor : 33.0906684315023
Effective Dilution : 1.14
Method: SW8270C 827OC Hazardous Substance List Units:pg/Kg
Analyte CAS #Concentration RL PQL
t
I
.J
Acenaphthene
Acenaphthylene
Anthracene
Benzo(b&k)fl uoranthene
Benzo(a)anthracene
26
40
63
120
64
190
190
190
380
190
83-32-9
208-96-8
120-12-7
205-99-2+k
56-5s-3
Benzo(a)pyrene
Benzo(g,h,i)perylene
Benzoic acid
Benzyl alcohol
Bis(2-chloroethyl)eth er
50-32-8
191-24-2
65-85-0
100-51-6
111-44-4
2
67
66
t10
59
57
190
190
380
190
190
Bis(2-chlo roethoxy)methan e
Dichlorodiisopropyl ether
Bis(2-ethylhexyl)phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
29
74
81
75
75
190
190
190
190
190
1 1 1-91-1
1 08-60-1
117-81-7
101-55-3
85-68-7
4-Chloroaniline
4-Chloro-3-methylphen ol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
72
82
39
48
56
190
190
190
190
190
10647-8
59-50-7
91-58-7
95-57-8
7005-72-3
Chrysene
Dibenz(a, h)anthracene
Dibenzofuran
Di-n-butylphthalate
1,2-Dichlorobenzene
64
73
43
70
50
190
190
190
190
'190
218-01-9
53-70-3
132-64-9
84-74-2
95-50-1
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
(r
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3, 3' -Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
72
51
230
50
58
190
190
380
190
190
541-73-1
106-46-7
91-94-1
120-83-2
84-66-2
2,4-Dimethylphenol
Dimethylphthalate
4, 6-Dinitro-2-m ethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
110
65
140
200
53
190
190
190
380
190
1 05-67-9
131-1 1-3
534-52-1
51-28-5
121-14-2
2,6-Dinitrotoluene
Di-n-oc$phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
606-20-2
117-84-0
20644-0
86-73-7
118-74-1
92
66
66
39
34
190
190
190
190
190
Hexachlorobutadiene 87-68-3 64 190
U - Not Dstlcted al the Reporting Limit (RL)
J - Analyte detected below Practical Quantitation Limit (PQL)
E - Extrapolated value. See rerun al dilution.
B - tualyte dste*a i.ffi*iated MethodBlank
S - Spike Recovery outside accepted recovery limits
* - Compound detected above regulatory limit.
X - Not Applicable.
/ue
Q.qtifiers:
Analyst Approved I l/0U2001 9:33 AM
I
I
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 425-6021
Client Sample ID :
Lab Sample ID :
Date Collected :
Date Received :
Date Prepared :
Date Analyzed :
P3CI IGL8
0l-6007-05A
tU0U200r
tU02t200t
tu06t200t
7t/07t2001
t3.02PercentMoisture:
Client Project [D : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSl107\1601009.D
Method Blank : MB-10506
Prep Factor : 33.0906684315023
Effective Dilution : 1.14
Method: SW8270C 827OC Hazardous Substance List Units: pg/KS
Analyte CAS #Concentration RL POL
Hexachlo rocyclopentadien e
Hexachloroethane
lndeno( 1,2, 3-cd)pyrene
lsophorone
77-474
67-72-1
1 93-39-5
78-59-1
51
53
ot
38
190
190
190
190
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline
36
130
87
43
70
190
190
190
190
190
91-57-6
9548-7
10644-5
91-20-3
88-74-4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
83
67
42
52
150
190
190
190
190
190
N-Nitrosodiphenylamin e
N-Nitrosodipro pylamin e
Pentachlorophenol
Phenanthrene
Phenol
86-30-6
621-64-7
87-86-5
85-01-8
1 08-95-2
bb
36
120
43
47
190
190
190
190
190
Pyrene
1,2,4-Trichlorobenzene
2,4, 5-Trichlorophenol
2,4,6-Trichlorophenol
129-00-0
120-82-1
95-95-4
88-06-2
47
61
92
76
190
190
190
190
Surrogate Recovery
2-Fluorophenol
Phenol-d6
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-d14
61o/o
64%
69o/o
67o/o
75%
83%
QC Limits
9 - 119
11 - 115
18 - 120
26 - 115
7-129
7-125
l2
U - Not Detected atlhe Reporting Limit (RL)
J - Analyte dct cted below Practical Quantitation Limit (PQL)
E - Extrapolaled value. See rerun at dilution.
B - Analyte detected the associated Method Blank
S - Spike Recovery outside aocepted recovery limits
I - Compound detecled above regulatory limit.
X - Not Applicable.
Qrrdiffels:
Analyst Approved 11/0U2001 9:33 AM
I
P*r
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Sample ID :
Lab Sample ID :
Date Collected :
Date Received :
Date Prepared :
Date Analyzed :
Percent Moisture :
P3CIOHS3
0l-6007-06A
tU0U200l
1t/0212001
tt/06t2001
tU09l200r
17.05
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSIl08\3201032.D
Method Blank : MB-10506
Prep Factor z 165.72754391'7199
Effective Dilution : 1.2
Method: SW8270C 827OC Hazardous Substance List Units: US/Kg
Analyte CAS #Concentration RL PQL
130
210
330
610
340
Acenaphthene
Acenaphthylene
Anthracene
Benzo(b&k)fl uoranthene
Benzo(a)anthracene
83-32-9
208-96-8
120-12-7
205-99-2+k
56-5s-3
990
990
990
2000
990
Benzo(a)pyrene
Benzo(g,h,i)perylene
Benzoic acid
Benzyl alcohol
Bis(2-chlo roethyl)ether
50-32-8
191-24-2
65-85-0
100-51-6
111-444
350
350
1 100
310
300
990
990
2000
990
990
Bis(2-chlo roeth oxy)methane
Dichlorodiisopropyl ether
Bis(2-ethylh exyl)phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
111-91-1
1 08-60-1
117 -81-7
1 01 -55-3
85-68-7
990
990
990
990
990
150
390
420
390
390
4-Chloroaniline
4-Chlo ro-3-methyl phen ol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
106-47-8
59-50-7
91-58-7
9s-57-8
7005-72-3
380
430
200
250
300
990
990
990
990
990
Chrysene
Dlbenz(a, h)anth racene
Dibenzofuran
Di-n-butylphthalate
1,2-Dichlorobenzene
218-01-9
53-70-3
132-64-9
84-74-2
95-50-1
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
990
990
990
990
990
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3, 3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
541-73-1
106-46-7
91 -94-1
120-83-2
84-66-2
380
270
1200
260
3'10
990
990
2000
990
990
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-m ethylphen ol
2,4-Dinitrophenol
2,4-Dinitrotoluene
1 05-67-9
1 31-1 1-3
534-52-1
51-28-5
121-14-2
570
340
750
1 100
280
990
990
990
2000
990
2,6-Dinitrotoluene
Di-n-octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
480
350
350
200
180
990
990
990
990
990
606-20-2
117-84-0
20644-0
86-73-7
118-74-1
Hexachlorobutadiene 87-68-3 340 990
U - Not Detrctld at the Reporting Limit (RL)
J - Analyte detected below Praclical Quantitation Limit (PQL)
E - Extrapolated value. See rerun at dilution.
B - Analvte det€cted inthe associated Method Blank't tb
S - Spike Recovery outside accepted recovery limits
* - Compound detected above regulatory limit.
X - Not Applicable.
N*tc
Qualifiers:
Analyst Approved 11/09/2001 4:01 PM
340
380
220
370
260
Client Sample ID :
Lab Sample ID :
Date Collected :
Date Received :
Date Prepared :
Date Analyzed :
Percent Moisture
P3CIOHS3
0l-6007-064
tu0r/200t
rU02t200t
Lu06t200t
tU09/2001
17.05
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 425-6021
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSI108\3201032.D
Method Blank : MB-10506
Prep Factor : 165.72'754391'7799
Effective Dilution : 1.2
)
Method: SW8270C 827OC Hazardous Substance List Units: pg/Kg
Analyte CAS #Concentration RL POL
Hexachlorocyclopentadien e
Hexachloroethane
lndeno( 1,2, 3-cd)pyrene
lsophorone
77474
67-72-1
1 93-39-5
78-59-1
270
280
350
200
990
990
990
990
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline
91-57-6
95-48-7
10644-5
91-20-3
88-74-4
I
190
660
460
220
370
990
990
990
990
990
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
990
990
990
990
990
440
350
220
270
800
N-Nitrosodiphenylamine
N-Nitrosodipropylamine
Pentachlorophenol
Phenanthrene
Phenol
340
190
620
230
240
990
990
990
990
990
86-30-6
621-64-7
87-86-5
85-01-8
1 08-95-2
Pyrene
1,2,4-Trichlorobenzene
2,4, 5-Trichlorophenol
2,4,6-Trichlorophenol
250
320
480
400
990
990
990
990
Surrogate Recovery
2-Fluorophenol
Phenol-d6
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-d14
87%
72%
91%
87%
67o/o
92o/o
QG Limits
9 - 119
11 - 115
18 - 120
26 - 115
7-129
7-125
U - Not Detected at the Reporting Limit (RL)
J - Analyte detected below Practical Quantitation Limit (PQL)
E - Extrapolated value. See rerun at dilution.
B - Arnlyte detected [p the associated Method Blark
tA
S - Spike Recovery outside accepted recovery limits
* - Compound detected above regulalory limit.
X - Not Applicable.
,,QA K
Qualiliers:
Analyst Approved 1 l/09/2001 4:01 PM
I
129-00-0
120-82-1
95-95-4
88-06-2
Client Sample ID : P3C10GL3
Lab Sample ID : 0l{007-074
Date Collected : lll01/2001
Date Received : ll/02/2001
DatePrepared : 111061200l
Date Analyzed : lll0'712001
Percent Moisture : 10.82
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSll0T\1801011.D
Method Blank : MB-10506
Prep Factor : 33.255'736614566
Effective Dilution : l. 12
Method: SW8270C 827OC Hazardous Substance List Units: pg/KS
Analyte CAS #Concentration RL PQL
Acenaphthene
Acenaphthylene
Anthracene
Benzo(b&k)fl uoranthene
Benzo(a)anthracene
25
40
62
110
63
190
190
190
370
190
83-32-9
208-96-8
120-12-7
205-99-2+k
56-55-3
Benzo(a)pyrene
Benzo(g,h,i)perylene
Benzoic acid
Benzyl alcohol
Bis(2-chloroethyl)ether
50-32-8
191-24-2
65-85-0
100-51-6
111444
65
64
210
58
56
190
190
370
190
190
Bis(2-chloroeth oxy)methane
Dichlorodiisopropyl ether
Bis(2-ethylhexyl)phth alate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
28
72
79
73
74
190
190
190
190
190
111-91-1
1 08-60-1
117-81-7
101-55-3
85-68-7
4-Chloroaniline
4-Chlo ro-3-methylphen ol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
70
80
38
47
55
190
190
190
190
190
10647-8
59-50-7
91-58-7
95-57-8
7005-72-3
Chrysene
Dibenz(a, h)anthracene
Dibenzofuran
Di-n-butylphthalate
1,2-Dichlorobenzene
63
71
42
68
49
190
190
190
190
190
218-01-9
53-70-3
132-64-9
84-74-2
95-50-1
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3, 3' -Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
71
50
220
49
57
190
190
370
190
190
541-73-1
106-46-7
91-94-1
120-83-2
84-66-2
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
110
64
140
200
52
190
190
190
370
190
1 05-67-9
1 31-1 1-3
534-52-1
51-28-5
121-14-2
2,6-Dinitrotoluene
Di-n-octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
606-20-2
117-84-O
206-44-0
86-73-7
118-74-1
90
65
65
38
34
190
190
190
190
190
Hexachlorobutadiene 87-68-3 63 190
U - Not Detecled allhe Reporting Limit (RL)
J - Analyte detected below Practical Quantitation Limit (PQL)
E - Extrapolaled value. See rerun at dilution.
B - Analvte detected in the associaled Method Blank
/"
S - Spike Recovery outside accepted recovery limits
* - Compound detected above regulatory limit
X - Not Applicable.
fifr-/t
Quallffers:
Analyst Approved l1/08/2001 9:334M
I
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Sample ID : P3Cl0GL3
Lab Sample ID : 0l-6007-07A
DateCollected : l1101/2001
Date Received : ll/02/2001
Date Prepared : 11106/2001
Date Analyzed : lll0'7/2001
Percent Moisture : 10.82
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSll0T\1801011.D
Method Blank : MB-10506
PrepFactor :33.255736614566
Effective Dilution : l.12
Method: SW8270C 827OC Hazardous Substance List Unils: lrg/l S
Analyte CAS #Goncentration RL IQL
Hexachlorocyclopentadien e
Hexachloroethane
lndeno( 1,2,3-cd)pyrene
lsophorone
7747-4
67-72-',1
1 93-39-5
78-59-1
50
52
66
37
90
90
90
90
.t
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline
91-57-6
95-48-7
10644-5
91-20-3
88-744
36
120
85
42
69
i90
190
190
190
190
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
82
66
41
5'r
150
'190
190
190
190
190
N-Nitrosodiphenylamine
N-Nitrosodipro pylamin e
Pentachlorophenol
Phenanthrene
Phenol
86-30-6
621-64-7
87-86-5
85-01-8
1 08-9s-2
190
190
190
190
190
Pyrene
1,2,4-Trichlorobenzene
2,4, 5-Trichlorophenol
2,4,6-Trichlorophenol
1 29-00-0
120-82-1
95-95-4
88-06-2
46
59
90
75
190
190
190
190
Surrogate Recovery
2-Fluorophenol
Phenol-d6
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-d14
65%
72%
7 1o/o
73o/o
82o/o
92o/o
QC Limits
9 - 119
11 - 115
18 - 120
26 - 115
7-129
7-125
U - Not Detected at thc Reporting Limit (RL)
J - Analyte detected below Practical Quartitalion Limit (PQL)
E - Extrapolated value. See renrn at dilution.
S - Spike Recovery outside accepted recovery limils
* - Compound detected above regulatory limi1.
X - Not Applicable.
QrrellIl6l3;
B - Analyte detected in the associated Method Blank
Approved 1 l/08/2001 9:33 AM
I
i
l
64
35
120
42
46
I
i
lnalyst
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Sample ID : P3C8GL5
Lab Sample ID : 0l-6007-08A
Date Collected : ll/0112001
Date Received : ll/0212001
Date Prepared : 11106/2001
Date Analyzed : ll/09/2001
Percent Moisture : 8.5
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMS1108\1401014.D
Method Blank : MB-10506
PrepFactor : 33.255736674566
Effective Dilution : 1.09
Method: SW8270C 8270C Hazardous Substance List Units: pg/Kg
Analyte CAS #Concentration RL PQL
Ir
Acenaphthene
Acenaphthylene
Anthracene
Benzo(b&k)fl uoranthene
Benzo(a)anthracene
24
39
61
110
62
180
180
180
360
180
83-32-9
208-96-8
120-12-7
205-99-2+k
56-55-3
Benzo(a)pyrene
Benzo(g,h,i)perylene
Benzoic acid
Benzyl alcohol
Bis(2-chloroethyl)ether
50-32-8
191-24-2
65-85-0
'l 00-51 -6
111-44-4
64
63
200
57
55
Bis(2-chloroethoxy)methane
Dichlorodiisopropyl ether
Bis(2-ethylh exyl) phth alate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
27
70
77
71
72
180
180
180
180
180
111-91-1
1 08-60-1
117-81-7
101-55-3
85-68-7
4-Chloroaniline
4-Chloro-3-m ethylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
106-47-8
59-50-7
91-58-7
95-57-8
7005-72-3
68
78
37
46
54
180
180
180
180
180
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Chrysene
Dibenz(a, h)anthracene
Dibenzofuran
Di-n-butylphthalate
1,2-Dichlorobenzene
2'r8-01-9
53-70-3
132-64-9
84-74-2
95-50-1
61
69
41
66
48
180
180
180
180
180
I
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3, 3' -Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
69
49
220
48
56
180
180
360
180
180
541-73-1
106-46-7
91-94-1
120-83-2
84-66-2
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-m ethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
100
62
140
190
51
180
180
180
360
180
1 05-67-9
1 31-1 1-3
534-52-1
51-28-5
121-14-2
I
2,6-Dinitrotoluene
Di-n-octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
606-20-2
117-84-O
206-44-0
86-73-7
118-74-1
88
63
63
37
33
'180
180
'180
180
180
Hexachlorobutadiene 87-68-3 62 180
U - Not Detected at the Reporting Limit (RL)
J - Anallte del€cted below Practical Quantitalion Limit (PQL)
E - Extrapolated value. See renrn at dilution.
B - Analvte daected in f,re associated Melhod Blank' i/Lv
S - Spike Recovery outside accepted recovery limits
t - Compound detected above regulatory limit.
X - Not Applicable.
r€4lL
Qualifters:
Analyst Approved 1 l/09/2001 2:54 Ptl
180
180
360
180
180
,l
I
I
Client Sample ID : P3C8GL5
Lab Sample ID : 0l-6007-08A
Date Collected : lll0l/20D1
Date Received : ll/02/2001
DatePrepared : 111061200l
Date Analyzed : lll09/2001
Percent Moisture : 8.5
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSll08\1401014.D
Method Blank : MB-10506
PrepFactor :33.255736614566
Effective Dilution : 1.09
Method: SW8270C 8270C Hazardous Substance List Units: lrS/KS
CAS #Concentration RL PQL
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-cd)pyrene
lsophorone
49
51
64
36
180
180
180
180
77-47-4
67-72-1
1 93-39-5
78-59-1
N
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline
35
120
83
41
67
180
180
180
180
180
91-57-6
95-48-7
106-44-5
91-20-3
88-744
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
80
64
40
50
140
180
180
180
180
180
N-Nitrosodiph enylamine
N-Nitrosodipropylamine
Pentachlorophenol
Phenanthrene
Phenol
63
34
110
41
44
180
180
180
180
180
86-30-6
621-64-7
87-86-5
85-0'l-8
1 08-95-2
Pyrene
1,2,4-T richloro benzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
45
58
88
73
180
180
180
180
129-00-0
120-82-1
95-95-4
88-06-2
Surrogate Recovery
2-Fluorophenol
Phenol-d6
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-d14
59%
79o/o
62%
67%
69%
87o/o
QC Limits
9 - 119
11 - 115
18 - 120
26 - 115
7-129
7-125
\
i
il
U - Not Detected at the Reporting Limit (RL)
J - Analyte detected below Practical Quarflitation Limit (PQL)
E - Extrapolated value. See rerun at dilution.
B - Analvte detectcd in the associa&d Method Blankt
S - Spike Recovery outside accepted rocovery limits
* - Compound detected above regulatory limit.
X - Not Applioable.
Qualiliers:
Analyst Approved l1/09/2001 2:54 PM
Analyte
,(*t<
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
!Client Sample ID : P3C7GL7
Lab Sample ID : 0l-6007-09A
Date Collected : lll0ll200l
Date Received : ll/0212001
Date Prepared : 111061200l
Date Analyzed : 11/0912001
Percent Moisture : I l.18
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSI108\1501015.D
Method Blank : MB-10506
PrepFactor :33.255736614566
Effective Dilution : l.12
Method: SW8270C 8270C Hazardous Substance List Units: pg/Kg
CAS #PQLConcentration
Acenaphthene
Acenaphthylene
Anthracene
Benzo(b&k)fl uoranthene
Benzo(a)anthracene
25
40
62
110
63
190
190
190
370
190
83-32-9
208-96-8
120-12-7
205-99-2+k
56-55-3
Benzo(a)pyrene
Benzo(g,h,i)perylene
Benzoic acid
Benzyl alcohol
Bis(2-chloroethyl)eth er
50-32-8
191-24-2
65-85-0
100-51-6
111-44-4
66
65
10
59
56
2
190
'190
370
190
190
Bis(2-chlo roethoxy)methane
Dichlorodiisopropyl ether
Bis(2-ethylhexyl)phthalate
4-Bromophenyl phenyl ether
Bu$ benzyl phthalate
111-91-1
1 08-60-1
117-81-7
101-55-3
85-68-7
28
72
80
73
74
190
190
190
190
190
4-Chloroaniline
4-C hloro-3-methylph enol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
106-47-8
59-50-7
91-58-7
95-57-8
7005-72-3
70
81
38
47
55
190
190
190
190
190
Chrysene
Dibenz(a, h)anthracene
Dibenzofuran
Di-n-butylphthalate
1,2-Dichlorobenzene
63
72
42
68
49
190
190
190
190
190
218-O1-9
53-70-3
132-64-9
84-74-2
9s-50-1
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
I
{
1 ,3-Dichlorobenzene
1 ,4-Dichlorobenzene
3, 3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
190
190
370
190
190
541-73-1
106-46-7
91-94-1
120-83-2
84-66-2
2,4-Dimethylphenol
Dimethylphthalate
4, 6-Dinitro-2-methylphen ol
2,4-Dinitrophenol
2,4-Dinitrotoluene
110
64
140
200
52
190
190
190
370
190
1 05-67-9
131-11-3
534-52-1
51-28-5
121-14-2
2,6-Dinitrotoluene
Di-n-octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
606-20-2
117-84-0
20644-0
86-73-7
118-74-1
90
65
65
38
34
190
190
190
190
190
Hexachlorobutadiene 87-68-3 63 190
U - Not Detected at the Reporting Limit (RL)
J - Analyte detected below Practical Quantitation Limil (PQL)
E - Extrapolaled value. See rerun at dilution.
B - Analvte detected in the associaled Method Blank't lI^I
S - Spike Recovery outside accepted recovery limits
r - Compound detected above regulatory limit.
X - Not Applicable.
Qualifiers:
Analyst Approved 1 1/09/2001 2:54 PM
71
50
220
49
57
Client Sample ID : P3C7GL7
Lab Sample ID : 0l-6007-09A
DateCollected : lll01/2001
Date Received : lll02/2001
Date Prepared : ll/06/2001
Date Analyzed : lll09l200l
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Project ID : Unocal Parachute
Lab Work Order : 01-6007
Sample Matrix : Soil
Lab F'ile ID : GCMSI108\1501015.D
Method Blank : MB-10506PrepFactor :33.255736614566
Effective Dilution : L12Percent Moisture :11.18
Method: SW8270C 827OC Hazardous Substance List Units: Ig/Kg
Analyte cAs #Concentration RL POL
H exachlorocyclopentadiene
Hexachloroethane
lndeno( 1,2,3-cd)pyrene
lsophorone
77-474
67-72-1
1 93-39-5
78-59-1
50
52
66
37
190
190
190
'190
U
U
U
U
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline
91-57-6
95-48-7
106-44-5
91-20-3
88-74-4
50 36
20
85
42
69
190
190
190
190
190
1
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
99-09-2
100-01-6
98-95-3
88-75-5
10a-02-7
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
82
66
41
51
150
190
190
190
190
190
N-Nitrosodiph enylamine
N-Nitrosodipropylamine
Pentachlorophenol
Phenanthrene
Phenol
86-30-6
621-64-7
87-86-5
85-01-8
1 08-95-2
65
35
120
42
46
190
190
190
190
190
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
129-00-0
120-82-1
95-95-4
88-06-2
46
60
90
75
190
190
190
190
Surrogate Recovery
2-Fluorophenol
Phenol-d6
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-d14
62%
78%
66%
69%
64%
86%
QC Limits
9 - 119
11 - 115
18 - 120
26 - 115
7-129
7-125
U - Not Delected at the Reporting Limit (RL)
J - Analyte detected below Practical Quanlitalion Limit (PQL)
E - Extrapolaled value. See rerun at dilution.
B - Anallt detected in the associated Method Blank
tl'
S - Spike Recovery oulside accepted recovery limits
t - Compound detected above regulalory limit
X - No1 Applicable.
trAK
Qualiliers
Analyst Approved 1 1/09/2001 2:51 PM
D
I
i
I
Client Sample ID :
Lab Sample ID :
Date Collected i
Date Received :
Date Prepared :
Date Analyzed :
Percent Moisture :
P3CIGL6
01-6007-t0A
LU0y200t
tU02l200t
tU06t200t
1U0912001
I1.59
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Proiect ID :
Lab Work Order :
Sample Matrix
Lab File II)
Method Blank
Prep Factor :
Effective Dilution :
Unocal Parachute
0l-6007
Soil
GCMSI108\1601016.D
MB-10506
33.0906684315023
l. l3
Method: SW8270C 8270C Hazatdous Substance List Units: Fg/Kg
Analyte CAS #Concentration RL PQL
Acenaphthene
Acenaphthylene
Anthracene
Benzo(b&k)fl uoranthene
Benzo(a)anthracene
25
40
62
110
63
190
190
190
370
190
83-32-9
208-96-8
120-12-7
205-99-2+k
56-55-3
Benzo(a)pyrene
Benzo(g,h,i)perylene
Benzoic acid
Benzyl alcohol
Bis(2-chloroethyl)ether
50-32-8
191-24-2
65-85-0
100-51-6
111-44-4
66
65
210
58
56
190
190
370
190
190
Bis(2-chloroethoxy)methane
Dichlorodiisopropyl ether
Bis(2-ethylhexyl )phth alate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
28
72
79
73
74
190
190
190
190
'190
111-91-1
1 08-60-1
117-81-7
101-55-3
85-68-7
4-Chloroaniline
4-Chloro-3-methylphen ol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
70
81
38
47
55
190
190
190
190
190
106-47-8
59-50-7
91-58-7
95-57-8
7005-72-3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Chrysene
Dibenz(a, h)anthracene
Dibenzofuran
Di-n-butylphthalate
1,2-Dichlorobenzene
218-01-9
53-70-3
132-64-9
84-74-2
95-50-1
63
72
42
68
49
190
190
190
190
190
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
71
50
220
49
57
190
190
370
190
190
541-73-1
106-46-7
91-94-1
120-83-2
84-66-2
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-methylphen ol
2,4-Dinitrophenol
2,4-Dinitrotoluene
110
64
140
200
52
190
190
190
370
190
105S7-9
131-1 1-3
534-52-1
51-28-5
121-14-2
2,6-Dinitrotoluene
Di-n-octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
606-20-2
117-84-0
206-44-0
86-73-7
118-74-1
90
65
65
38
34
190
190
190
190
190
Hexachlorobutadiene 87-68-3 63 '190
U - Not Detected allhe Reporting Limit (RI)
J - Analyte detected below Practical Quantitalion Limit (PQL)
E - Exhapolated value. See rerun at dilution.
B - Analyte delected the associated Method Blar*
S - Spike Recovery outside accepted recovery limils
* - Compound detesled above regulatory limit.
X - Not Applicable.
Enx
Qualiliers:
Analyst Approved 11/09/2001 2:54 PM
Client Sample ID : P3C1GL6
Lab Sample ID : 0l-6007-l0A
Date Collected : ll/0112001
Date Received : ll/02/2001
Date Prepared : ll/06/2001
Date Analyzed : ll/0912001
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 425-6021
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSll08\1601016.D
Method Blank : MB-10506
Prep Factor : 33.0906684375023
Effective Dilution : l. 13Percent Moisture : 11.59
Method: SW8270C 8270C Hazardous Substance List Units: pg/KS
Analyte CAS #Concentration RL PQL
Hexachlorocyclopentadiene
Hexachloroethane
lndeno( 1,2,3-cd)pyrene
lsophorone
77-47-4
67-72-1
1 93-39-5
78-59-1
50
52
66
37
190
190
190
190
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline
36
120
85
42
69
190
190
190
190
190
91-57-6
9548-7
106-44-5
91-20-3
88-744
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
82
66
41
51
150
190
190
190
190
190
N-Nitrosodiphenylamine
N-Nitrosodipropylamine
Pentachlorophenol
Phenanthrene
Phenol
86-30-6
621-64-7
87-86-5
85-01-8
1 08-95-2
65
35
120
42
46
190
190
190
190
190
Pyrene
1,2,4-Trichlorobenzene
2,4, 5-Trichlorophenol
2,4,6-Trichlorophenol
129-00-0
120-82-1
95-95-4
88-06-2
46
60
90
75
190
190
190
190
Surrogate Recovery
2-Fluorophenol
Phenol-d6
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-d14
684/o
81o/o
760/o
73%
64o/o
81%
QC LimitsI - 119
11 - 115
18 - 120
26 - 115
7-129
7-125
U - Not De{ected al1he Reporring Limit (RL)
J - Anal)'te daected below Practical Quantitation Limit (PQL)
E - Extrapolated valuc. See rerun at dilution.
B - Analyte detected inthe associated Method Blank
S - Spike Recovery outside accepted recovery limits
t - Compound detected above regulatory limit
X - Not Applicable.
44K
Qualiliers:
Analyst Approved 1 1/09/2001 2:54 PM
l-
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-602r
Client Sample ID : P3C2GL9
Lab Sample ID : 0l-6007-llA
DateCollected : ll/01/2001
Date Received : ll/02/2001
DatePrepared : ll/06/2001
Date Analyzed : ll/09/2001
Percent Moisture : 11.1
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSIl08Ul0l02l.D
Method Blank : MB-10506
Prep Factor : 33.2336324360253
Effective Dilution : l.l2
Method: SW8270C 8270C Hazardous Substance List Units:Fg/Ks
Analyte CAS #Concentration POLRL
Acenaphthene
Acenaphthylene
Anthracene
Benzo(b&k)fl uoranthene
Benzo(a)anthracene
25
40
62
110
63
190
190
190
370
190
83-32-9
208-96-8
120-12-7
205-99-2+k
56-55-3
Benzo(a)pyrene
Benzo(g,h,i)perylene
Benzoic acid
Benzyl alcohol
Bis(2-chlo roethyl)ether
65
65
210
58
56
190
190
370
190
190
50-32-8
191-24-2
65-85-0
100-51-6
111-444
Bis(2-chloroeth oxy)meth an e
Dichlorodiisopropyl ether
Bis(2-ethylhexyl) phth alate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
28
72
79
73
74
190
190
190
190
190
'l 1 1-91 -1
1 08-60-1
117-81-7
1 01 -55-3
85-68-7
4-Chloroaniline
4-Chlo ro-3-m ethylph enol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
70
81
38
47
55
190
190
'190
190
190
106-47-A
59-50-7
91-58-7
9s-57-8
7005-72-3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Chrysene
Dibenz(a, h)anth racene
Dibenzofuran
Di-n-butylphthalate
1,2-Dichlorobenzene
218-01-9
53-70-3
132-64-9
84-74-2
95-50-1
o5
71
42
68
49
190
190
190
190
190
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3, 3' -Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
71
50
220
49
57
190
190
370
190
190
541-73-1
10646-7
91 -94-1
120-83-2
84-66-2
2,4-Dimethylphenol
Dimethylphthalate
4, 6-Dinitro-2-m ethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
110
64
140
200
52
190
190
190
370
190
1 05-67-9
131-1 1-3
534-52-1
51-28-5
121-14-2
2,6-Dinitrotoluene
Di-n-octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
90
65
65
38
34
190
190
190
190
190
606-20-2
117-84-0
206-44-0
86-73-7
118-74-1
Hexachlorobutadiene 87-68-3 63 190
U - Not Detected althe Reporting Limit (RL)
J - Analyte detected below Practical Quantitalion Limit (PQL)
E - Extrapolated value. See rerun at dilution.
B - Analyte detected inthe associatod Method Blar&
S - Spike Recovery outside accepted recovery limits
| - Compound detected above regulatory limit
X - Not Applicable.
fid-/<
Qualifiers:
Approved I l/09/2001 2:54 PM
l"
'Analyst
Client Sample ID : P3C2GL9
Lab Sample ID : 0l-6007-llA
Date Collected : ll/01/2001
Date Received : 1110212001
DatePrepared : l1106/2001
Date Analyzed : lll09l200l
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSll08U10102l.D
Method Blank : MB-10506PrepFactor :33.2336324360253
Effective Dilution : l.12Percent Moisture : ll.l
Method: SW8270C 827OC Hazardous Substance List Units: pg/Kg
Analyte CAS #Concentration RL PQL
Hexachlorocyclopentadiene
Hexachloroethane
lndeno( 1,2,3-cd)pyrene
lsophorone
77-47-4
67-72-1
1 93-39-5
78-59-1
50
52
66
37
190
'190
190
190
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline
91-57-6
95-48-7
106-44-5
91-20-3
88-74-4
36
120
85
42
69
190
190
190
190
190
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
3-Nitroaniline
4-Nitroanlline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
82
66
41
51
150
190
190
'190
190
190
N-Nitrosodiphenylamine
N-Nitrosodipropylamin e
Pentachlorophenol
Phenanthrene
Phenol
86-30-6
621-64-7
87-86-5
85-01-8
108-95-2
65
35
20
42
46
1
190
190
190
190
190
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
1 29-00-0
120-82-1
95-95-4
88-06-2
46
60
90
75
190
190
190
1902
Surrogate
U
2-Fluorophenol
Phenol-d6
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-d14
63%
79%
70%
74o/o
67%
86%
QC Limits
9 - 119
11 - 115
18 - 120
26 - 115
7-129
7-125
U - Not Det€cted at the Reporting Limit (RL)
J - &ralyt€ detected below Practical Quantitation Limit (PQL)
E - Extrapola&d value. See rerun al dilution.
the associated Method Blark
S - Spike Recovery outside accepted recovery limits
| - Compound detecied above regulatory limit.
X - Not Applicable.
Queliflgrs;
B - Analyte
Analyst Approved 11/09/2001 2:54 PM
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Sample ID : P3C2GL9DUP
Lab Sample tD : 0l-6007-12,{
Date Collected : ll/01/2001
Date Received : ll/0212001
Date Prepared : lll06l200L
Date Analyzed : ll/09/2001
Percent Moisture : 13.51
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSI108U201022.D
Method Blank : MB-I0506
PrepFactor :33.0797221303341
Effective Dilution : l.15
Method: SW8270C 827OC Hazardous Substance List Units: pg/KS
Analyte CAS #Concentration RL PQL
Acenaphthene
Acenaphthylene
Anthracene
Benzo(b&k)fl uoranthene
Benzo(a)anthracene
26
41
64
120
65
190
190
190
380
190
83-32-9
208-96-8
120-12-7
205-99-2+k
56-55-3
Benzo(a)pyrene
Benzo(g,h,i)perylene
Benzoic acid
Benzyl alcohol
Bis(2-chloroethyl)ether
50-32-8
191-24-2
65-85-0
100-51-6
111-44-4
67
66
10
60
58
2
190
190
380
190
190
Bis(2-chloroeth oxy) m ethane
Dichlorodiisopropyl ether
Bis(2-ethylhexyl) phthalate
4-Bromophenyl phenyl ether
29
74
81
75
75
190
190
190
190
190Eutyl benzyl phthalate
4-Chloroaniline
4-Chlo ro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
106-47-8
59-50-7
91-58-7
95-57-8
7005-72-3
72
82
39
48
57
190
190
190
190
190
Chrysene
Dibenz(a, h)anthracene
Dibenzofuran
Di-n-butylphthalate
1,2-Dichlorobenzene
65
73
43
70
51
190
190
190
190
190
218-01-9
53-70-3
132-64-9
84-74-2
95-50-1
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1,3-Dichlorobenzene
1 ,4-Dichlorobenzene
3, 3' -Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
73
51
230
50
58
190
190
380
190
190
541-73-1
106-46-7
91 -94-1
120-83-2
84-66-2
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
'110
66
140
200
53
190
190
190
380
190
105-67-9
131-1 1-3
534-52-1
51-28-5
121-14-2
2,6-Dinitrotoluene
Di-n-octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
606-20-2
117-84-0
20644-0
86-73-7
118-74-1
92
67
66
39
35
190
190
'190
190
190
Hexachlorobutadiene 87-68-3 65 190
U - Not Detrcted atlhe Reporting Limit (RL)
J - Andyt€ detected below Practical Quantitation Limit (PQL)
E - Extrapolaled value. See rerun at dilution.
B - Andyte detected. in rhe associated Method Blank
A
S - Spike Recovery outside accepted recovery limits
| - Compound detected above regulatory limit.
X - Not Applicable.
/Q//-/<
Qualiliers:
Analyst Approved 1 1/09/2001 2:54 PM
111-91-'l
1 08-60-1
117-81-7
1 01-55-3
85€8-7
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 425-6021
Client Sample ID : P3C2GL9DLIP
Lab Sample ID : 0l-6007-l2A
Date Collected : lll0l/2001
Date Received : lll02l200l
Date Prepared : 111061200l
Date Analyzed : ll/09/2001
Percent Moisture : 13.51
Client Project ID : Unocal Parachute
Lab Work Order : 01-6007
Sample Matrix : Soil
Lab File ID : GCMS1108U20l022.D
Method Blank : MB-10506
Prep Factor : 33.0797221303341
Effective Dilution : l.15
Method: SW8270C 827OC Hazardous Substance List Units:pg/Kg
Analyte CAS #Concentration RL PQL
H exachlorocyclopentadiene
Hexachloroethane
lndeno( 1,2,3-cd)pyrene
lsophorone
77-47-4
67-72-1
1 93-39-5
78-59-1
51
53
68
38
190
't90
190
190
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline
37
'130
87
43
71
190
190
190
190
190
91-57-6
95-48-7
106-44-5
91-20-3
88-744
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
ll
U
U
U
U
U
U
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
84
67
42
52
150
190
190
190
190
190
N-Nitrosodiphenylamine
N-Nitrosodipropylamine
Pentachlorophenol
Phenanthrene
Phenol
86-30-6
621-64-7
87-86-5
85-0'l-8
1 o8-95-2
bb
36
120
43
47
190
190
190
190
190
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
47
61
92
77
190
190
190
190
1 29-00-0
120-82-1
95-95-4
88-06-2
Surrogate Recovery
2-Fluorophenol
Phenol-d6
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-d14
620/o
760/o
70o/o
74%
72%
88%
QC LimitsI - 119
11 - 115
18 - 120
26 - 115
7-129
7-125
U - Not Detected al the Reporting Limit (RL)
J - Analyte detected below Practical Quantitation Limit (PQL)
E - Exlrapolated value. See rerun at dilution.
detected in the associated Melhod Blank
S - Spike Recovery outside accepted recovery limits
t - Compound detected above regulatory limit.
X - Not Applicable.
/?*/<
Qurlillers:
B - Analyte
Analyst Approved 1)/09/2001 2:54 PM
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Sample ID : P3C3GL2
Lab Sample ID : 0l-6007-13A
Date Collected : l1/01/2001
Date Received : ll/02/2001
Date Prepared : 1710612001
Date Analyzed : ll/09/2001
Percent Moisture : 6.94
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSI108U301023.D
Method Blank : MB-10506PrepFactor :33.2005312084993
Effective Dilution : 1.07
Method: SW8270C 827OC Hazardous Substance List Units: pg/Kg
Analyte CAS #PQLConcentration
Acenaphthene
Acenaphthylene
Anthracene
Benzo(b&k)fl uoranthene
Benzo(a)anthracene
24
38
59
110
60
'180
180
180
360
180
83-32-9
208-96-8
120-12-7
205-99-2+k
56-55-3
Benzo(a)pyrene
Benzo(g,h,i)perylene
Benzoic acid
Benzyl alcohol
Bis(2-chlo roethyl)ether
50-32-8
191-24-2
65-85-0
100-51-6
111-44-4
62
62
200
56
54
180
180
360
180
180
Bis(2-chloroethoxy)meth ane
Dichlorodiisopropyl ether
Bis(2-ethylhexyl)phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
27
69
76
70
70
180
180
180
180
180
111-91-1
1 08-60-1
117 -81-7
1 01 -55-3
85-68-7
4-Chloroaniline
4-Chloro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
106-47-8
59-50-7
91-58-7
95-57-8
7005-72-3
67
77
36
45
53
180
180
180
180
180
Chrysene
Dibenz(a, h)anthracene
Dibenzofuran
Di-n-butylphthalate
1 ,2-Dichlorobenzene
60
68
40
65
47
180
180
180
180
180
218-01-9
53-70-3
132-64-9
84-74-2
95-50-1
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3, 3' -Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
541-73-1
106-46-7
91-94-1
120-83-2
84-66-2
68
48
210
47
55
180
180
360
180
180
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-methylphen ol
2,4-Dinitrophenol
2,4-Dinitrotoluene
105-67-9
131-11-3
534-52-1
51-28-5
121-14-2
100
61
130
'190
50
180
180
180
360
180
2,6-Dinitrotoluene
Di-n-octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
606-20-2
117-84-0
20644-0
86-73-7
118-74-1
86
62
62
50
32
180
180
180
180
180
Hexachlorobutadiene 87-68-3 60 180
U - Not Detect€d atlhe Reporting Limit (RL)
J - Analyte detected below Practical Quantitalion Limit (PQL)
E - Extrapolated value. See rerun at dilution.
B - Analyt€ detecte.d inlhe associated Method Blank
A
S - Spike Reoovery outside accepted recovery limits
| - Compound detected above regulalory limit.
X - Not Applioable.
Quelifiers:
Analyst Approved 1 1/09/2001 2:54 PM
RL
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Sample ID : P3C3GL2
Lab Sample ID : 0l-6007-l3,{
Date Collected : ll/01/20O1
Date Received : ll/02/2001
Date Prepared : ll/0612001
Date Analyzed : lll09/2001
Percent Moisture : 6.94
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSll08U301023.D
Method Blank : MB-10506
PrepFactor :33.2005312084993
Effective Dilution : 1.07
Method: SW8270C 827OC Hazardous Substance List Units:ps/Kg
Analyte CAS #PQLRLConcentration
Hexachlorocyclo pentadiene
Hexachloroethane
lndeno( 1,2,3-cd)pyrene
lsophorone
77-474
67-72-1
1 93-39-5
78-59-1
48
50
63
35
180
180
180
180
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline
91-57-6
95-48-7
106-44-5
91-20-3
88-74-4
34
120
81
40
66
180
180
'180
180
180
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
78
63
39
49
140
180
180
180
180
180
N-Nitrosodiphenylamine
N-Nitrosodipro pylamine
Pentachlorophenol
Phenanthrene
Phenol
86-30-6
621-64-7
87-86-5
85-01-8
1 08-95-2
62
34
110
40
44
'180
180
180
180
180
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
129-00-0
120-82-1
95-954
88-06-2
44
57
86
72
180
180
180
180
Surrogate Recovery
2-Fluorophenol
Phenol-d6
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-d14
65o/o
80%
73%
76%
68%
860/o
QC LimitsI - 119
11 - 115
18 - 120
26 - 115
7-129
7-125
U - Not Detected at the Reporting Limit (RL)
J - Andyl€ deteded below Practical Quantitalion Limit (PQL)
E - Extrapolafed value. See rerun at dilution.
B - Analte detscted inthe associated Mahod Blank'l k-
S - Spike Recovery outside accepted recovery limits
+ - Compound detected above regulatory limit.
X - Not Applicable.
Qurliffsrx;
Analyst Approved 1 1/09/2001 2:54 PM
pl
Client Sample ID :
Lab Sample ID :
Date Collected :
Date Received :
Date Prepared i
Date Analyzed :
Percent Moisture :
P3C9GL7
0l{007-l4A
tt/0y2001
ty02t200t
lt/0612001
tU09/2001
t2.35
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSll08U60l026.D
Method Blank : MB-10506
Prep Factor : 33.3000333000333
Effective Dilution : l.14
Method: SW8270C 8270C Hazardous Substance List Unats: IS/KS
Analyte CAS #Concentration RL PQL
Acenaphthene
Acenaphthylene
Anthracene
Benzo(b&k)fl uoranthene
Benzo(a)anthracene
26
40
63
120
64
190
190
190
380
190
83-32-9
208-96-8
120-12-7
205-99-2+k
56-5s-3
Benzo(a)pyrene
Benzo(g,h,i)perylene
Benzoic acid
Benzyl alcohol
Bis(2-chloroethyl)ether
50-32-8
191-24-2
65-85-0
100-51-6
11144-4
66
66
210
59
57
190
190
380
190
190
Bis(2-chlo roethoxy)methane
Dichlorodiisopropyl ether
Bis(2-ethylhexyl)phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
111-91-1
1 08-60-1
117-81-7
1 01 -55-3
85-68-7
29
73
81
75
75
190
'190
190
190
'190
4-Chloroaniline
4-C hloro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
10647-8
59-50-7
91-58-7
95-57-8
7005-72-3
71
82
39
48
56
190
190
190
190
190
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Chrysene
Dibenz(a, h)anth racene
Dibenzofuran
Di-n-bu$phthalate
1,2-Dichlorobenzene
218-01-9
53-70-3
132-64-9
84-74-2
95-50-1
64
73
43
70
50
190
190
'190
190
190
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3' -Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
72
51
230
50
58
190
190
380
190
190
541-73-1
106-46-7
91-94-1
120-83-2
84-66-2
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-methylph enol
2,4-Dinitrophenol
2,4-Dinitrotoluene
110
65
140
200
53
'190
190
190
380
190
1 05-67-9
131-11-3
534-52-1
51-28-5
121-14-2
2,6-Dinitrotoluene
Di-n-octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
92
66
bb
39
34
190
190
190
190
190
606-20-2
117-84-0
206-44-0
86-73-7
118-74-1
Hexachlorobutadiene 87-68-3 64 190
U - Not Detected at the Reporting Limit (RL)
J - Analyte detEcted below Practical Quantitation Limit (PQL)
E - Extapolated value. See rerun at dilution.
B - Andyte detected inthe associated Method Blank
/^
S - Spike Recovery outside accepled recovery limits
* - Compound detected above regulatory limit.
X - Not Applicable.
Qualiliers:
h"ty.t Approved I 1/09/2001 2:54 PM
fttt<
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO E0033
(303) 42s-6021
Client Sample ID : P3C9GL7
Lab Sample ID : 0l-6007-14A
Date Collected : lll0l/2001
Date Received : lll02/2001
Date Prepared : 71106/2001
Date Analyzed : ll/09/2001
Percent : 12.35
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSll08U60l026.D
Method Blank : MB-10506
Prep Factor : 33.3000333000333
Effective Dilution : l.14
Method: SW8270C 827OC Hazardous Substance List Units:pg/Kg
Analyte CAS #Concentration RL POL
Hexachlo rocyclopentadien e
Hexachloroethane
lndeno( 1,2,3-cd)pyrene
lsophorone
77-474
67-72-1
193-39-5
78-59-1
51
E2
67
38
190
190
190
190
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline
36
130
87
43
70
190
190
190
190
190
91-57-6
95-48-7
1 06-44-5
91-20-3
88-74-4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
83
67
42
52
150
190
190
190
190
190
N-Nikosodiphenylamine
N-Nitrosodipropylamine
Pentachlorophenol
Phenanthrene
Phenol
86-30-6
621-64-7
87-86-5
85-01-8
1 08-95-2
66
36
120
43
47
190
190
190
190
190
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
1 29-00-0
120-82-1
95-95-4
88-06-2
U
U
U
47
61
92
76
190
190
190
1902,4,6-Trichloro
Surrogate Recovery
2-Fluorophenol
Phenol-d6
Nitrobenzene-d5
2-Fluorobiphenyl
, 2,4,6-Tribromophenol
Terphenyl-d14
50%
60%
53%
57%
52o/o
66%
QC Limits
9 - 119
11 - 115
18 - 120
26 - 115
7-129
7-125
U - Not Detected at the Reporting Limit (RL)
J - Analyt detected below hactical Quantitation Limit (PQL)
E - Extrapolated value. See rerun at dilution.
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
* - Compound detected above regulatory limit.
X - Not Applicable.
Qualifiers:
Analyst Approved l1/09/2001 2:54PM
I
Client Sample ID : P3C4GL4
Lab Sample ID : 0l-6007-l5A
Date Collected : lll0l/2001
Date Received : lll02l200l
Date Prepared : 111061200l
Date Analyzed : lll09l200l
Percent Moisture : 11.44
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 425-602r
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSll08U70l027.D
Method Blank : MB-10506
PrepFactor :33.1345261762757
Effective Dilution : 1. 12
Method: SW8270C 8270C Hazardous Substance List Units: Ug/Kg
Analyte CAS #Concentration
Acenaphthene
Acenaphthylene
Anthracene
Benzo(b&k)fl uoranthene
Benzo(a)anthracene
83-32-9
208-96-8
120-12-7
205-99-2+k
56-55-3
25
40
62
110
63
'190
190
190
370
190
Benzo(a)pyrene
Benzo(g,h,i)perylene
Benzoic acid
Benzyl alcohol
Bis(2-chloroethyl)ether
50-32-8
191-24-2
65-85-0
100-51-6
111-44-4
65
65
210
58
56
190
190
370
190
190
Bis(2-chloroethoxy)m ethane
Dichlorodiisopropyl ether
Bis(2-ethylheryl)phth alate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
190
190
190
190
190
111-91-1
1 08-60-1
117 -81-7
101-55-3
85-68-7
4-Chloroaniline
4-Chloro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
70
81
38
47
55
190
190
190
190
190
106-47-8
59-50-7
91-58-7
95-57-8
7005-72-3
Chrysene
Dibenz(a, h)anthracene
Dibenzofuran
Di-n-butylphthalate
'l ,2-Dichlorobenzene
72
42
68
49
190
190
190
190
190
218-01-9
53-70-3
132-64-9
84-74-2
95-50-1
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
63
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3' -Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
71
50
220
49
57
190
190
370
190
190
541-73-1
106-46-7
91-94-'l
120-83-2
84-66-2
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
110
64
140
200
52
190
190
190
370
190
1 05-67-9
131-11-3
534-52-1
51-28-5
121-14-2
2,6-Dinitrotoluene
Di-n-octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
606-20-2
117-84-0
206-44-0
86-73-7
118-74-1
90
65
65
38
34
190
190
190
190
190
Hexachlorobutadiene 87-68-3 63 190
U - Not Detected al the Reporting Limit (RL)
J - Analyte detected below Practica.l Quantilation Umit (PQL)
E - Extrapolated value. See rerun at dilution.
B - Analyt€ detected in the associated Melhod Blank
lL
S - Spike Recovery oulside accepted recovery limits
r - Compound detected above regulatory limil.
X - Not Applicable.
Qualiliers:
Analyst Approved l1/09/2001 2:54 PM
RL POL
28
72
79
73
74
rt
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Sample ID : P3C4GL4
Lab Sample ID : 0l-6007-15A
Date Collected : lll0L/2001
Date Received : lll02l200l
Date Prepared : 11106/2001
Date Analyzed : lll09l200l
Percent Moisture : 11.44
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSI108U701027.D
Method Blank : MB-10506PrepFactor :33.1345261762757
Effective Dilution : 1.12
Method: SW8270C 8270C Hazardous Substance List Units: llS/KS
Analyte CAS #Concentration RL PQL
Hexachlorocyclopentadiene
Hexachloroethane
lndeno( 1,2, 3-cd)pyrene
lsophorone
77-47-4
67-72-1
1 93-39-5
78-59-1
50
52
66
37
190
190
190
190
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline
91-57-6
95-48-7
106-44-5
91-20-3
88-744
1
36
20
85
42
69
190
'190
190
190
190
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
82
66
41
51
150
190
190
190
190
190
N-Nitrosodiphenylam ine
N-Nitrosodipropylamine
Pentachlorophenol
Phenanthrene
Phenol
86-30-6
621-64-7
87-86-5
85-01-8
1 08-95-2
65
35
120
42
46
190
190
190
190
190
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
129-00-0
120-82-1
95-95-4
88-06-2
46
60
90
75
190
190
190
190
Surrogate Recovery
2-Fluorophenol
Phenol-d6
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-d14
65%
79%
72%
74%
71%
87%
QC LimitsI - 119
11 - 115
18 - 120
26 - 115
7-129
7-125
U - No1 Detected at the Reporting Limit (RL)
J - Analyte dstected below Practical Quartitation Limit (PQL)
E - Extrapolated value. See rerun at dilution.
B - Andyte detected inthe associated Method Blank
S - Spike Recovery outside accepted recovery limits
'- Compound detected above regulatory limit.
X - Not Applicable.
L
Qualiffers:
Analyst Approved 11/09/2001 2:54PM
I
I
lt^k
Client Sample ID : P3C5HS,|
Lab Sample ID : 0l-6007-164
Date Collected : ll/01/2001
Date Received : lll02l200l
DatePrepared : ll/0612001
Date Analyzed : ll/09/2001
Percent Moisture : 11.09
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Project ID : Unocal Parachute
Lab Work Order : 01-6007
Sample Matrix : Soil
Lab File ID : GCMSI108\2801028.D
Method Blank : MB-10506
PrepFactor :33.21155'76220525
Effective Dilution : 1.12
Method: SW8270C 8270C Hazardous Substance List Units: pS/KS
Analyte CAS #Concentration RL PQL
Acenaphthene
Acenaphthylene
Anthracene
Benzo(b&k)fl uoranthen e
Benzo(a)anthracene
25
40
62
110
63
190
190
190
370
190
83-32-9
208-96-8
120-12-7
205-99-2+k
56-55-3
Benzo(a)pyrene
Benzo(g,h,i)perylene
Benzoic acid
Benzyl alcohol
Bis(2-chloroethyl)ether
50-32-8
191-24-2
65-85-0
100-51-6
11144-4
65
65
r10
58
56
2
190
190
370
190
190
Bis(2-chlo roethoxy)methan e
Dichlorodiisopropyl ether
Bis(2-ethylhexyl)phthatate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
28
72
79
73
74
190
190
190
190
190
111-91-1
1 08-60-1
117-81-7
101-55-3
85€8-7
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
4-Chloroaniline
4-Chloro-3-methylph enol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
106-47-8
59-50-7
91-58-7
95-57-8
7005-72-3
70
8'1
38
47
55
190
190
190
190
190
Chrysene
Dibenz(a, h)anthracene
Dibenzofuran
Di-n-butylphthalate
1,2-Dichlorobenzene
63
71
42
68
49
190
190
190
190
190
2't8-01-9
53-70-3
132-64-9
84-74-2
95-50-1
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3' -Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
71
50
220
49
57
190
190
370
190
190
541-73-1
10646-7
91-94-1
120-83-2
84-66-2
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-m ethylph enol
2,4-Dinitrophenol
2,4-Dinitrotoluene
1 05-67-9
131-1 1-3
534-52-1
51-28-5
121-14-2
110
64
140
200
52
190
190
190
370
190
2,6-Dinitrotoluene
Di-n-octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
606-20-2
117-84-O
20644-0
86-73-7
118-7 4-1
U
U
U
U
U
90
65
65
38
34
190
190
190
190
'190
Hexachlorobutadiene 87-68-3 63 190
U - Not Deteoted at the Reporting Limit (RL)
J - Anallte detected below Practical Quantitation Limit (PQL)
E - Extrapolaled value. See rerun at dilution.
B - Anallte detected in the associated Method Blank
b
S - Spike Recovery outside accepted recovery limits
* - Compound detected above regulatory limit.
X - Not Applicable.
Qualifiers:
Analyst Approved 11/09/2001 2:54PM
n4L
Evergreen Analytical, Inc.
4036 Younglield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Sample ID : P3C5HS4
Lab Sample ID : 01-6007-164
Date Collected : 1l/01/2001
Date Received : lll02l200l
DatePrepared : ll/06/2001
Date Analyzed : ll/09/2001
Percent Moisture : 11.09
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSI108U801028.D
Method Blank : MB-10506
PrepFactor :33.2115576220525
Effective Dilution : 1.12
Method: SW8270C 827OC Hazardous Substance List units: Pg/Kg
Analyte CAS #Concentration PQLRL
Hexachlorocyclopentadiene
Hexachloroethane
lndeno( 1,2, 3-cd)pyrene
lsophorone
77-47-4
67-72-1
1 93-39-5
78-59-1
50
52
66
37
190
190
190
190
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline
91-57-6
95-48-7
1 06-44-5
91-20-3
88-74-4
1
36
20
85
42
69
190
190
190
190
190
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
82
66
41
51
150
190
'190
190
190
190
N-Nitrosodiphenylamin e
N-Nitrosodipro pylamine
Pentachlorophenol
Phenanthrene
Phenol
86-30-6
621-64-7
87-86-5
85-01-8
108-95-2
64
35
120
42
46
190
190
190
190
190
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
129-00-0
120-82-1
95-95-4
88-06-2
46
60
90
75
190
190
190
190
Surrogate Recovery
2-Fluorophenol
Phenol-d6
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-d14
58%
71%
65%
67%
620/o
72%
QC Limits
I - 119
11 - 115
18 - 120
26 - 115
7-129
7-125
U - Not Detected atthe Reporting Limit (RL)
J - Arulyte detected below Practical Quantitalion Limit (PQL)
E - E:<trapolated value. See rerun at dilution.
B - Anatyte detected in the associated Method Blankll
S - Spike Recovery outside accepted recovery limits
r - Compound delected above regulatory limit.
X - Not Applicable.
Qualifiers:
Analyst Approved I 1/09/2001 2:54 PM
fr/&K
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 425-6021
Client Sample ID : P3C5GL6
Lab Sample ID : 0l-6007-17A
Date Collected : ll/0112001
Date Received : lll02/2001
Date Prepared : ll/06/2001
Date Analyzed : ll/09/2001
Percent Moisture : 12.47
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSll08U90l029.D
Method Blank : MB-10506
PrepFactor :33.2336324360253
Effective Dilution : l.14
Method: SW8270C 827OC Hazardous Substance List Units: pg/Kg
Analyte CAS #POLRL
Acenaphthene
Acenaphthylene
Anthracene
Benzo(b&k)fl uoranthene
Benzo(a)anthracene
83-32-9
208-96-8
120-12-7
205-99-2+k
56-55-3
26
40
63
20
64
1
190
190
190
380
190
Benzo(a)pyrene
Benzo(g,h,i)perylene
Benzoic acid
Benzyl alcohol
Bls(2-chloroethyl)eth er
50-32-8
191-24-2
65-85-0
100-51-6
111-44-4
66
oo
210
59
57
190
190
380
190
190
Bis(2-chloroethoxy)methan e
Dichlorodiisopropyl ether
Bis(2-ethylh exyl)phth alate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
29
73
8'l
74
75
190
190
190
190
190
111-91-1
1 08-60-1
117-81-7
101-55-3
85-68-7
4-Chloroaniline
4-Chloro-3-methylphen ol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
10647-8
59-50-7
91-58-7
95-57-8
7005-72-3
71
82
39
48
56
190
190
190
190
190
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Chrysene
Dibenz(a, h)anthracene
Dibenzofuran
Di-n-butylphthalate
1,2-Dichlorobenzene
218-01-9
53-70-3
132-64-9
84-74-2
95-50-1
64
73
43
69
50
190
190
190
190
190
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3' -Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
72
51
230
50
58
190
190
380
190
190
541-73-1
10646-7
91-94-1
120-83-2
84-66-2
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
110
65
140
200
53
190
190
190
380
190
1 05-67-9
13'l-11-3
534-52-1
51-28-5
121-14-2
2,6-Dinitrotoluene
Di-n-octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
606-20-2
117-84-0
20644-0
86-73-7
118-74-1
92
66
66
39
34
190
190
190
190
190
Hexachlorobutadiene 87-68-3 64 190
U - Not Ddected at the Reporting Limit (RL)
J - Analyte del€c'ted below Practical Quanlitation Limit (PQL)
E - Extrapolated value. See rerun at dilution.
B - Anallte detected in the associaled Method Blank
A
S - Spike Recovery outside acceped recovery limits
| - Compound dctected above regulatory limit.
X - Not Applicable.
RAK
Quelifiers:
Analyst 6pr""d 1 1/09/2001 2:54 PM
Concentration
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Sample ID : P3C5GL6
Lab Sample ID : 0l-6007-174
Date Collected : I l/0 l/2001
Date Received : 1l/02/2001
DatePrepared : 111061200l
Date Analyzed : lll09/2001
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Sample Matrix : Soil
Lab File ID : GCMSIl08U901029.D
Method Blank : MB-10506
PrepFactor :33.2336324360253
Effective Dilution : l.14Percent Moisture : 12.47
Method: SW8270C 827OC Hazardous Substance List Units: pg/Kg
Analyte CAS #Concentration RL PQL
Hexachlorocyclo pentadiene
Hexachloroethane
lndeno( 1,2,3-cd)pyrene
lsophorone
51
53
67
38
190
190
190
190
77-47-4
67-72-1
1 93-39-5
78-59-1
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline
36
130
87
43
70
190
190
190
190
190
91-57-6
95-48-7
106-44-5
91-20-3
88-74-4
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
83
67
42
52
'150
190
190
190
190
190
N-Nitrosodiphenylamine
N-Nitrosodipro pylamine
Pentachlorophenol
Phenanthrene
Phenol
86-30-6
621-64-7
87-86-5
85-01-8
1 08-95-2
66
36
20
43
46
1
Pyrene
1,2,4-Trichlorobenzene
2,4, 5-Trichlorophenol
2,4,6-Trichlorophenol
47
61
92
76
190
190
190
190
1 29-00-0
120-82-1
95-95-4
88-06-2
Surrogate Recovery
2-Fluorophenol
Phenol-d6
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-d14
63%
79%
73%
70%
65%
86%
QC Limits
9 - '119
11 - 115
18 - 120
26 - 115
7-129
7-125
U - Not Detected al the Reporting Limit (RL)
J - Analyte dsr€ded below Practical Quarnildion Limit (PQL)
E - Extrapolatcd value. See renrn at dilution.
B - Analyt! detected inthe associated Method Blank
S - Spike Recovery outside accepted recovery limits
r - Compound detected above regulatory limit.
X - Not Applicable.
It
Qualifiers:
ena$st Approved 1l/09/2001 2:54PM
I
190
190
190
190
190
Lab Sample ID
Date Prepared
Date Analyzed
MB-10506
tU06/2001
tt/07t2001
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-602r
Method Blank Report
Client Project ID : Unocal Parachute
Lab Work Order: 016007
Lab File ID : GCMSl107\1001003.D
Prep Factor : 33.3333333333333
Effective Dilution : I
Method: SW8270C SEMIVOLATILE ORGANICS 8270C Units: Ug/Kg
Analyte CAS #Concentration RL POL
Acenaphthene
Acenaphthylene
Anthracene
Benzo(b&k)fl uoranthene
Benzo(a)anthracene
22
35
56
100
56
170
170
170
330
170
83-32-9
208-96-8
120-12-7
205-99-2+k
56-55-3
Benzo(a)pyrene
Benzo(g,h,i)perylene
Benzoic acid
Benzyl alcohol
Bis(2-chloroethyl)eth er
50-32-8
191-24-2
65-85-0
100-s1-6
11144-4
58
58
80
52
50
170
170
330
170
170
Bis(2-chlo roethoxy)methane
Dichlorodiisopropyl ether
Bis(2-ethylhexyl)phthalate
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
111-91-1
1 08-60-1
117-81-7
1 01 -55-3
85-68-7
25
64
71
65
66
170
170
170
170
170
4-Chloroaniline
4-Chlo ro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
106-47-8
59-50-7
91-58-7
95-57-8
7005-72-3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
63
72
34
42
49
170
170
170
170
170
Chrysene
Dibenz(a, h)anthracene
Dibenzofuran
Di-n-butylphthalate
1,2-Dichlorobenzene
56
64
37
61
44
170
170
170
170
170
218-01-9
53-70-3
132-64-9
84-74-2
95-50-1
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3, 3' -Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
541-73-1
10646-7
91-94-1
120-83-2
84-66-2
63
45
200
44
51
170
170
330
170
170
2,4-Dimethylphenol
Dimethylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
95
57
120
180
46
170
170
170
330
170
105-67-9
131-1 1-3
534-52-1
51-28-5
121-14-2
2,6-Dinitrotoluene
Di-n-octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
606-20-2
117-84-0
20644-0
86-73-7
118-74-1
80
58
58
34
30
170
170
170
170
170
U - Not Detected at the Reporting Limil (RL)
J - Andyt€ detected below Practical Quanlitalion Limit (PQL)
E - Extrapolated value. See rerun al dilution.
B - Analyte dstocted in the associated Method Blark
S - Spike Recovery outside accepted recovery limils
X - Not fuplicable.
fi&-/(*IL
Qrrnlifi615;
Analyst 6pr"*d 1Y0A2001 9:27 AM
Lab Sample II)
Date Prepared
Date Analyzed
MB-10506
tt/0612001
tv0'712001
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Method Blank Repoft
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6007
Lab File ID : GCMSll0T\1001003.D
Prep Factor : 33.3333333333333
Effective Dilution : I
Method: SW8270C SEMIVOLATILE ORGAN]CS 8270C Units: Ug/Kg
Analyte CAS #Concentration RL PQL
Hexachlorobutadiene
H exachlo rocyclopentadiene
Hexachloroethane
lndeno('1,2, 3-cd)pyrene
lsophorone
87-68-3
77-47-4
67-72-1
1 93-39-5
78-59-1
56
45
47
59
33
170
170
170
170
170
2-Methylnaphthalene
2-Methylphenol
4-Methylphenol
Naphthalene
2-Nitroaniline
91-57-6
95-48-7
106-44-5
91-20-3
88-744
32
110
76
37
62
170
170
170
170
170
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
73
59
37
45
130
170
170
170
170
170
N-Nitrosodiph enylamine
N-Nitrosodipropylamine
Pentachlorophenol
Phenanthrene
Phenol
58
31
100
38
41
170
170
170
170
170
86-30-6
621-64-7
87-86-5
85-01-8
108-95-2
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
41
53
81
67
170
170
170
170
129-00-0
120-82-1
95-954
88-06-2
Surrogate Recovery
2-Fluorophenol
Phenol-d6
Nitrobenzene-d5
2-Fluorobiphenyl
2,4,6-Tribromophenol
Terphenyl-d14
65%
71%
67%
760
75%
94%
QC Limits
I - 119
11 - 115
18 - 120
26 - 115
7-129
7-125
U - Not Detectpd at the Reporting Limil (RL)
J - Anallte dst€ct€d below Pras'tical Quantilalion Limil (PQL)
E - Extrapolaled value. See rerun at dilution.
B - Analyt€ dstBcted inlhe associated Method Blark
S - Spike Recovery outside accepted recovery limits
X - Not Applicable.
Qrrnllft613;
11/0U2001 9:27AM
R*k
hliroved
Client Sample ID : P3C6HSl
Lab Sample ID : 0l-6169-0lA
Date Collected : lll0l/2001
Date Received : llll2l200l
DatePrepared : ll/1312001
Date Analyzed : llll3l200l
Percent Moisture : 39.19
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 425-602r
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6169
Sample Matrix : Soil
Lab File ID : VOA3I I l3\13915.D
Method Blank : RBlll30l
Prep F'actor : I
Effective Dilution : 8.22
Method: SW8260B Hazardous Substance List - Volatile Organics Units: US/Kg
Analyte CAS #Concentration PQLRL
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
2000 99
8.2
8.2
8.2
8.2
490
82
82
82
U
U
U
U
41
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
78-93-3
75-1 5-0
56-23-s
1 08-90-7
75-00-3
5001 74
8.2
8.2
8.2
25
410
82
82
82
120
2-C hloroethylvinyleth er
Chloroform
Chloromethane
Dibromochloromethane
1 ,'1-Dichloroethane
1 10-75-8
67-66-3
74-87-3
12448-1
75-34-3
160
8.2
16
8.2
8.2
820
82
82
41
82
1,2-Dichloroethane
1 , 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
107-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
8.2
8.2
8.2
8.2
16
82
82
41
82
41
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
10061-01-5
10061-02€
100-414
591-78-6
75-09-2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
8
16
16
8.2
16
8.2
82
82
82
160
82
4-Methyl-2-pentanone
Styrene
Tetrachloroethene
1,1,2,2-f et achlo roeth a n e
Toluene
1 08-1 0-1
100-42-5
127-184
79-34-5
1 08-88-3
82
8.2
16
16
8.2
4 10
82
82
82
82
71-55-6
79-00-5
79-01-6
1 08-05-4
75-O1-4
8.2
16
16
16
16
82
82
82
82
82
Total Xylene 1330-20-7 33 160
Surrogate Recovery
1,2-Dichloroethane.d4 (SS-1 )
Toluen+dB (SS-2)
4-Bromofl uorobenzene (SS-3)
103o/o
95%
99o/o
QC Limits
75 - 110
82 - 125
74 - 115
U - Not De(ected ar the Repo,rting Limil (RL)
J - Analyte detected below Practical Quantitation Limit (PQL)
E - Extrapolated value. See rerun at dilution.
detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
* - Compound detected above regulatory limit.
X - Not Applicable.
-?o
Qualifiers:
B-
Analyst Approved l1/14/2001 l:44PM
1, 1, 1 -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
Quantitation Report
Dat.a File : c: \npcHEM\1\DATA\voA31113\1391s.DAcq On : 13 Nov 2001 7:25 pmSample : 01- 61-69 -01A DF=5Misc : SAMP 8260 S
MS Integration Paramsl rteint.p
Quant Time: Nov L4 13:38 2001 euant
Vial-:
Operator:
f nst. :
Multiplr:
27
Steve Tyson
VOA3
1.00
MethodTitleLast Update
Res se vl_a
: c: \uecHEM\1\METHoDS\82501102.M (nrp: 8260: Fri Nov 02 15:03:01 2001: Initial Calibration
Results File: 82601102.RF^
Integrator)
TIC: 13915.D
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13915.D 82501102.M Wed Nov 14 13:39:08 2001 Page 2
Client Sample ID :
Lab Sample ID :
Date Collected :
Date Received :
Date Prepared :
Date Analyzed :
Percent Moisture
P3C6GL3
0l-6169-02A
tU0y200l
rt/12t2001
tUt3/2001
tUt3t200t
t3.77
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 425-6021
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6169
Sample Matrix : Soil
Lab File ID : VOA3I I l3\13895.D
Method Blank : RBlll30l
Prep Factor : I
Effective Dilution : 5.79
Method: SW8260B Hazardous Substance List - Volatile Organics Units: pg/KS
Analyte CAS #Concentration RL PQL
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67$4-1
7143-2
75-27-4
75-25-2
74-83-9
35070
5.8
5.8
5.8
5.8
80
58
29
58
58
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
78-93-3
75-15-O
s6-23-5
1 08-90-7
75-00-3
290
58
58
58
87
52
5.8
5.8
5.8
17
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
110-75-8
67-66-3
74-87-3
12448-1
75-34-3
110
5.8
12
5.8
5.8
580
58
58
29
58
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans- 1,2-Dichloroethene
1,2-Dichloropropane
107-06-2
75-354
1 56-59-2
156€0-5
78-87-5
5.8
5.8
5.8
5.8
12
29
58
58
29
58
cis-1, 3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
12
12
58
12
5.8
58
58
58
120
58
't 0061-01-5
10061-02-6
10041-4
591-78€
75-09-2 8
4-MethyL2-pentanone
Styrene
Tetrachloroethene
1,1,2,2-f efi ach lo roeth a n e
Toluene
1 08-1 0-1
100-42-5
127-184
79-34-5
1 08-88-3
58
5.8
12
12
5.8
290
58
58
58
58
1, 1, 1 -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
71-55-6
79-00-5
79-01-6
108-05-4
75-01-4
J
U
U
U
U
U
U
U
U
U
U
U
5.8
12
12
12
12
58
58
58
58
58
TotalXylene 1330-20-7 23 120
Surrogate Recovery
1,2-Dichloroethane.d4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl uorobenzene (SS-3)
105o/o
99%
960/"
QC Limits
75 - 110
82 - 125
74 - 115
U - Not Daecled at the Reporting Limit (RL)
J - Analyte detected below Practical Quantiration Limit (PQL)
E - Efrapolated value. See rerun at dilution.
S - Spike Recovery outside accepted recovery limirs
' - Compound detected above regulatory limit.
X- NotApplicable.
tu
Qualifiers:
B.detected in the associated Method Blank
Approved l1/11/2001 10:55AM
Client Sample ID : P3CI2GL5
Lab Sample ID : 0l-616943A
Date Collected : lll01/2001
Date Received : ll/12/2O01
Date Prepared : llll3/2D01
Date Analyzed z ll/l3l2o0l
Percent Moisture : 13.91
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Project ID : Unocal Parachute
Lab Work 0rder : 015169
Sample Matrix : Soil
LabFileID : VOA3lll3\13916.D
Method Blank : RBlll30l
Prep tr'actor : I
Effective Dilution : 5.8
Method: SW8260B Hazardous Substance List - Volatile Organics Units: pg/Kg
Analyte cAs #Concentration RL PQL
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67-64-1
71-43-2
75-274
75-25-2
74-83-9
70
5.8
5.8
5.8
5.8
58
29
58
58
350
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
78-93-3
75-1 5-0
s6-23-5
108-90-7
75-00-3
52
5.8
5.8
5.8
17
290
58
58
58
87
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
110-75-8
67-66-3
74-87-3
12448-1
75-34-3
110
5.8
12
5.8
5.8
580
58
58
29
58
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
107-06-2
75-35-4
1 56-59-2
156S0-5
78-87-5
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
5.8
58
5.8
5.8
12
29
58
58
29
58
cis-1,3-Dichloropropene
trans-1, 3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
10061-01-5
1006't-02-6
100-414
591-786
75-09-2 10
12
12
5.8
12
5.8
58
58
58
120
58
4-Methyl-2-pentanone
Styrene
Tetrachloroethene
1,1,2,2-T etr ach lo roeth a n e
Toluene
1 08-1 0-1
100-42-5
127-184
79-34-5
1 08-88-3
290
58
58
58
58
58
5.8
12
12
5.8
1 ,1 , 1 -Trichloroethane
1,'1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
71-55-6
79-00-5
79-016
't08-05-4
75-01-4
5.8
12
12
12
12
58
58
58
58
58
Total Xylene 1330-20-7 23 120
Surrogate Recovery
1,2-Dichloroethane.d4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl uorobenzene (SS-3)
106%
96%
95o/o
QC Limits
75 - 110
82 - 125
74 - 115
U - Not Detected atthe Reponing Limit (RL)
J - Analyte detected below Practical Quantitation Limit (PQL)
E - Exlrapolated value. See rerun at dilution.
B - Analvte^detected in the associated Method Blank
)tufL
S - Spike Recovery outside accepted recovery limits
| - Compound detected above regulatory limit.
X - Not Applicable.
-Vu
Qualifiers:
y'*rt-t Approved ll/14/2001 I:52Plvt
i
Client Sample ID : P3Cl lHS2
Lab Sample ID : 01616944,{
Date Collected : l1/01/2001
Date Received : llll2l200l
DatePrepared : ll/13/2001
Date Analyzed : llll3l200l
Percent Moisture: 16
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-602r
Client Project ID : Unocal Parachute
Lab Work Order : 01.6169
Sampte Matrix : Soil
Lab File ID : VOA3lll3\13897.D
Method Blank : RBlll30l
Prep Factor : I
Effective Dilution : 5.95
Method: SW8260B Hazardous Substance List - Volatile Organics Units: pg/KS
Analyte CAS #Concentration RL PQL
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
36071
6
6
6
6
60
30
60
60
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
78-93-3
75-1 5-0
56-23-5
1 08-90-7
75-00-3
54 300
60
60
60
89
6
o
b
18
2-C hloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
1 ,1-Dichloroethane
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
110 600
60
60
30
60
6
12
o
b
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
1 ,2-Dichloroethane
1 ,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
107-06-2
75-35-4
1 56-59-2
1 56-60-5
78-87-5
30
60
60
30
60
6
o
b
6
12
cis-1,3-Dichloropropene
trans- 1, 3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
12
12
b
12
6
60
60
60
120
60
10061-01-5
10061-02-6
100-414
591-78-6
75-09-2
4-Methyl-2-pentanone
Sgrene
Tetrachloroethene
1,1,2,2-f etachloroethane
Toluene
1 08-1 0-1
100-42-5
127-18-4
79-34-5
1 08-88-3
60
6
12
12
6
300
60
60
60
60
1, 1, 1 -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chlonde
71-556
79-00-5
79-01-6
108-054
75-01-4
6
12
12
12
12
60
60
60
60
60
Total Xylene 1330-20-7 24 120
Surrogate Recovery
1,2-Dichloroethane-d4 (SS-1 )
Toluen+.d8 (SS-2)
4-Bromofl uorobenzene (SS-3)
1O2o/o
98o/o
95%
QC Limits
75 - 110
82 - 125
74 - 115
U - Not Daeded at the Reporting Limit (RL)
J - AndytE d€tecled below hactical Quantitation Limit (PQL)
E - Extrapolated value. See rerun at dilution.
S - Spike Recovery outside accepted recovery limils
| - Compound detected above regulatory limit.
X - Not Applicable.
-D-,-
j-(._,/
Qualifiers:
B - Analyte the associated Method Blank
Approved I 1/14/2001 I 1:05 A,tl
8
Client Sample ID : P3Cl lGL8
Lab Sample ID : 0l-6169-05A
DateCollected : ll/ol/2001
Date Received : llll2/2001
Date Prepared : ll/1312001
Date Analyzed : ll/13/2001
Percent Moisture : 12.49
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6169
Sample Matrix : Soil
Lab File ID : VOA3lll3\13898.D
Method Blank : RBlll30l
Prep tr'actor : I
Effective Dilution : 5.71
Method: SW8260B Hazardous Substance List - Volatile Organics Units:Fg/KS
Analyte cAs #Concentration RL PQL
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67$4-1
71-43-2
75-27-4
75-25-2
74-83-9
69
5.7
5.7
5.7
5.7
340
57
29
57
57
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
78-93-3
75-15-0
56-23-5
1 08-90-7
75-00-3
51
5.7
5.7
5.7
17
290
57
57
57
86
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1 10-75-8
6766-3
74-87-3
12448-1
75-34-3
110
5.7
11
5.7
5.7
570
57
57
29
57
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
107-06-2
75-35-4
1 56-59-2
156€0-5
78-87-5
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
57
5.7
57
5.7
11
29
57
57
29
57
cis-1, 3-Dichloropropene
trans-1, 3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
10061-01-5
10061-02-6
100414
591-78-6
75-09-2 30
11
11
5.7
11
5.7
57
57
57
110
57
4-Methyl-2-pentanone
Styrene
Tetrachloroethene
1,1,2,2-T etr achloroeth an e
Toluene
I 08-1 0-1
10042-5
127-18-4
79-34-5
1 08-88-3
290
57
57
57
57
57
5.7
11
11
5.7
1 ,1 , 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
71-55-6
79-00-5
79-01-6
108-054
75-014
5.7
11
11
11
11
57
57
57
57
57
Total Xylene 1330-20-7 23 110
Surrogate Recovery
1,2-Dichloroethane-d4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl uorobenzene (SS-3)
104o/o
101o/o
91o/o
QC Limits
75 - 110
82 - 125
74 - 115
U - Not Detected atlhe Reporting Limit (RL)
J - Analyte detecled b€low Practical Quantitation Limit (PQL)
E - Extrapolated value. See rerun at dilution.
S - Spike Recovery outside accepted recovery limits
* - Compound deteaed above regulatory limit.
X - Not Applicable.')o
Quelillers:
B - Analyte in the associated Method Blank
Approved l1/14/2001 I1:134M
i
Client Sample ID : P3CI0HS3
Lab Sample ID : 0l-6169-06A
Date Collected : lll0ll200l
Date Received : ll/1212001
DatePrepared : ll/1312001
Date Analyzed : llll3l200l
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s{021
Client Project ID : Unocal Parachute
Lab Work Order : 0l{169
Sample Matrix : Soil
LabfileID : VOA3lll3\13917.D
Method Blank : RBlll30l
Prep Factor : I
Effective Dilution : 6.8Percent Moisture :26.5'7
Analyte CAS #Concentration RL PQL
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67-64-1
71-43-2
75-27-4
7s-25-2
74-83-9
40082
6.8
6.8
6.8
6.8
10
68
34
68
68
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
78-93-3
75-1 5-0
56-23-5
1 08-90-7
75-00-3
61
6.8
6.8
6.8
20
340
68
68
68
100
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1 1 0-75-8
6766-3
74-87-3
124-48-1
75-34-3
130
6.8
14
6.8
6.8
680
68
68
34
68
1,2-Dichloroethane
1 , 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
107-06-2
75-354
1 56-59-2
15660-5
78-87-5
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
6.8
6.8
6.8
6.8
14
34
68
68
34
68
cis-1, 3-Dichloropropene
trans-1, 3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
14
14
6.8
14
6.8
68
68
68
140
68
10061-01-5
10061-02-6
10041-4
591-78-6
75-09-2 10
4-Methyl-2-pentanone
Styrene
Tetrachloroethene
1, 1,2,2-T elr ach lo roeth a n e
Toluene
1 08-1 0-1
100-42-5
127-18-4
79-34-5
108-88-3
340
68
68
68
68
68
6.8
14
14
6.8
1, 1, 1 -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
71-55-6
79-00-5
79-01-6
1 08-05-4
75-01-4
6.8
14
14
14
14
68
68
68
68
68
Total Xylene 1330-20-7 27 140
Surrogate Recovery
1,2-Dichloroethane-d4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl uorobenzene (SS-3)
1O4o/o
100o/o
96%
QG Limits
75 - 110
82 - 125
74 - 115
U - Nol Detected atlhe Reporting Limit (RL)
J - Analyte delected below Practical Quantitation Limit (PQL)
E - Extrapolated value. See rerun at dilution.
B - Analvte detecled in the associated Mahod Blankk!^
S - Spike Recovery outside accepted recovery limits
t - Compound detected above regulatory limit.
X - Not Applicable.
Qualiliers:
W Approved 1)/14/2001 l:58PM
Method: SW8260B Hazardous Substance List - Volatile Organics Units: ps/Kg
Client Sample ID : P3C10GL3
Lab Sample ID : 0l-6169-07A
Date Collected : llloll200l
Date Received : llll2l2O0l
Date Prepared : ll/13/2001
Date Analyzed z llll3l2O0l
Percent Moisturc z 12.44
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 425-6021
Client Project ID : Unocal Parachute
Lab Work Order : 0l.6169
Sample Matrix : Soil
Lab File ID : VOA3I I l3\13902.D
Method Blank : RBlll30l
Prep Factor : I
Effective Dilution : 5.71
Method: SW826OB Hazardous Substance List - Volatile Organics Units: pS/Kg
Analyte CAS #Concentration RL PQL
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
3400069
5.7
5.7
5.7
5.7
57
29
57
57
2-Butanone
Carbon disutfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
78-93-3
75-1 5-0
56-23-5
1 08-90-7
75-00-3
290
57
57
57
86
51
5.7
5.7
5.7
17
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
'l
, 1-Dichloroethane
I 1 0-75-8
67-66-3
74-87-3
12448-1
75-34-3
110
5.7
11
5.7
5.7
570
57
57
29
57
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
1,2-Dichloroethane
1,1-Dichloroethene
cis- 1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
107-06-2
75-35-4
1 56-59-2
156-60-5
78-87-5
5.7
5.7
5.7
5.7
11
29
57
57
29
57
cis-1, 3-Dichloropropene
trans-1, 3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
1 0061-01-5
10061-02-6
10041-4
591-78€
75-09-2
11
11
5.7
11
57
57
57
57
110
57
4-Methyl-2-pentanone
Styrene
Tetrachloroethene
1,1,2,2-T etr ach lo roetha n e
Toluene
1 08-1 0-1
100-42-5
127-184
79-34-5
1 08-88-3
290
57
57
57
57
57
5.7
11
11
5.7
1, 1, 1 -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
71-556
79-00-5
79-01-6
1 08-05-4
75-01-4
5.7
11
11
11
11
57
57
57
57
57
Total Xylene 1330-20-7 23 110
Surrogate Recovery
1,2-Dichloroethane-d4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl uorobenzene (SS-3)
103oh
1O0o/o
98o/o
QC Limits
75 - 110
82 - 125
74 - 115
U - Not kecled at the Reporting Limit (RL)
J - Anal/e daected below Praclical Quamibtion Limit (PQL)
E - Extrapolated value. See rerun at dilution.
S - Spike Recoveryoutside acceptedrecovery limits
* - Compound daected above regulatory limit.
X - Not Applicable.
-b
Quelifien:
B-detected in the associated Melhod Blank
Approved 1|/t4/2001 l1:48AM
I
Client Sample ID :
Lab Sample ID :
Date Collected :
Date Received :
Date Prepared :
Date Anallzed :
Percent Moisture :
P3C8GL5
016169-084
tU0U200t
tt/12t200r
rr/t31200t
tllt31200t
9.94
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-602r
Client Project ID : Unocal Parachute
Lab Work Order : 0l{169
Sample Matrix : Soil
Lab File ID : VOA3I I l3\13903.D
Method Blank : RBll l30l
Prep Factor : I
Effective Dilution : 5.55
Method: SW8260B Hazardous Substance List - Volatile Organics Units:rc/Kg
Analyte cAs #Goncentration RL PQL
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67-64-1
7143-2
75-274
75-25-2
74-83-9
330
56
28
56
56
67
5.6
5.6
5.6
5.6
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
78-93-3
75-15-0
56-23-5
1 08-90-7
75-00-3
50
5.6
5.6
5.6
17
280
56
56
56
83
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
1 , 1-Dichloroethane
110-75-8
67-66-3
74-87-3
12448-1
75-34-3
560
56
56
28
56
110
5.6
11
5.6
5.6
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
'l ,2-Dichloroethane
1 , 1-Dichloroethene
cis-1,2-Dichloroethene
trans- 1,2-Dichlo roethene
1,2-Dichloropropane
107-06-2
75-354
I 56-59-2
156-60-5
78-87-5
5.6
5.6
5.6
5.6
11
28
56
56
28
56
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
11
11
5.6
11
5.6
56
56
56
110
56
10061-01-5
10061-026
100414
591-786
75-09-2 20
4-MethyL2-pentanone
Styrene
Tetrachloroethene
1,1,2,2-f et achloroeth a n e
Toluene
1 08-1 0-1
10042-5
127-18-4
79-34-5
1 08-88-3
56
5.6
11
11
5.6
280
56
56
56
56
1 , 1 ,1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
71-556
79-00-5
79-01€
108-054
75-01-4
5.6
11
11
11
11
56
56
56
56
56
Total Xylene 1330-20-7 22 110
Surrogate Recovery
1,2-Dichloroethane-d4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl uorobenzene (SS-3)
104%
101o/o
97%
CIC Limits
75 - 110
82 - 125
74 - 115
U - Not Detected at the Reporting Limit (RI)
J - Analyte ddected below Practical Quantitation Limit (PQL)
E - Extrapolated value. See renrn at dilution.''w'*S - Spike Recovery outside accepted recovery limits
| - Compound detected above regulatory limit.
X - Not Applicable.>
Quelifiers:
z
-
/ Analyst Approved I l/14/2001 11:56AM
Client Sample ID :
Lab Sample ID :
Date Collected :
Date Received .
Date Prepared :
Date Analyzed :
Percent Moisture :
P3C7GL7
0l-6169-09A
lt/0U200t
tUtzt200r
rUt3/2001
tUt3t200t
ll Tl
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Client Project ID : Unocal Parachute
Lab Work Order : 016169
Sample Matrix : Soil
Lab ['ile ID : VOA3lll3\13904.D
Method Blank : RBlll30l
Prep Factor : I
Effective Dilution : 5.66
Method: SW8260B Hazardous Substance List - Volatile Organics Units: pS/Kg
Analyte CAS #Concentration RL PQL
'Ptt
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
340
57
28
57
57
68
5.7
5.7
5.7
5.7
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
78-93-3
75-15-0
56-23-5
1 08-90-7
75-00-3
51
5.7
5.7
5.7
17
280
57
57
57
85
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
110-75-8
6766-3
74-87-3
124-48-1
75-34-3
110
5.7
11
5.7
5.7
570
57
57
28
57
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
107-06-2
75-354
1 56-59-2
1 56-60-5
78-87-5
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
5.7
5.7
5.7
5.7
1',1
28
57
57
28
57
cis- 1, 3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
1 0061-01-5
10061-026
1 00-41 -4
591-786
75-09-2 20
11
11
5.7
11
5.7
57
57
57
110
57
4-Methyl-2-pentanone
Styrene
Tetrachloroethene
1,1,2,2-T elr ach lo roethan e
Toluene
1 08-1 0-1
100-42-5
127-18-4
79-34-5
1 08-88-3
280
57
57
57
57
57
5.7
11
11
5.7
1 ,1 , 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
71-55-6
79-00-5
79-016
108-05-4
75-014
5.7
11
11
11
11
57
57
57
57
57
Total Xylene 1330-20-7 23 110
Surrogate Recovery
1,2-Dichloroethane-d4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl uorobenzene (SS-3)
105o/o
98o/o
97o/o
QC Limits
75 - 110
82 - 125
74 - 115
U - Not Detected at rhe Repo,r'ting Limit (RL)
J - Analyte deleaed below Praaical Quantiation Limit (PQL)
E - Extrapolated value. See rerun at dilution.
B - Analrte detected in lhe associated Method Blank)RL
S - Spike Recovery outside accepted recovery limits
| - Compound dctecred above regulato,ry limit.
X - Not Ap,plicable.
D>
Qudifiers:
/ arriyst Approved ll/14/2001 12:07PM
I
Evergreen Analytical, Inc.
4036 Youngfield St, Wheat Ridge, CO 80033
(303) 42s-6021
Client Sample ID :
Lab Sample ID :
Date Collected :
Date Received :
Date Prepared :
Date Analyzed :
Percent Moisture
P3CIGL6
0l-6169-10A
tU0v200l
tUr2t200t
lUt31200t
tUt3t200t
11.64 Effective Dilution : 5.65
Client Project ID : Unocal Parachute
Lab Work Order : 0l{169
Sample Matrix : Soil
Lab File ID : VOA3ll l3\13907.D
Method Blank : RBlll30l
Prep Factor : I
Method: SW826OB Hazardous Substance List - Volatile Organics Units: FS/KS
Analyte CAS #Concentration RL PQL
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
68
5.7
5.7
5.7
5.7
57
28
57
57
340
.,
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
78-93-3
75-1 5-0
56-23-5
1 08-90-7
75-00-3
51
5.7
5.7
5.7
17
280
57
57
57
85
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
1 , 1-Dichloroethane
110-75-8
67€6-3
74-87-3
12448-1
75-34-3
110
5.7
11
5.7
5.7
570
57
57
28
57
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
107-06-2
75-354
1 56-59-2
1 56-60-5
78-87-5
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
5.7
5.7
57
5.7
11
28
57
57
28
57
cis-1, 3-Dichloropropene
trans-1, 3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
10061-01-5
10061-02-6
100-414
591-78€
75-09-2
11
11
5.7
11
5.7
57
57
57
110
57
4-Methyl-2-pentanone
Styrene
Tetrachloroethene
1,1,2,2-T etr ach lo roeth an e
Toluene
1 08-1 0-1
10042-5
127-18-4
79-34-5
108-88-3
280
57
57
57
57
57
5.7
11
11
5.7
1, 1, 1 -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
71-556
79-00-5
79-01-6
108-05-4
75-014
57
11
11
11
11
57
57
57
57
57
Total Xylene 1330-20-7 110
Surrogate Recovery
1,2-Dichloroethane-d4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl uorobenzene (SS-3)
104o/o
102o/o
960/o
QC Limits
75 - 110
82 - 125
74 - 115
U - Not Detected al lhe Reporting Limit (RL)
J - Analyte detected below Practical Quantitation Limit (PQL)
E - Extrapolated value. See renrn at dilution.
B - Analyte detected in the associated Mahod BlankHl/^_
S - Spike Recovery outside accepred recovery limits
r - Compound detected above regulatory limit.
Y - 1i161 4pplicable.
2<--
Qualifiers:
darratyst Approved 1l/14/2OOl I2:38PM
23
4r
Evergreen Analytical, Inc.
4036 Youngfield St, Wheat Ridge, CO E0033
(303) 42s{021
Client Sample ID :
Lab Sample ID :
Date Collected :
Date Received :
Date Prepared :
Date Analyzed :
Percent Moisture :
P3C2GL9
0l-6169-l lA
tt/0t/2001
lllt2l200l
lUt3t200r
tUt3t200t
884
Client Project ID : Unocal Parachute
Lab Work Order : 016169
Sample Matrix : Soil
Lab File ID : VOA3I I l3\13908.D
Method Blank : RBlll30l
Prep Factor : I
Effective Dilution : 5.48
Method: SW8260B Hazardous Substance List - Volatile Organics Units: rc/KS
Analyte CAS #Concentration RL POL
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67-64-1
7143-2
75-274
75-25-2
74-83-9
66
5.5
5.5
5.5
5.5
55
27
55
55
330
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
78-93-3
75-1 5-0
56-23-5
1 08-90-7
75-00-3
49
5.5
5.5
5.5
'16
270
55
55
55
82
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1 10-75-8
6766-3
74-87-3
12448-1
75-34-3
100
5.5
11
5.5
5.5
550
55
55
27
55
5.5
5.5
5.5
5.5
11
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans- 1, 2-Dichloroethene
1,2-Dichloropropane
107-06-2
75-354
I 56-59-2
156€0-5
78-87-5
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
27
55
55
27
55
cis-1, 3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
10061-0'l-5
10061-02-6
100414
591-786
75-09-2
11
11
5.5
11
5.5
55
55
55
110
55
4-Methyl-2-pentanone
Styrene
Tetrachloroethene
1,1,2,2-I elr ach lo roeth a n e
Toluene
1 08-1 0-1
10042-5
127-184
79-34-s
1 08-88-3
55
5.5
11
11
5.5
270
55
55
55
55
1, 1, 1 -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
71-55€
79-00-5
79-01-6
108-05-4
75-014
5.5
11
11
1',1
11
55
55
55
55
55
Total Xylene 1330-20-7 22 110
Surrogate Recovery
1,2-Dichloroethan+.d4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl uorobenzene (SS-3)
101o/o
105%
91o/o
CIC Limits
75 - 110
82 - 125
74 - 115
U - Not Detected at the Reporting Limit (RI)
J - Analyte detected below Practical Quantitation Limit (PQL)
E - Extrapolafed value. See rerun at dilution.
B - Analvte detested in lhe associated Melhod Blank'0--L- - -)
2t+ )z-/t4-_
S - Spike Recovery outside accepted recovery limits
t - Cornpound detected above regulatory limit.
X - Not Applicable.
D>
Quallfiers:
Arrtytt Approved 11/14/2OOl 12:15PM
20
I
r
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s{021
Client Sample ID : P3C2GL9DUP Client Project ID : Unocal Parachute
Lab Sample ID :01-6169-12A Lab Work Order : 0l-6169
Date Collected : Il/0112001 Sampte Matrix : Soil
Date Received : ll/l2l200l Lab File ID : VOA3lll3\13909.D
Date Prepared : I lll3/2001 Method Blank : RBI I l30l
Date Analyzed : llll3l2O0l Prep Factor : I
Percent Moisture : I l.l2 Effective Dilution : 5.62
Method: SW8260B Hazardous Substance List - Volatile Organics Units: pg/KS
Analyte CAS #PQLRLConcentration
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67s,4-1
7143-2
75-27-4
75-25-2
74-83-9
90 68
5.6
5.6
5.6
5.6
340
56
28
56
56
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
78-93-3
75-15-0
56-23-5
1 08-90-7
75-00-3
51
5.6
5.6
5.6
17
280
56
56
56
84
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1 10-75-8
6766-3
74-87-3
12448-1
75-34-3
110
5.6
11
5.6
5.6
s60
56
56
28
56
1 ,2-Dichloroethane
'1 ,1-Dichloroethene
cis-1,2-Dichloroethene
trans- 1,2-Dichloroethene
1 ,2-Dichloropropane
107-06-2
75-354
1 56-59-2
15660-5
78-87-5
28
56
56
28
56
J
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
5.6
5.6
5.6
5.6
11
cis-1, 3-Dichloropropene
trans-1,3-Dlchloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
10061-01-5
10061-02€
100414
591-78€
7s-09-2 10
11
11
5.6
11
5.6
56
56
56
110
56
4-Methyl-2-pentanone
Styrene
Tetrachloroethene
1, 1,2,2-f etr ach loroeth a n e
Toluene
1 08-1 0-1
10042-5
127-184
79-34-5
1 08-88-3
56
5.6
11
11
5.6
280
56
56
56
56
1 , 1 ,1 -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinylchloride
71-55$
79-00-5
79-01-6
1 08-05-4
75-01-4
5.6
11
11
11
11
56
56
56
56
56
Total Xylene 1330-20-7 22 110
Surrogate Recovery
1,2-Dichloroethaned4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl uorobenzene (SS-3)
107%
119%
83%
QC Limits
75 - 110
82 - 125
74 - 115
U - Not Deteacd at the Reporting Limit (RL)
J - Analyte detected below Praaical Quantitation Limit (PQL)
E - Extrapolated value. See rerun ar dilution
B - Analvte deteaed in the associared Method Blank-var
S - Spike Recovery outside accepted recovery limits
'- Compound detected above regulatory limit.
a - IJs1 Applicable.>
Qualifiers:
/xaill-.Approved 1 1/14/200) 12:53 PM
Client Sample ID : P3C3GL2
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO E0033
(303) 425-6021
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6169
Sample Matrix : Soil
Lab File ID : VOA3lll3\13910.D
Method Blank : RBlll30l
Prep tr'actor : I
Effective Dilution: 5.4
Lab Sample II)
Date Collected
Date Received
Date Prepared
Date Analyzed
: 0l-6169-l3A
: lll0l/2001
: ll/12/2001
: ll/1312001
: ll/13/2001
Percent Moisture : 7.56
Method: SW8260B Hazardous Substance List - Volatile Organics Units: US/Kg
Analyte CAS #Concentration RL PQL
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
65
5.4
5.4
5.4
5.4
54
27
54
54
320
2-Butanone
Carbon disutfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
78-93-3
75-1 5-0
56-23-5
1 08-90-7
75-00-3
49
54
5.4
5.4
'16
270
54
54
54
8'r
2-Chloroethylvinyleth er
Chloroform
Chloromethane
Dibromochloromethane
1 , 1-Dichloroethane
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
100
5.4
11
54
5.4
540
54
54
27
54
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
107-06-2
75-35-4
1 56-59-2
156€0-5
78-87-5
5.4
5.4
5.4
5.4
11
27
54
54
27
54
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
11
11
5.4
11
5.4
54
54
54
110
54
10061-01-5
10061-02-6
100-414
591-78-6
75-09-2
4-Methyl-2-pentanone
Styrene
Tetrachloroethene
1, 1,2,2-T etr ach lo ro eth a n e
Toluene
'108-10-1
100-42-5
127-184
79-34-5
1 08-88-3
270
54
54
54
54
54
5.4
11
11
5.4
1 , 1 ,1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
71-55-6
79-00-5
79-01-6
108-054
75-01-4
5.4
11
11
11
11
54
54
54
54
54
Total Xylene 1330-20-7 22 110
Surrogate Recovery
1,2-Dichloroethane'd4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl ugrobenzene (SS-3)
100%
lOOo/o
9OVo
QC Limits
75 - 110
82 - 125
74 - 115
U - Not Detected at the Reporting Limit (RL)
J - Analyte detected below hactical Quantitation Limit (PQL)
E - Extrapolated value. See rerun at dilution.
detected in the associated Method Bla*
S - Spike Recovery oulside accepted recovery limits
t - Compound detected above regulatory limil.
X - Not Applicable.
Qualifiers:
B.
Analyst Approved 1 1/1 4/2001 I :03 PM
1 ,2-Dichloroethane
1 , 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
Client Sample ID :
Lab Sample ID :
Date Collected :
Date Received :
Date Prepared :
Date Analyzed :
Percent Moisture
P3C9GL7
0l-6169-l4A
tU0t/200t
tv12/2001
lt/t3/2001
tr/13/200t
tt.32
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s{021
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6169
Sample Matrix : Soil
Lab File ID : VOA3lll3\l39ll.D
Method Blank : RBlll30l
Prep Factor : I
Effective Dilution : 5.63
Method: SW8260B Hazardous Substance List - Volatile Organics Units: rc/KS
Analyte CAS #Concentration RL PQL
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
340
56
28
56
56
68
5.6
5.6
5.6
5.6
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
51
5.6
5.6
5.6
17
280
56
56
56
85
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
1 ,1 -Dichloroethane
110-75-8
67-66-3
74-87-3
124-48-1
75-34-3
110
5.6
11
5.6
56
560
56
56
.28
56
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
'1 ,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
107-06-2
75-35-4
1 56-59-2
156$0-5
78-87-5
5.6
5.6
5.6
5.6
11
28
56
56
28
56
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
11
11
5.6
11
5.6
56
56
56
110
56
1 0061 -01 -5
10061-02-6
100-414
591-78€
75-09-2 20
4-Methyl-2-pentanone
Styrene
Tetrachloroethene
1, 1,2,2-T etr ach I o roeth a n e
Toluene
1 08-1 0-1
104-42-5
127-184
79-34-5
1 08-88-3
280
56
56
56
56
56
5.6
11
11
5.6
1 , 1 ,1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
71-556
79-00-5
79-01-6
1 08-05-4
75-01-4
56
11
11
11
11
56
56
56
56
56
Total Xylene 1330-20-7 23 '1 10
Sunogate Recovery
1,2-Dichloroethane-d4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl uorobenzene (SS-3)
1O1o/o
1O3o/o
9}Yo
QC Limils
75 - 110
82 - 125
74 - 115
U - Not Detected al the Reporting Limit (RL)
J - Analye deleaed below Practical Quantitation Limit (PQL)
E - Extrapolaled value. See rerun at dilution.
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
* - Compound detected above regulatory limit.
X - Not Applicable.-2u-HAr
Qualifiers:
FrryT Approved ll/14/2001 1:lOPlvl
Client Sample ID : P3C4GL4
Lab Sample ID : 0t-6169-l5A'
Date Collected : lll0l/2O01
Date Received : llll2/2o01
Date Prepared : ll/13/2O01
Date Analyzed : lll13/2001
Percent Moisture : 12.01
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO E0033
(303) 42s-6021
Client Project ID : Unocal Parachute
Lab Work Order : 0l-6169
Sample Matrix : Soil
Lab File ID : VOA3lll3\13912.D
Method Blank : RBlll30l
Prep Factor : I
Effective Dilution : 5.68
Method: SW8260B Hazardous Substance List - Volatile Organics Units: pg/Kg
Analyte CAS #PQLRLGoncentration
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
68
5.7
5.7
5.7
5.7
57
28
57
57
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
340
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
78-93-3
75-15-0
56-23-5
1 08-90-7
75-00-3
51
5.7
5.7
5.7
17
280
57
57
57
85
2-C hloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
1 , 1-Dichloroethane
1 10-75-8
67-66-3
74-87-3
124-48-1
75-34-3
110
5.7
11
5.7
5.7
570
57
57
28
57
1 ,2-Dichloroethane
I , 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
5.7
5.7
5.7
5.7
11
28
57
57
28
57
cis-1,3-Dichloropropene
trans-1, 3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
11
11
5.7
11
5.7
57
57
57
110
57
10061-01-5
10061-02-6
100-414
591-78$
75-09-2 20
4-Methyl-2-pentanone
Styrene
Tetrachloroethene
1,1,2,2-T elr ach lo roeth a n e
Toluene
1 08-1 0-1
100-42-5
127-184
79-34-5
1 08-88-3
57
5.7
11
11
5.7
280
57
57
57
57
1 ,1 , 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
5.7
11
11
11
11
57
57
57
57
57
71-55-6
79-00-5
79-01€
1 08-05-4
75-O1-4
Total Xylene 1330-20-7 23 110
Surrogate Recovery
1,2-Dichloroethane-d4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl uorobenzene (SS-3)
102%
102%
93%
QC Limits
75 - 110
82 - 125
74 - 115
U - Not Detec'ted at the Rcporting Limit (RL)
J - Analle detected below Practical Quantitation Limit (PQL)
E - E:<trapolared value. See rerun at dilution.
S - Spike Recovery outside accepted recovery limits
r - Compound detected above regulatory limit.
X - Not Applicable.
72
Qualifiers:
B - Analyte the mmiated Method Blank
Approved l1/14/2001 1:17PM
I
107-06-2
75-35-4
1 56-59-2
156€0-5
78-87-5
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO E0033
(303) 42s-6021
Client Sample ID : P3C5HS4 Client Project ID : Unocal Parachute
Lab Sample ID : 0l{169-16A Lab Work Order : 016169
Date Collected : I l/01/2001 Sample Matrix : Soil
Date Received z ll/12/2001 Lab File ID : VOA3lll3\13913.D
Date Prepared : I l/1312001 Method Blank : RBI I l30l
Date Analyzed : llll3/2001 Prep Factor : I
Percent Moisture : 12.3 Effective Dilution : 5.7
Method: SW8260B Hazardous Substance List - Volatile Organics Units: pg/Ks
Analyte cAs #RL PQLGoncentration
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67-64-1
7143-2
75-27-4
75-25-2
74-83-9
68
5.7
5.7
5.7
5.7
340
57
28
57
57
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
51
5.7
5.7
5.7
17
280
57
57
57
86
78-93-3
75-1 5-0
56-23-5
108-90-7
75-00-3
2-C hloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
1 , 1-Dichloroethane
110-75-8
67-66-3
74-87-3
12448-1
75-34-3
110
5.7
11
5.7
5.7
570
57
57
28
57
1,2-Dichloroethane
1 ,1-Dichloroethene
cis-1,2-Dichloroethene
trans- 1,2-Dichloroethene
1 ,2-Dichloropropane
107-06-2
75-354
'156-59-2
156€0-5
78-87-5
28
57
57
28
57
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
5.7
5.7
5.7
5.7
11
cis-1, 3-Dichloropropene
trans-1, 3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
10061-01-5
10061-026
100414
591-786
75-09-2 0
11
11
5.7
11
5.7
57
57
57
110
57
4-Methyl-2-pentanone
Styrene
Tetrachloroethene
1,1,2,2-T elrachloroethane
Toluene
1 08-1 0-1
100-42-5
127-184
79-34-5
1 08-88-3
57
57
11
11
5.7
280
57
57
57
57
1 ,'1 , 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
71-55-6
79-00-5
79-01-6
108-05-4
75-01-4
5.7
11
11
11
11
57
57
57
57
57
Total Xylene 1330-20-7 23 110
Surrogate Recovery
1,2-Dichloroethane-d4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl uorobenzene (SS-3)
101o/o
102o/o
88o/o
QC Limits
75 - 110
82 - 125
74 - 115
U - Not Detected at the Reporting Linit (RL)
J - Analyte detected below Praclical Quantitation Limit (PQL)
E - Extrapolated value. See rerun at dilution.
the associated Method Blank
S - Spike Recovery outside accepted recovery limits
t - Compound detected above regulatory limit.
X - Not epplicable.
vo
Qualifiers:
B-
Analyst Approved 11/14/2001 l:25PM
i
Client Sample ID : P3C5GL6
Lab Sample ID : 0l-6169-l7A
DateCollected : ll/01/2001
Date Received : ll/12/2001
DatePrepared : ll/1312001
Date Analyzed : llll3/2O01
Percent Moisture : 12.85
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 425-6021
Client Project ID : Unocal Parachute
Lab Work Order : 015169
Sample Matrix : Soil
Lab file ID : VOA3IIl3\139l4.D
Method Blank : RBlll30l
Prep Factor : I
Effective Dilution : 5.73
Method: SW8260B Hazardous Substance List - Volatile Organics Units: pS/Kg
Analyte CAS #Concentration RL PQL
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67-64-1
7143-2
75-27-4
75-25-2
74-83-9
69
5.7
5.7
5.7
5.7
57
29
57
57
340
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
78-93-3
75-15-0
56-23-5
108-90-7
75-00-3
52
5.7
5.7
5.7
17
290
57
57
57
86
2-C hloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
1,1-Dichloroethane
1 10-75-8
67-66-3
74-87-3
124-48-1
75-34-3
1'10
5.7
11
5.7
5.7
570
57
57
.29
57
1,2-Dichloroethane
1 ,1-Dichloroethene
cis- 1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
107-06-2
75-35-4
1 56-59-2
1 56-60-s
78-87-5
29
57
57
29
57
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
J
U
U
U
U
U
U
U
U
U
U
U
5.7
5.7
5.7
5.7
11
cis-1, 3-Dichloropropene
trans-1, 3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
10061-01-5
1 0061 -02-6
't00-414
591-78-6
75-09-2 8
11
11
5.7
11
5.7
57
57
57
110
57
4-Methyl-2-pentanone
Styrene
Tetrachloroethene
1,1,2,2-f et ach lo roeth ane
Toluene
1 08-1 0-1
100-42-5
127-184
79-34-5
1 08-88-3
57
5.7
11
11
5.7
290
57
57
57
57
1, 1, 1 -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
71-55S
79-00-5
79-01-6
1 08-05-4
75-014
5.7
11
11
11
11
57
57
57
57
57
Total Xylene 1330-20-7 23 110
Surrogate Recovery
1,2-Dichloroethane-d4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl uorobenzene (SS-3)
103o/o
99o/o
92o/o
QC Limits
75 - 110
82 - 125
74 - 115
U - Not Detected at the Reporting Limit (RL)
J - Analyte detected below Praaical Quantitation Limit (PQL)
E - Extrapolated value. See renrn at dilution.
in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
| - Compound detected above regulatory limit.
X - Not Applicable.
tu
Quallfiers:
B.
Analyst Approved ll/14/2001 I:3) PM
I
Lab Sample ID
Date Prepared
Date Analyzed
RBI I l30l
tUt3t200t
tt/1312001
Evergreen Analytical, Inc.
4036 Youngfield St., Wheat Ridge, CO 80033
(303) 42s-6021
Method Blank Report
Client Project ID : Unocal Parachute
Lab Work Order: 0l-6169
Lab File ID : VOA3lll3\13893.D
Prep Factor : I
Effective Dilution : I
Method: SW8260B voA 8260 Units: pg/Kg
Analyte CAS #RLConcentration PQL
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
67-64-1
71-43-2
75-27-4
75-25-2
74-83-9
2
1
1
1
1
1 60
10
5
10
10
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
78-93-3
75-15-0
56-23-5
1 08-90-7
75-00-3
I
I
1
1
3
50
10
10
10
15
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
1,'t-Dichloroethane
110-75-8
67€6-3
74-87-3
124-48-1
75-34-3
19
1
2
1
1
100
10
10
5
10
1,2-Dichloroethane
1 ,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1, 2-Dichloroethene
1,2-Dichloropropane
107-06-2
75-354
156-59-2
1 56-60-5
78-87-5
5
10
10
5
10
1
1
1
1
2
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
10061-01-5
10061-02-6
100-41-4
591-78-6
75-09-2
2
2
1
2
1
10
10
10
20
10
4-Methyl-2-pentanone
Styrene
Tetrachloroethene
1, 1,2,2-T etr ach lo roeth ane
Toluene
1 08-1 0-1
10042-5
127-18-4
79-34-5
1 08-88-3
10
1
2
2
1
50
10
10
10
10
1, 1, 1 -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl acetate
Vinyl chloride
71-55-6
79-00-5
79-01-6
108-05-4
75-01-4
1
2
2
2
2
10
10
10
10
10
Total Xylene 1330-20-7 4 20
Surrogate Recovery
1,2-Dichloroethane-d4 (SS-1 )
Toluene-d8 (SS-2)
4-Bromofl uorobenzene (SS-3)
99o/o
97o/o
98%
QC Limits
75 - 110
82 - 125
74 - 115
U - Not Derected at the Reporting Limit (RL)
J - Analyte detected below hactical Quantitation Limit (PQL)
E - Extrapolated value. See rerun at dilution.
B - Analyte detected in lhe associated Method Blank
S - Spike Recovery outside accepted recovery limits
X - Not fuplicable.
'-P---Klo,
Qualiliers:
/nr:rrtyst Approved 11/14/2001 10:55AM
I
cis-1,3-Dichloropropene
trans-1, 3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
Evergreen Analytical, Inc Dale: l4-Nov-2001
CLIENT:
Work Order:
Key Laboratories
0l-6169
Unocal Parachute
QC SUMMARY REPORT
Laboratory Control Spike - generic
Sample lD: LCSl11301
Client lD:
Analyte
Matrix: Soil Test Code: SW8260B
Batch lD: VOA-3_011113A
PQL SPK value SPK Ref Val
Run lD: VOAS_0l1113A
Seq No: 3tl882il
LowLimit HighLimit RPD Ref Val
202
12',1
1N
150
161
163
137
't24
't16
144
165
1Zi
137
132
127
1B
123
122
't21
1m
119
132
123
180
125
173
127
12'l
158
Prep Date: 13-Nov-2001
Analysis Date: 13-Nov-2001 1:02 PM
%RPD RPDLimit Qual
Units: pg/Kg
%REC
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-C hloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
1 ,1 -Dichloroethane
1 ,2-Dichloroethane
I ,1-Dichloroethene
cis-,l,2-Dichloroethene
trans-1,2-Dichloroethene
1 ,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Methylene chloride
utMethyl-2-pentanone
Styrene
Tekachloroethene
1, 1,2,2-Tetrachloroethane
Result
47.94
49.28
47.49
40.88
47.14
43.99
52.57
6.24
48.98
52.72
4.O7
51 .92
44.05
45.77
53.3
51.26
55.11
52.76
55.01
49.45
49.43
47.'.t3
49.66
M.62
50.57
45.97
45.46
47.92
44.66
60
10
5
't0
10
50
10
10
10
15
100
10
10
5
10
5
10
10
5
10
10
10
10
20
10
50
10
10
10
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
24
79
79
67
38
69
6l
77
82
61
36
78
58
7E
76
79
75
77
76
81
81
82
69
60
75
62
77
71
62
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
53
47
50
50
50
50
50
50
50
95.9%
98.6%
95.0%
81.8%
94.3%
88.0%
105.1%
92.5%
98.0%
't05.4%
96.1%
103.8%
88.1%
91.5%
't06.6%
102.5%
110.2%
't05.5%
110.0%
98.9%
93.3%
100.3%
99.3%
89.2%
101.'t%
91.9%
90.9%
95.8%
89.3%
J
J
J
J
ND - Not Detected at the Reporting Limit
J - An.l)4e detected below quantilation limits
i - Not applicable to matrix spikes or LCS.
E - Analyte detected above calibration limits
B - Analyte delected in the associated Method Blank
S - Spike Recovery outside accepted recovery limils
R - RPD outside acceped recovery limits
Qualltler::
I of 3
MW
Key Laboratories
2479 Rjver Road, Unit A
Grand Junction, Colorado 8 1502
Phone (970) 243-5311 Fax (970) 243-6010
Lab Sample ID:
Client Sample ID:
Client Project ID:
Date Sampled:
Date Received:
Date Reported:
0t-1264
P3C6HS1+I
Pond #3 Closure
l1l15/01
lll15/01 @ 10:10
r 1/l 5/01
soI
UNOCAL
Dick Brammer
546 Main St. #404
Grand Junction, CO 81501
UOC Phone: 241-7632, Fax: 241-0065
HLA Phone: 242-5784
Sample Matrix :
Preservation:
QAQC Number:
Pre-Treatments/dig.:
coc 2388
EPA 3O5IA
EPA IVIethod
Parameter Results RSD Units MDL Date MCL
Metals
6020 Total Arsenic 6.83 0.7 mg/Kg 0.06 I l/15/01
Notes: RSD - Relative Standard Deviation, MDL - Method Detection Limit, MCL - Maximum Concentration Limit., nd - not detected.
tt/ t5/0t
Page 1
\
MW
Key Laboratories
2479 Nver Road, Unit A
Grand Junction, Colorado 81502
Phone (970) 243-5311 Fax (970) 243-6010
Lab Sample ID:
Client Sample ID:
Client Project ID:
Date Sampled:
Date Received:
Date Reported:
0r-1265
P3C11HS2+1
Pond #3 Closure
I t/15/01
lll15/01 @ 10:10
tutSt0t
SOIL
LINOCAL
Dick Brammer
546 Main St. #404
Grand Junction, CO 81501
UOC Phone: 241-7632, Fax: 241-0065
HLA Phone: 242-5784
Sample Matrix :
Preservation:
QAQC Number:
Pre-Treatrnents/dig.
coc 2388
EPA 3O5IA
l
N
)
EPA Method
6020
Parameter
Metals
Total Arsenic
Results RSD Units MDL Date MCL
6.68 2.3 mg/Kg 0.06 tUtst}t
Notes: RSD - Relative Standard Deviation, MDL - Method Detection Limit, MCL - Maximum Concentration Limit., nd - not detected.
tt/ t5/01
Page 1
I
i
MW
Key Laboratories
2479 River Road, Unit A
Grand Junction, Colorado 81502
Phone (970) 243-5311 Fax (970) 243-6010
LINOCAL
Dick Brammer
546 Main St. #404
Grand Junction, CO 81501
UOC Phone: 241-7632, Fax: 241-0065
HLA Phone: 242-5784
Lab Sample ID:
Client Sample ID:
Client Project ID:
Date Sampled:
Date Received:
Date Reported:
0t-1266
P3ClOHS3+I
Pond #3 Closure
tUtSt0t
ll/15/01 @ 10:10
tLnSt0l
SOIL
coc 2388
EPA 3O5IA
Sample Matrix :
Preservation:
QAQC Number:
Pre-Treaftnents/dig.
0
EPA Method
Parameter
Metals
6020 Total Arsenic
Results RSD Units MDL Date MCL
5.89 2.6 mg/Kg 0.06 ttlts/Ot
i
Notes: RSD - Relative Standard Deviation, MDL - Method Detection Limit, MCL - Maximum Concentration Limit., nd - not detected
1,t/ 15/0t
Page 1
MW
Key Laboratories
2479 River Road, Unit A
Grand Junction, Colorado 81502
Phone (970) 243-5311 Fax (970) 243-6010
UNOCAL
Dick Brammer
546 Main St. #404
Grand Junction, CO 81501
UOC Phone: 241-7632, Fax: 241-0065
HLA Phone: 242-5784
EPA Method
Parameter
Metals
6020 Total Arsenic
coc 2388
EPA 305 I
Results RSD Units MDL Date MCL
% RECOVERY
9s.78 l1l15l0t
Lab Sample ID:
Client Sample ID:
Client Project ID:
Date Sampled:
Date Received:
Date Reported:
Sample Matrix :
Preservation:
QAQC Number:
0I-1266 SPIKE
P3CIOHS3+1
Pond #3 Closure
tUtSt0t
1l/15/01 @ 10:10
lutSt0t
SOIL
\
Notes: RSD - Relative Standard Deviation, MDL - Method Detection Limit, MCL - Maximum concentration Limit., nd - not detected.
Lt/15/0r
Page 1
,i
I
ffi . rrrttr{r- tu I r..r ffi
.i-.lffiffi:
I WW
Key Laboratories
2479 River Road, Unit A
Grand Junction, Colorado 81502
Phone (970) 243-5311 Fax (970) 243-6010
Lab Sample ID:
Client Sample ID
Client Project ID:
Date Sampled:
Date Received:
Date Reported:
LAB BLANK
Pond #3 Closure
I 1/15/01
ttltsl0t @ 10:10
I 1/1 5/0 I
WATER
at'
l
LINOCAL
Dick Brammer
546 Main St. #404
Grand Junction, CO 81501
UOC Phone: 241-7632, Fax: 241-0065
HLA Phone: 242-5784
Sample Matrix :
Preservation:
QAQC Number:
Pre-Treatrnents/dig. :
EPA Method
Parameter Results RSD [Inits MDL Date MCL
Metals
6020 Total Arsenic 0.00006 mglL 0.06 I l/15/01
Notes: RSD - Relative Standard Deviation, MDL - Method Detection Limit, MCL - Maximum Concentration Limit., nd - not detected.
rt/t5/0t
Page 1 JK*,"*",
Appendix E
AGENCY CORRESPONDENGE AND LETTERS
'ruL-22-Et? 13.51 FROU.HARDING LAwEoN ABaoc. ID.goa2E24ElGl
07/2ltgi 08:ll trlI S0ilTEgSlES CDff,E H^'rlT PAGE 2/2gogt
STATEOFCOIOI(ADO
Frybrcr,(hurrrir-skqft,harirBlcl
f&d opct5rJ&rpfry*htsrrrdmrac* C lt p4 dM
HA'ATDOIII ilmilXJ pw/l5rE tAIrOInII qu3(Il
@
{IoECbrYord(f-A AnS.ChM.hllt2
Ocav:t A&ndc ffi2-1580 CnadjtnCq,Colcr&lr5m-Iln6ltlleBGlESL:lsm DlFatuDrartrSlf*tro$,tT$l' ld662aart5
JUlyZl,1997
Itilr. BiohsdL fucr, ldErtrr
ttnmdCcportim
P.O. Btr 9r,
ttraeht, Cotsdo 81635.007
Hl{tFst{fr ttt qr5 F&t
t Lp S"I^rrtrf oh*.r[+r,.E!.
tFltt T'7gl49?,.597lD-'l{rs t[t
BEt Clonur Plt fu Taporrry Birfu L 4 rod 3l rsil CImc PIll fu tto Courtmdim
Crnt Eoet Du{ PrrM CtGkSd! OA Upp& Fidlily
DE{ ifr. FrqIFrGr,
ltr Coludo Uesrud of h$UE forlL d ErvtrmeA, Erartous filrtdrtr pd flese
Melgmrrt, Divido (fu DtyHcr[ nndtd E eEaE .r i'g frE F&lic mo pciod sn ihe
!bou. rr&urod CXolurt EIEs. fbcrtert, bd o E pveicns rrflifi oftto GbEE llas, wE
tFouy rygrwe tn RCRA Ctoil. Ct'ruc HE fu Try E .irr l, 2. qd 3 Gd b AwsErdor
Cqllloldhg Pqd.
[f ytu hcrE ry grfrig rugrding lhcs trilm, plpre crll ua s CJO3) 692-3356-
Ldrr
PcmiEudcryllrethir
Fcdut FriHicr ProFUI
oq Erdr:ir,bB-Dsmdg CDPHEIIIIEMD
ScUcDdr, EPA
Addd CoW Dsft6lu of oanlopmt
ILvidBmtrq AOO
Jul-22-99 04:28pm From-HLA COI\ISTRUCTI0N DIV
07 /22/gg 15:36 Ef97028593al
+303221 I 361
UNULAL AA\
T-583 P.02 F-183
UilOGAL@
Unocal Corporedoa
OhrsEilied Businreses
PO Eor 907
10705 Counry Road 215
Parachute. colorado E1 635
Telephone (grct 205-7600
Facsimile (s70) 245-9334
July'1, 1999
Bichard L Bmmmer
R€Eidenl iarrrsEi
Erwrloononret homgoiation Scrvioa Mr. Gregg R. Squire
Colorado Department gf Natural
Resources
DMsion of Minerals and Geology
1313 Sherman Strest, Room 215
Denve( Golorado 80203
UnocalTamporary B.Fin No. 3
Salt Disposa! Project
Parachute, Colorado
Dear Gregg:
The purpose of thls letter is to inform the Colorado Division of Minerals and Geology
(DMG) of the Unocal Oil Company of Callbmia's (dba Unocal) intent to place certain
uraste materials in tre Unocal Parachute Creek Shale Oll Project mine as part of the
RetoruUpgmde dEcommissioning and closure activities atthe Unocalfacility near
Paradrrrte. Colorado. The decommissioning and closure activitiEs ane scheduled for
la6 summer 1999 and 2000. Unocalhas revlened state environmental prograrns and
conesponding regulations that may affed the projec{. This letter describes horv waste
materials willbe managed in aocordance with the applicable regulations and solicG
DMG's comments on our proposed approacfi.
Wasta Materials
The Unocal Paracfiute Creek Shale Oll Project conslsted of a 13,500 ton-perday mine,
a 10,000 barrel-perday abweground Rdort Facility. where oilshale was heated to
recover raw shale oil, and a 10,000 barrel-perday Upgrade Facll3ty where raw shale oil
uras @nvert'Ed lnto syncrude. Dudng the period of operations, a series of surf;ace
impoundmenb at the Upgrade Facilfi received trcaEd nraters fiom process areas.
Procgss waters floued fiom the Upgrade Facility production units through the oily water
sewer lines, the API Separator, and lnto the Active/lnactive Basins. These waters were
then eused to moisturize and cool retorted shale- \Mten watef production exceeded
the amountthat could be reused, tfie waterwa's diverted from the Ac{iva/lnadive
Basins through the Plant Effluent Llft Station to the Holding Pond and the three
Temporary Basins located atthe Upgrade Facility.
Jul-22-98 04:28pm From-HLA C0I{STRUCTI0N DIV
o7 / 22/ SS t5 z 27 8S7 o2I593 34
+303221 I 361
UlvA! AItr
T-583 P.03/tZ F-483
cregg Squire, (DMG)
July 1, 1999
Page 2 of 3
Process waters stored in the Unocal Upgrade Facilrty basins from 1991 were
characteristt'cally hazardous due to elevated concerrtrations of arsenlc and benzene
and were regulated by the Hazardous Matedals and Waste Managemefi Division of
CDPHE. Unocalbegan closure of the basins in 1994, and to date, the Astive Basin,
lnactive Basin, Holding Pond, and Temporary. Basin Nos. 1 and 2 have approved clean
dosure ceffications firom CDPHE. As part of closure, Unocaltreated approximately
25 miltion gallons of hazardous wastanrater to reduce the aeenic conoenhations to
nonhazardous levels. Temporary Basin No. 3 is the last basin to be closed and
contains approximately 10 million gallons qf nonhazardous wastewater.
To compleE closure of Temporary Basin No. 3, Unocalwillevaponate the 10 milllon
gallons to approrimately 2.5 million gallons of nonhazardous liquid and treat the water
in a submerged quench evapomtor. Because the vrater is high in total dissolved solids
(IDS), the finalteatnent willyield approximately 2000 tons of a nonhazardous salt
materialthatwlll subscquently be solidffied wtth fly ash or cement klln dusL wttich wlll
increase the amount of materialto about 4000 tonB. Based on bencfi scale tests, fie
saft material is erpested to be nonhazardous. Unocal conducted pllot Esting of
submerged quenc-tr evaporabr systems ln June 19e9. Atthattime, samples of the satt
matErialwere collested fortesting to confirm that lt is indeed nonhazardots, ln
addilion, Unocalwill colleet sampl* of the material when full scale operations begin in
2000 to confirm the characterization of the materials- AnalyticalresuJts of the salt
materialfrom the pilottests and fullscale operation wtll be provlded fur your review.
Unocalwill place the solidified nonhazardous material in an engineered rcpository in the
Unocal Panactrute CreEk Shale Oil Project oil shale minE, as further described beloral.
No hazardous wastes will be placed in the mine-
Repository Design
The repository will be located just inside the rnine in an unused heading orffthe
Conveyor Drlft, as shonn in Figure 1. Access to the area wlll be through the Main
Reftrm Airway and the 106 Drift, as shown in Figure 2- Figure 3 shovrrs a concepfual
isomEtrlc of the rEposibry. ln general, a 1-fostthict sand base wlllbe placed in the
repository and then werlain with a 60 mil HDPE llner or40 mil reirrforaed PP linerthat
will be anchorsd irrto the ribs of thE heading. A z-foot protective layer of sand will be
placed on top of the liner, as shorrn in Figurc 4.
This portion of the mine is dry and no urater is erpec{ed b enbrthe heading.
Nevertheless, the reposltory is deslgned to keep uraterftom entering and mntacting thE
uraste mabrial, and to eliminac migration of liquids from the cell, if any. Therefore,
once the solidified salt material has been placed in the repository, a @ver liner will be
placed over thE materiat and welded to the boftom and vrrall liner as shown in
I
Ju l -22-99 01 r 28pn F
o7/22/99 15:27
ron-HLA C0IISTRUCTI0N DIV +303221 I 361
A.ug - _-__
T-583 P.01/12 F-183
+!l_ey ESgzozss93J4
Gregg Squire, (DMG)
July 1,'1999
Page 3 of 3
Figures 5 through 7. The heading wtth the totally-sealed reposltory willthen be bermed
offto dbaltour any later traffic into the area.
Regulatory Compliance
The satt material that will be placed in the repository is a nonhazardous solid uraste
resulting from the final treatment of wasfierreater stored in Ternporary Basin No. 3. As
describEd above, the materialwill not be a characteristic or listed hazardous \i/aste
according to the regulations in 6 CCR 1007{, part 261, and will not be regulated under
the RCRA hazardoue waste regulations. Because the mlne and retort facility are
regulated under the Colorado Division of Minenals and Geology (DMG) Permit
M-78.263UG, the plaoement of the salt material in the mine is also exemptffom the
stab solid waste regulatlons as stated at 6 GCR 1007-2, section 1.4.2. That section
states that facilities for solid raraste disposal are exempt from the solid vnaste permifting
provisions where a person "engaged in mining operations permitted by IDMGI performs
solict waste disposal of mlning or other solid wastes generated by such operations
wifrrin the permitted area for suott operatlons."
No additional permits appear to be necessary for placement of the materials in the
mine. Nonetheless, Unocal notified Ms. Donna Stoner (CDPHE) regarding solid urasb
and Mr. Joe Sctrie{felin (GDPHE){razardous waste, regarding the mine permit, to
confirm that the GDPHE ls in agreemEnt wtth the proPosed approach. A copy of Ms.
Stone/s approrral letter dated June 18, 1999 is atached-
Unocal will schadule contrac'tors to begin construstion of the reposibry later this
summer and begin placement of material in the spring of 2000- This letbr is intended
to inform you of the underground repository as we continue to decommission the
Parachute Creek Shale Oil Shale Facilities and solicit any comments CDPHE may have
with this proposed approaclr. Please call me al97U2E5-7600 exL?22 if yotl have any
questons or wlsh to arrange yoursite vis'tt l'll be orfi of the office July 12-1S.
Sincerely,
Richard L. Brammer
Asset Manager
Attaoh.
Jul-22-99 01:29pm From-HLA C0I\STRUCTIOiI DIV +303221 I 36t T-583 P.05/12 F-183
STATEOFCOLOTUDO
Eif OilqrtGwnf
|rnGEl5ltdr &qdrrCIrcca
arft1d 5 p-mi*.ad i'rp.a,lqg d|a hoilf end cnviorrarrrr of drc popE of
Cnd lusin RcrinelOfficr
2r:l 5. G.t 9- REIlrGradtndcr. @ AS0t-276!
fer lgroa 2{8.7t9C Jfi 2 I lssg
h\
CdoradoDuruntnr
oftutEfkdA."'ardErvimnrna
alune 18, L999
Ilti. Leon Pahlar, Ph.o-, senLoE Scient,ist MvLsor
Unocal CorporatlonP.o. Box 9O?Paractrute co 81635
EE: Unocal. Teuporary Basin No.f salt Disposal Project
Patraehute, Gartield Countsy, Colofado
fhe C'olorado Delnz{oenE of Rrblic Health and, EnvironDen€, HazardousUaterials and Waste lttanageTerrt Division has reviewed the tenporarysasin #3 SaIt X"reatnent and Dlsposal Plan for ttre above referencedsite. The report tras subnitted for revier June Z, 1999. lthe
Prrrpose of the t-reatuent and distrlosal activities is to coaplete ttreclosure of TeBEorary Basin No. 3.
After carGful conslderation ve are pleased to grant an apprsvial ofttre t Eoposed treatment and dlsposal activitiea to be corrducted attlris site. Bouever, placement of the salt naterial ln the uinenust be in eoupliance with the Colorado Division of t(inerals andGeology reEu1atl,ons.
Iour coSreration Ln dealing ;lroperly witlr tbis site ls a;rpreciated.
Should you lrave any gue-stions concerning thls letter, fee)- free tocontact ue at 970-24A-7168.
0
Dorura Stoner
enrlronnenta1 ProtectLon Specialist
So],l.d Baete UnItempl:lance prograE
:le
l{r. ,foe SchlGftelln, CDEEE, Denver
8W GAR MTO 4EEiIe
^a.nf Aa rD lta1---^^-- r a tra
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Jul-22-89 01:29pn From-HLA C0IISTRUCTl0t{ DIV
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UNOCAL@
Unoca! Corporatlon
R€al Estate, Remediation Servicos, Mining Operations
546 Meln Sl. #404
Grand Junction, Colorado 81501
Telephone: (970) 241 -7632
Facsimile (970) 241 -0065
April 12,2001
Rlchard L Brammer
Aros Manag€r
Eastem Regbn
Mr. Gregg R. Squire
Division of Minerals and Geology
Department of Natural Resources
1313 Sherman Street, Room 215
Denver, Colorado 80203
!lv:
Richard Brammer
N
Dear Mr. Squire:
Unocal would like to change the location in the Long Ridge Mine of the approved
depository for the solidified salts recovered an the closure of Temporary Basin#3.
The requested alternative location is within the ore storage gallery toward the
south wall and beyond the draw down cone of any reclaim feeder. Being in a
dead storage area the material would not be disturbed in any future activity if the
mine were restarted. This location is dry and has a floor comprised of twenty feet
thickness of concrete separating the storage area from the lower reclaim feeder
tunnel. This dry, sealed area would preclude the need to contain the stabilized
salts within a wrapping, as was the previous depository configuration.
The materialwould be stacked on the floor; covered with the high-density
polyethylene pond liner and guarded with concrete barriers so as to prevent
future disturbance from any renewed activity.
The bench testing has shown the solidified material to be wellwithin the
parameters of safety as depicted by the Toxic Characteristic Leaching
Procedure. The leaching limits of arsenic from Unocal's testing were 0.3 to 0.4
ppm. are below the RCRA hazardous limits.
l-
Ref: Permit number 78-263
Attachments: Map of location
Laboratory data
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Key l:boratories
2479 River Road. Unir A
Grand Junction, Colorado 8 l -502
Phone (970) 243-531I Fax (970) 24-1-60t0
UNOCAL
Dick Brammer
546 Main St. #404
Grand Junction, CO 8l -501
UOC Phone: 241-7632. Far: 241-0065
HLA Phone: 242-5784
EPA ll{ethod
Parameter
I\{etals
Lab Sanrple ID:
Client Saurple ID:
Client Project ID:
Date Sampled:
Dale Received:
Date Reported:
0l-0156
uol-10
TINOCAL TEIT{P 3
3/13/01
3/13/01 @ 17:00
3n6t0r
SOLIDS
coc2208
TCLP EXTRACTION
Sanrple Matrix :
Preservation:
QAQC Number:
Pre-Treatmens/dig.:
Results RSD Units MDL Date N{CL
6020
6020
TCLP Arsenic
TCLP Selenium
0.30
nd
0.06
0.06
mg/L
mg/L
3/t6t0t
3/t6/0t
Notes: RSD - Relarive Standard Deviation, MDL - Merhod Detecrion Limir,MCL - Maximum Concentration Limit., nd - not detected.
)/ 16/0t
l':r.4c I A na lyst/l(cv icwcr
1.5
nd
I
mafrepoCI0
Key l"aboratories
2479 River Road. Uuit A
Grand Jrurction. Colorado 8 1502
Phone (970) 241-53 I I Fax (970) 243-6010
UNOCAL
Dick Branmrer
546 Main Sr. #404
Grand Junction, CO 81501
UOC Phone: 241-7632, Fax: 241-0065
HLA Phone: 242-5784
EPA I\Iethod
;, Parameteri_ _:::.:..::_i:.
IUetals
Results RSD Units MDL Date MCL
Lab Sample ID:
Client Sample ID
Client Projecr ID:
Date Sampled:
Date Received:
Date Reported:
Sauple Mauix :
Preservation:
QAQC Number:
Pre-Treatrnens/dig.:
0l-0155
uol-9
I.'NOCAL TEII{P 3
3/13/01
3/13/01 @ l7:00
3/16/01
SOLIDS
coc2208
TCLP EXTRACTION
6020
6020
TCLP Arsenic
TCLP Selenium
0.30
nd
0.7
nd
mg/L
mg/L
0.06
0.06
3n6t0t
3/16t01
Notes: RSD - Relative Standard Dcviation, MDL - Merhod Derecrion Limir, MCL - Maximum Conccntration Limit., nd - not dctccted
1/ 16/01
I':rgc I Analyst/ltcv icwcr
I
:r
I
I
MW
Key l-aboratories
2479 Rivcr Road. Unit A
Grand Junction. Colorado 81502
Phone (970) 24-1-53I I Fax (970) 243-60l0
UNOCAL
Dick Brammer
546 Main St. #404
Grand Junction, CO 81501
UOC Plrone: 241-7632, Fax: 241-0065
HLA Phone: 242-5184
Lab Saurple [D:
Client Sample ID
Client Proiecr ID:
Date Sanpled:
Date Received:
Date Reported:
Sanple Matrix :
Presen,ation:
QAQC Number:
Pre-Treauuens/dig.
0l-0154
trol-7
TINOCAL TEI\{P 3
3/r3/0r
3/13/01 @ l7:00
3/16/01
SOLIDS
coc2208
TCLP EXTRACTION
Units I\{DL Date MCL
6020
6020
Metals
TCLP Arsenic
TCLP Selenium
0.40
nd
mg/L0.3
nd mg/L
0.06
0.06
3tr6t0r
3n6/01
J
Notes: RSD - Rclative Standard Deviation, MDL - Merhod Detection Limir, MCL - Maximum Concentration Limit., nd - not dctectcd.
J/ t6/01
l'agc t
s
A nalyst-/l(cvicwcr
:r EPA l\{ethod
Parameter
I
I
mdepom
Key Laboratories
2479 Rivcr Road, Urrit A
Grand Junction. Colorado 81502
Phone (970) 243-531 I Fax (970) 24-1-6010
UNOCAL
Dick Brammer
546 Main Sr. #404
Grand Junction. CO 8l -501
UOC Phone: 241-7632, Fax: 241-006-5
HLA Phone: 242-5184
EPA l\{ethod
Parameter
Metals
Lab Sample ID:
Client Sample ID
Client Proiect ID:
Date Sampled:
Date Received:
Date Reported:
Sample Matrix :
Presen,ation:
QAQC Number:
Pre-Treatuents/dig.
0r{ls3
uol{
UNOCAL TEMP 3
3/13/01
3/13/01 @ l7:00
3/16/01
SOLIDS
coc2208
TCLP EXTRACTION
3lt6t0r
3tr6/0t
Results RSD Units MDL Date MCL
6020
6020
TCLP Arsenic
TCLP Selenium
0.43
nd
0.06
0.06
0.6
nd
mglL
mg/L
Noles: RSD - Relative Standard Dcviation, MDL - Mcthod Dctection Limit, MCL - Maximum Concenration Limit., nd - nor dctected
J/ t6/01
l't,gc I
a
A na lyst/l{cv icwcr
ii
il
rl
t
t
;
MW
Key l-aboratories
2479 River Road. Unir A
Graud Junction. Colorado 81502
Phone (970) 24-1-5-11 I Fax (970) 243-6010
UNOCAL
Dick Branurrer
546 Main St. #404
Grand Junction, CO 81501
UOC Plrone: 241-7632. Fax: 241-0065
HLA Phone: 242-5784
Lab Sarrple ID:
Client Sample ID:
Clieut Project ID:
Date Sampled:
Date Received:
Date Reported:
Saurple Matrix :
Presen,ation:
QAQC Number:
Pre-Treatments/dig.:
0l-01s2
uor-3
UNOCAL TEI\{P 3
3/13/01
3/13/01 @ 17:00
3/16/0t
SOLIDS
coc2208
TCLP EXTRACTION
r EPA l\Iethod
Parameter
Metals
TCLP Arsenic
TCLP Selenium
0.7
3.2
mg/L
mg/L
Results RSD Units MDL Date MCL
6020
6020
0.42
0.07
0.06
0.06
3t16t0l
3lt6/0r
T
Notcs: RSD - Relative Standard Deviation,MDL - Method Dctecrion Limit, MCL - Maximum conccntration Limir., nd - not detected
3/ t6/0t
I'aiic I Analyst/ltc vic wcr
I
WW
Kcy Laboratories
2479 River Road, Unir A
Grand Junction. Colorado 81502
Phone (970) 243--53 I I Fax (970) 24-t-60 l0
TiNOCAL
Dick Branuner
546 Main Sr. #404
Grand Junction, CO 8l 501
UOC Phone: 241-7632, Fax: 241-0065
HLA Phone: 242-5784
Parameter
. :l -. r::: ::.=j j , -:::j :::j-.::--:
:
i,Units MDL Dare MCL li:
:r EPA Method
Results RSD
Latr Sample ID:
Client Sanrple ID:
Client Proiecr ID:
Date Sarrrpled:
f)ate Received:
Date Reported:
Sanrple Matrix :
Presen,ation:
QAQC Number:
Pre-
0l-0151
uol-2
IINOCAL TEI\{P 3
3/13/01
3/13/01 @ l7:00
3/16/01
SOLIDS
coc2208
TCLP EXTRACTION
3lt6t0r
3/t6/01
6020
6020
I\Ietals
TCLP Arsenic
TCLP Selenium
0.32
nd
1.5
nd
m-e/L
mglL
0.06
0.06
Notcs: RSD - Relarive Standard De*iation, MDL - Merhod Detecrion Limit, MCL -Maxrmum Concentration Limit., nd - nol detected.
1/ t6/0t
l'agc I
I
A rralyst/llcvicwcr
I
i : .:::.:_: ..j1. -_i :-: ..-j:::. r. .-_
STA|E OF COLORADO
Bill Owens, Covernor
Jane E. Norton, Executive Director
Dedicated to protecting and improving the health and environment of the people of Colorado
4300 Cherry Creek Dr. S. Laboratory and Radiation Services Division
Denver, Colorado 80246-1 530 8100 Lowry Blvd.
Phone (303) 692-2000 Denver, Colorado 80230-5928
TDD Line $03) 691-77oo (303) 692-3090
Located in Clendale, Colorado
http ://www. c d p h e. state. c o. u s
Colorado Department
of PublicHealth
andEnvironment
January 24,2002
Mr. Richard L. Brammer, Area Manager
Unocal Corporation
546 Main Street, #404
Grand Junction, Colorado 81501
RE: Closure Verification and Certification and Closure Approval of Temporary Basin 3 at the
Unocal Parachute Creek Upgrade Facility and Compliance Order #95-12-21-01 Close-out
Dear Mr. Brammer,
On December 17,2001, Kathryn Stewart and Joyce Williams, as hazardous waste inspectors for the
Colorado Department of Public Health and Environment, Hazardous Materials and Waste Management
Division (the Division), performed a closure verification inspection of Temporary Basin 3. At that time,
all closure activities for Temporary Basin 3 had been completed with the exception of revegetation.
Subsequent to the inspection, we have reviewed the Final Clean Closure Report for Temporary Basin 3
dated December 14, 1998. We have also received and reviewed the independent closure certification
from Harding ESE, as well as the closure certification from Unocal for this same basin.
After our inspection and review, which verified that Temporary Basin 3 had been backfilled, and graded,
and review of the aforementioned information submitted by Unocal, we hereby approve the clean
closure of Temporary Basin 3.
In a separate letter from Unocal dated December 12,2007, Unocal requested termination of Compliance
Order #95-12-21-01 and termination of ground water monitoring in the Holding Pond vicinity. In this
letter, Unocal stated that all work required by the Compliance Order has been successfully completed.
After reviewing the submitted information and information in our files, we concur with Unocal's request
and hereby close-out and terminate Compliance Order #95-12-21-01. In addition, we concw with
Unocal that ground water monitoring is no longer required around the soil repository in the vicinity of
the Holding Pond and can be terminated.
2r/l,
This brings to successful conclusion all hazardous waste activities and clean-up at the Unocal Parachute
Creek facilities. It has been a long effort. We very much appreciate your efforts and the efforts of your
staff over the years to accomplish these tasks. We also appreciate the workjng relationship we have
shared with you, your staff, and your contractors. If you have any questions please feel free to call me at
303-692-3356.
Sincerely,
Joe Schieffelin, Unit Leader
Hazardous Waste Compliance Unit
cc Walter Avramenko, CDPHE
Garfield County Department of Development
Lrnocal parachute
FaciIit"v/LrSO
e{H'ifi#i".x,r*:,ttr;:,;rr#j,rili'ii,'
PER/2.6. 1.1 ./6s
,,_,,,11!Jl I ll [ [ tt'ilttt"it tt tt
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0
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B
January 2023 Phase I
ESA
Phase I
Environmental Site
Assessment
Wheeler Gulch Solar LLC
Garfield County, Colorado
Prepared for
Caerus Operating LLC
January 27, 2023
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
TABLE OF CONTENTS
i
Table of Contents
Executive Summary ....................................................................................................................................... 1
1.0 Introduction ..................................................................................................................................... 5
1.1 Purpose ......................................................................................................................... 5
1.2 Report Users ................................................................................................................. 6
1.3 Scope of Services, Significant Assumptions, and Limitations ....................................... 6
2.0 Site Description ................................................................................................................................ 8
2.1 Location and Legal Description .................................................................................... 8
2.2 Site and Vicinity Characteristics ................................................................................... 8
2.3 Description of Structures, Roads, and Other Site Improvements ................................ 8
2.4 Area Geology and Hydrogeology .................................................................................. 9
3.0 User-Provided Information ............................................................................................................ 12
4.0 Records Review .............................................................................................................................. 13
4.1 Environmental Records Review .................................................................................. 13
4.2 Additional Regulatory Information ............................................................................ 15
5.0 Historical Use Information ............................................................................................................. 16
5.1 Fire Insurance Maps ................................................................................................... 16
5.2 City Directory .............................................................................................................. 16
5.3 Historical Aerial Photographs ..................................................................................... 16
5.4 Historical Topographic Maps ...................................................................................... 17
5.5 Environmental Liens, AULs, and Additional Information ........................................... 17
5.6 Summary of Previous Environmental Investigations ................................................. 18
6.0 Interviews ...................................................................................................................................... 19
6.1 Landowner Interview ................................................................................................. 19
7.0 Site Reconnaissance ....................................................................................................................... 20
7.1 Utilities and PCBs ........................................................................................................ 20
8.0 Data Gap Analysis .......................................................................................................................... 21
9.0 Findings, Opinions, and Conclusions .............................................................................................. 22
9.1 Findings ...................................................................................................................... 22
9.2 Opinions ..................................................................................................................... 24
9.3 Conclusions ................................................................................................................. 24
10.0 Recommendations ......................................................................................................................... 25
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
TABLE OF CONTENTS
ii
11.0 Qualifications of Environmental Professionals .............................................................................. 26
11.1 Signatures and Qualifications ..................................................................................... 26
12.0 References ..................................................................................................................................... 27
Tables:
Table 1. Property Identification Numbers .................................................................................................... 8
Table 2. Summary of Environmental Database Search Results .................................................................. 13
Table 3. Historical Aerial Summary ............................................................................................................. 16
Figures:
Figure 1. Project Location ........................................................................................................................... 10
Figure 2. Project Detail ................................................................................................................................ 11
Figure 3 Government Database Map .......................................................................................................... 14
Appendices
Appendix A – Governmental Database Search Results
Appendix B – Historical Sources
Appendix C – AUL and Environmental Lien Search
Appendix D – Site Photographs
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
ACRONYMS
iii
List of Acronyms
AAI All Appropriate Inquiry
AST aboveground storage tank
AUL activity and use limitation
AST aboveground storage tank
ASTM ASTM International
AUL Activity Use Limitations
BBL Barrel (bbl) is defined a non-SI Metric System Unit typically used to measure the volume of liquid
hydrocarbons
BGS below ground surface
CDPHE Colorado Department of Public Health and Environment
CERCLA Comprehensive Environmental Response, Compensation, and Liability Act
COGCC Colorado Oil and Gas Conservation Commission
CORRACTS Lists of Federal RCRA facilities undergoing Corrective Action.
CREC controlled recognized environmental condition
EPA Environmental Protection Agency
ESA Environmental Site Assessment
HREC historical recognized environmental condition
LTANKS Active and Closed OPS Petroleum Release Events in Colorado.
LUST Leaking Underground Storage Tank
NFA No Further Action
NPL National Priorities List
NPMS National Pipeline Mapping System
RCRA Resource Conservation Recovery Act
REC recognized environmental condition
USGS United States Geological Survey
U.S.C. United States Code
UST underground storage tank
VOC volatile organic compound
Note: A more complete acronym list is in the Governmental Database Report, Appendix A.
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
EXECUTIVE SUMMARY
1
Executive Summary
HDR Engineering, Inc. (HDR) has completed a Phase I Environmental Site Assessment (Phase I ESA) of an
88-acre parcel located in Garfield County, Colorado. The parcel is the proposed site for a 10 megawatt
(MW) solar energy system referred to as the Wheeler Gulch Solar Project. Caerus Oil and Gas LLC (“User”),
current owner of the property for the proposed Wheeler Gulch Solar Project, has requested a Phase I ESA
for permitting support to develop the Wheeler Gulch Solar Project.
The property, referenced herein as the “Subject Property,” is an irregularly shaped lot (Parcel
Identification Number [PIN] 217133100020). The Subject Property is bound by American Soda LLP, a soda
ash manufacturing facility to the southeast and the Parachute Creek Natural Gas Plant to the northwest.
Parachute Creek runs through the southern portion of the Subject Property, and County Road 215 runs
through the northeast portion. The surrounding property land use consists of industrial facilities, open
rangeland, and oil and gas infrastructure. Figures 1 and 2 provide further detail regarding the boundaries
of the Subject Property.
The purpose of this Phase I ESA is to identify Recognized Environmental Conditions (RECs) that may
adversely affect the Subject Property. This Phase I ESA was conducted in accordance with the scope and
limitations of ASTM International (ASTM) Standard Practice E1527-21. This report includes a summary of
the site reconnaissance conducted on October 18, 2022, landowner interview, a review of environmental
databases, and a review of historical data sources. Any exceptions to or deletions from these ASTM
practices are described later in this report.
Findings
General findings of this assessment include the following:
• The Subject Property is situated on the western flank of the Colorado Rocky Mountains within a
river eroded basin. The local geology consists of Fluvial Deposits overlain by unconsolidated
alluvial materials. The surficial geology of the Subject Property consists of deposits from the
Wasatch Formation as well as the presence of deposits from intermountain lakes and related
deposits of marlstone. Bedrock thickness at the Subject Property is approximately 1500 feet and
soil at the site (Halaquepts) is classified as a clay loam with a very slow infiltration rate and is
considered poorly drained.
• Groundwater elevation data is not available for the Subject Property. However, nearby subsurface
investigations indicated that the depth to water is shallow (approximately 40 feet below ground
surface) and the groundwater flow direction is estimated to be southeastern toward Parachute
Creek. The computerized environmental database search conducted by EDR identified 13
monitoring wells at depths ranging from 35 to 55 feet within the Subject Property. Three out of
the ten wells were abandoned. Fifty well records were identified within 1-mile.
• The environmental database search conducted by EDR revealed no listings for the Subject
Property and three listings within the ASTM-designated search buffer (up to 1-mile). One orphan
site was also found in the search. The following listings of potential concern were identified within
the search buffer:
o UNOCAL CORP (2717 GARFIELD CR 215, MAP ID 1). This property is located 0.46 miles
downgradient of the Subject Property.
LTANKS/LUST– Records were found for a release on 5/10/1994. Limited details
on the tank contents or capacity were provided. A No Further Action (NFA) letter
was issued on 8/18/1994.
UST – One 4,018-gallon diesel underground storage tank (UST) and one 4,018-
gallon gasoline UST were reported as permanently closed on 12/31/1993.
o UNOCAL SHALE OIL FACILITY (2717 CNTY RD 215, MAP ID 2). This property is located 0.5
miles upgradient of the Subject Property.
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
EXECUTIVE SUMMARY
2
CORRACTS – This property was ranked as a medium corrective action (CA) priority
facility in 1993. An investigation began in 1995 to due to groundwater
contamination at active/inactive holding ponds, presence of oil in sewer water
upstream of the API Separator and a need to upgrade the drum storage area. The
investigation workplan was approved in 1997, remediation construction began in
2000 were complete as of 4/17/2000. This property was deferred to Resource
Conservation and Recovery (RCRA) Subtitle C for storage of benzene and was not
listed on the National Priorities List (NPL).
• A review of historical aerials, topographic maps, and other information concluded that the Subject
Property had historically been vacant up the late 1970s, early 1980s when two holding ponds and
associated infrastructure, referred to as the Holding Pond and East Holding Pond, were used to
support adjacent industrial facilities.
o The Holding Pond was constructed in 1983 and closed in 1993. Arsenic contaminated soils
exceeding natural background standards were identified. These soils were excavated and
placed in an on-site repository north of the main holding pond. HDR was unable to locate
the Closure Plan and associated regulatory approval documents.
o The East Holding Pond was present in the 1993 historic aerial and was undergoing closure
in the 1999 historic aerial. HDR was unable to locate documentation to identify the type
of liquids managed in the East Holding Pond or any regulatory documentation supporting
its closure.
• A review of historical aerials and topographic maps identified gas and oil infrastructure have been
present within the Subject Property, in the northwest and southeast corners, beginning in 2006.
• An AUL, in the form of a Deed Restriction and Notification executed in November 1998, was
identified on the site for the parcel where the soil repository containing arsenic contaminated
soils is located. The Deed Restriction and Notification limits uses of the repository parcel and
requires Colorado Department of Public Health and the Environment (CDPHE) notification before
any modification or disturbance to the repository commences.
• No lease documents or other contractual agreements were identified between the current
Landowner and the Leasee(s) for the two oil/gas well pads. A Landowner Questionnaire was
completed on December 5, 2022, by Mr. Jason Eckman, the Regulatory and Community Relations
Lead for the current landowner, Caerus Oil and Gas LLC. Mr. Eckman stated that the property has
been owned by Caerus Oil and Gas LLC for five years. Mr. Eckman sated the prior owners of the
Subject Property used it to support oil shale development. He was aware of two producing oil/gas
wells owned by Terra Energy Partners in the northwest and southeast portion of the Subject
Property and a soil repository parcel containing excavated soil contaminated with arsenic from a
holding pond in the northwest portion of the Subject Property. Mr. Eckman stated that the soil
repository and two producing oil/gas well pads are excluded from the Wheeler Gulch Solar
Project.
• HDR conducted the site reconnaissance on October 18, 2022. The Subject Property is a primarily
vacant, undeveloped parcel with mostly short herbaceous plants and some trees surrounding the
location of a former holding pond and near the banks of Parachute Creek. A barbed wire fence
was present around the majority of the Subject Property. Agricultural fields were present in the
northeast portion of the Subject Property, northeast of Highway 215. Trash was present in the
southwestern edge of the Subject Property including an old automobile, debris from a wooden
structure, and scrap metal. A well-maintained access road was present in the south-central area
of the Subject Property which led to an unfenced equipment storage yard containing a small shed
and conex box, as well as generators, trailers, and other construction equipment. Other small
areas of the property appeared to be leased to oil and gas businesses including some buildings on
the southeast corner of the property and an access road on the eastern side of the property.
• High voltage power lines transect the eastern portion of the Subject Property from north to south,
crossing over the access road to the equipment yard. Abandoned power infrastructure is
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
EXECUTIVE SUMMARY
3
scattered through the western portion of the parcel with some active infrastructure at the very
western edge.
Opinions
HDR has reviewed the stated data sources, which are part of the ASTM E1527-21 assessment protocol.
Based upon the review of the data, HDR has developed the following professional opinions:
• An equipment storage yard is present in the southern portion of the Subject Property. The
equipment storage yard contains a small shed and conex box, as well as generators, trailers, and
other construction equipment. Petroleum products for the generators may exist on site, but not
likely in significant quantities. This site is not considered to be a REC.
• A Holding Pond and settling ponds/aeration basins were located on the northeast Subject
Property from 1981 to 1993. The holding pond was taken out of service in November 1993 and
soils in the bottom of the holding pond were tested and shown to exceed the natural background
arsenic levels. Soils exceeding a CDPHE established performance standard were excavated and
placed in a soil repository parcel created out of the former aeration/settling basins immediately
north of the holding pond. HDR was unable to locate the Closure Plan and associated regulatory
approval documents. The soil repository is subject to a AUL that references the closure documents
with CDPHE in the form of a November 1998 Deed Restriction and Notification. Based on this
analysis, the soil repository parcel is considered a CREC and the footprint of the former holding
pond is considered a REC.
• The larger East Holding Pond was present in the 1993 historic aerial and remained on site in 1999,
undergoing closure, after the adjacent Holding Pond facility had been closed. HDR was unable to
locate documentation to identify the type of liquids managed in the East Holding Pond or any
regulatory documentation supporting its closure. The East Holding Pond is considered a REC.
• Oil and gas production in the northwest and southeast corners of the Subject Property has been
present since at least the early 2000s. The lease agreements for the two oil/gas well pads were
not available. No information was found regarding historical releases; however, a lack of an
agreement between the two parties opens up the User to liability should a release occur. The
oil/gas well pads are considered a business environmental risk due to a lack of documented
agreement between the User and the leasing party.
Conclusions
Based upon the above-detailed Findings and Opinions, HDR concludes that RECs have not been identified
in association with the Wheeler Gulch Solar Project, as summarized in the Opinions section above. The
following statement is required by ASTM E1527-21 as a declaration that RECs were found:
HDR has performed a Phase I ESA in conformance with the scope and limitations of ASTM E1527-21 of
the proposed Wheeler Gulch Solar Project located at 3477 County Road 215 Parachute, CO 81652. Any
exceptions to or deletions from these practices are described in following sections of this report. This
report has revealed no indications of RECs in connection with the Subject Property.
Recommendations
Recommendations included in this report were developed through the investigative procedures described
in the Scope of Services, Significant Assumptions, and Limitations sections of this report (See Section 2.3).
These findings should be reviewed within the context of the limitations provided in the Limitations
section.
Based upon the identification of RECs in the Subject Property, HDR makes the following
recommendations:
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
EXECUTIVE SUMMARY
4
Recommendation 1
HDR recommends a Phase II evaluation for soils in the footprint of the former Holding Pond and East
Holding Pond focused on areas where disturbance is anticipated. The evaluation will potentially
hazardous waste impacts and inform soil management needs during construction.
Recommendation 2
HDR recommends that the Wheeler Gulch Solar Project avoid construction in the location of the
arsenic soil repository and the operating oil and gas pads identified in Figure 2. If construction is
anticipated in the location of the arsenic soil repository, per the Deed Restriction and Notification, the
User must notify CDPHE before construction commences.
Recommendation 3
HDR recommends that the User complete and maintain lease agreements (or other appropriate legal
mechanism) with the operator(s) of the oil and gas pads to determine environmental liability should
a release occur due to Leasee operations.
Recommendation 4
HDR recommends that the User consider the “shelf life” of Phase I documents in determining risk.
ASTM E 1527-21 states that a conforming “Phase I” report is valid for a period of 180 days and may
be updated during the 180 days to 1-year timeframe. The report is valid for use in any of the CERCLA
defenses ONLY if it is updated within this time frame. If greater than one year passes from the final
report date, the Phase I effort would need to be repeated to remain in compliance with ASTM and
the “All Appropriate Inquiry” protections.
Report Viability Dates
Phase I ESA Component Date Collected
Database Search October 13, 2022
Interview(s) December 5, 2022
Site Reconnaissance October 18, 2022
Environmental Professional Declaration Report Date
AUL and Environmental Lien Search December 5, 2022
Report Expiration
*calculated from earliest collection date
April 11, 2023
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
INTRODUCTION
5
1.0 Introduction
1.1 Purpose
The purpose of this Phase I ESA is to document the evaluation of the Subject Property for indications of
“recognized environmental conditions,” as defined by ASTM International Practice E1527-21. This ASTM
standard defines the following categories of REC:
REC:
(1) The presence of hazardous substances or petroleum products in, on, or at the Subject Property due to
a release to the environment; (2) the likely presence of hazardous substances or petroleum products in,
on, or at the Subject Property due to a release or likely release to the environment; or (3) the presence of
hazardous substances or petroleum products in, on, or at the Subject Property under conditions that pose
a material threat of a future release to the environment.
ASTM E1527-21 defines release as a release of any hazardous substance or petroleum product shall have
the same meaning as the definition of “release” in CERCLA 42 U.S.C. § 9601(22). There are a number of
statutory exclusions from the definition of release that may impact the environmental professional’s
opinions and conclusions, such as the normal application of fertilizer.
Controlled REC (CREC):
A recognized environmental condition affecting the Subject Property that has been addressed to the
satisfaction of the applicable regulatory authority or authorities with hazardous substances or petroleum
products allowed to remain in place subject to implementation of required controls (for example, activity
and use limitations or other property use limitations).
Additional conditions that are not included under the definitions of a REC, but are defined by ASTM
Practice E1527-21 include:
Historical REC (HREC):
A previous release of hazardous substances or petroleum products affecting the Subject Property that has
been addressed to the satisfaction of the applicable regulatory authority or authorities and meeting
unrestricted use criteria established by the applicable regulatory authority or authorities without
subjecting the Subject Property to any controls (for example, activity and use limitations or other property
use limitations). A historical recognized environmental condition is not a recognized environmental
condition.
De minimis:
A condition that generally does not present a threat to human health or the environment, and that
generally would not be the subject of an enforcement action if brought to the attention of appropriate
governmental agencies. Conditions determined to be de minimis conditions are not RECs, historical RECs
nor CRECs.
Business Environmental Risk:
A risk which can have a material, environmental or environmentally-driven impact on the business
associated with the current or planned use of a parcel of commercial real estate, not necessarily limited
to those environmental issues required to be investigated in this practice.
Consideration of business environmental risk issues may involve addressing one or more non-scope
considerations.
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INTRODUCTION
6
1.2 Report Users
HDR received authorization from Caerus Oil and Gas LLC (User) to conduct a Phase I ESA of the Subject
Property. The Subject Property is the proposed site for the Wheeler Gulch Solar Project (specific project
limits are shown in Figures 1 and 2), located in Parachute, Garfield County, Colorado. This Phase I ESA has
been prepared for Caerus Oil and Gas LLC, and only Caerus Oil and Gas LLC has the right to rely on the
contents of this Phase I ESA without written authorization.
1.3 Scope of Services, Significant Assumptions, and
Limitations
The services provided for this project consisted of the following:
• Provide a description of the Subject Property including current land uses (Section 2.2 and 2.3)
• Provide a general description of the topography, soils, geology, and groundwater flow direction
(Section 2.4)
• Review reasonably ascertainable and reviewable regulatory information published by federal,
state, local, tribal, health, and/or environmental agencies pertaining to the Subject Property
(Section 4.0)
• Review historical data sources for the Subject Property, including aerial photographs, topographic
maps, fire insurance maps, city directories, and other readily available development data (Section
5.0)
• Interview current owner of the Subject Property and interview other persons with knowledge of
the development history of the Subject Property (Section 6.0)
• Conduct an area reconnaissance and an environmental review—including a visual review of
adjoining properties—with a focus on indications of hazardous substances, petroleum products,
polychlorinated biphenyls (PCBs), wells, storage tanks, solid waste disposal pits and sumps, and
utilities (Section 7.0)
• Determine data gaps in the information obtained and comment on their significance in identifying
RECs for the Subject Property (Section 8.0)
• Prepare a written report of methods, findings, opinions, and conclusions (Section 9.0).
The goal of this scope of services is to assist the user in identifying conditions in the Subject Property that
may indicate risks regarding hazardous materials storage, disposal, or other impacts. The resulting report
may qualify the user for relief from liabilities as one of three “defenses” identified in the 2002 Brownfields
Amendments to the CERCLA Section 9607 (All Appropriate Inquiry subsections). These three defenses
include:
1. The “innocent landowner” defense to potential liabilities under 42 United States Code [U.S.C.] § 9601
2. The “contiguous project corridor owner” defense pursuant to 42 U.S.C. § 9607q
3. The “bona fide prospective purchaser” defense pursuant to 42 U.S.C. §9607r
Federal regulations at (42 U.S.C §9601(35)(A) & (B), §9607(b)(3), §9607(q), and §9607(r)), promulgated by
the United States (U.S.) Environmental Protection Agency (EPA), require that liability release be based (in
part) on completion of All Appropriate Inquiries (AAI) prior to purchase of a property. Those inquiries are
documented by Phase I reports, or ESAs. EPA has agreed that the recently developed ASTM guidance
(ASTM Practice E1527-21: 3.2.6) specifies and interprets AAI requirements.
A user is defined by ASTM Practice E1527-21 as the party seeking to use Practice E1527 to complete an
ESA of the Subject Property and may include a potential purchaser of land in the Subject Property, a
potential tenant of the Subject Property, an owner of land in the Subject Property, a lender, or a project
manager. Investigative areas not included in the standard ASTM ESA scope include asbestos, lead-based
paint, lead in drinking water, radon or urea formaldehyde, wetland issues, regulatory compliance, cultural
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
INTRODUCTION
7
and historic resources, industrial hygiene, health and safety, ecological resources, endangered species,
and high voltage power lines.
Indoor air quality from sources such as mold and asbestos are not included in the ASTM standard, except
to the extent that indoor air impacts are caused by releases of hazardous substances into subsurface soil
or groundwater (vapor intrusion).
The potential for vapor encroachment or intrusion into structures in the Subject Property is considered
and identified from onsite or offsite sources based on the experience of the Environmental Professional.
The scope of services for ESA projects also does not include the completion of soil borings, the installation
of groundwater monitoring wells, or the collection of soil or groundwater samples. State and national
policies and standards relevant to vapor intrusion are in flux and subject to change.
HDR has made certain assumptions in preparing the scope of this assessment:
• Data gathered from public information sources (e.g., libraries or public regulatory agencies) are
accurate and reliable.
• Site operations reflect site conditions relative to potential releases, and no intentional
concealment of environmental conditions or releases has occurred.
• Interview information is directly reported as gathered by the assessor and is limited by the
accuracy of the interviewee’s recollection and experience.
• Published geologic information and site observations made by the environmental professional are
used to estimate likely contaminant migration pathways in the subsurface. These estimates by
the environmental professional are limited in accuracy and are generally cross-referenced with
existing information about similar sites and environmental releases in the area.
• Regulatory information is limited to sites identified after the late 1980s, because reliable records
were not kept by regulatory agencies prior to that time frame.
The findings and conclusions presented in this report are based on the procedures described in ASTM
Practice E1527-21, informal discussions with various agencies, a review of the available literature cited in
this report, conditions noted at the time of this Phase I ESA, and HDR’s interpretation of the information
obtained as part of this Phase I ESA. The findings and conclusions are limited to the specific project and
properties described in this report, and by the accuracy and completeness of the information provided by
others.
An ESA cannot entirely eliminate uncertainty regarding the potential for RECs. Conducting this assessment
is intended to reduce, but not eliminate, uncertainty regarding the potential for RECs in connection with
a Subject Property within reasonable limits of time and cost. In conducting its services, HDR used a degree
of care and skill ordinarily exercised under similar circumstances by reputable members of its profession
practicing in the same locality. This Phase I ESA conforms to the level of documentation required in ASTM
Practice E1527-21. However, HDR may omit discussion of certain records, i.e., sources deemed, in HDR’s
professional opinion, to be inapplicable, or of limited value, to the specific needs of this client. In
accordance with ASTM, however, if the lack of available documentation results in a data gap, this data
gap is identified herein, and its significance is discussed.
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SITE DESCRIPTION
8
2.0 Site Description
2.1 Location and Legal Description
The property, referenced herein as the Subject Property, is the proposed location for the Wheeler Gulch
Solar Project. The Subject Property is an irregularly shaped lot, approximately 88 acres in area, located at
the addresses listed in Table 1 below, in the town of Parachute, Garfield County, Colorado.
Table 1. Property Identification Numbers
PIN Address Land Use Lot Size
(acres)
Listed Owner
217133100020 3477 County Road 215
Parachute, CO 81652
Agricultural/Rural 88 acres Caerus Operating LLC
The Subject Property is bound by American Soda LLP, a sodium carbonate and sodium bicarbonate
manufacturer to the southeast and Parachute Creek Natural Gas Plant to the northwest. Parachute Creek
runs through the southern portion of the Subject Property, and County Road 215 runs through the
northeast portion.
Please refer to the Project Location and Project Detail Maps (Figures 1 and 2, respectively) for further
details regarding project limits and location.
2.2 Site and Vicinity Characteristics
The Subject Property lies within the southern half of Garfield County, in the town of Parachute, Colorado.
The surrounding property land use consists of industrial facilities, open rangeland, and oil and gas
infrastructure.
According to the United States Geological Survey (USGS) 7.5-minute topographic map for Parachute,
Colorado, the Subject Property lies within a creek bed and pitches south/southwest towards Parachute
Creek. The elevation ranges from 5540 (ft) above mean sea level (amsl) in the northeast corner, to 5370
amsl in the southern portion of the Subject Property. Mountain ranges are located to the northeast and
southwest of the Subject Property.
2.3 Description of Structures, Roads, and Other Site
Improvements
Two (2) high-pressure natural gas pipelines parallel the south side of County Road 215 and run through
the northeast corner of the Subject Property. A third high-pressure natural gas pipeline was located 300
feet from the western boundary of the Subject Property (NPMS 2022). American Soda LLP, a soda ash
manufacturing facility is located adjacent to the east boundary of the Subject Property. The Parachute
Creek Natural Gas Plant is located adjacent to the northwest portion of the Subject Property.
Thirteen (13) water wells are present within the Subject Property and are described further in section
2.4.2. Two (2) producing oil/gas wells are located in the northwest and southeast corner of the Subject
Property. A soil repository cell containing arsenic contaminated soils from a former holding pond is located
in the northwest portion of the Subject Property. An access road is present in the south-central area of
the Subject Property leading to an unfenced equipment storage yard. Parachute Creek runs through the
southern portion of the Subject Property and joins the Colorado River three miles to the southeast. County
Road 215 and Garden Gulch Road run through the northeast corner of the Subject Property. Several
transmission and distributions lines traverse the eastern portion of the Subject Property. Abandoned
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SITE DESCRIPTION
9
power infrastructure is scattered through the western portion of the Subject Property with some active
infrastructure along the western edge.
2.4 Area Geology and Hydrogeology
2.4.1 Geology
The Subject Property is situated on the western flank of the Colorado Rocky Mountains. The local geology
consists of Fluvial Deposits overlain by unconsolidated alluvial materials. The Subject Property lies within
a river eroded basin. The surficial geology of the Subject Property consists of deposits from the Wasatch
Formation, which are classified as fluvial deposits of claystone, sandstone, and conglomerate covered by
unconsolidated gravels and alluviums. Deposits from intermountain lakes and related deposits of
marlstone and shale are also present in the area (Tweto 1979). The underlying bedrock is the Wasatch
Formation which the Molina and Atwell Gulch Members. Bedrock thickness at the Subject Property is
approximately 1500ft (Donnell 1986). Soil at the site (Halaquepts) is classified as a clay loam with a very
slow infiltration rate and is considered poorly drained (NCSS 2022).
2.4.2 Groundwater and Well Information
According to the Colorado State Geological Survey, the underlying fluvial deposits and Wasatch formation
bedrock are not considered major drinking water aquifers in the area. Higher yields are typically found in
the deeply buried Mississippian Leadville Limestone.
Groundwater elevation data is not available for the Subject Property. However, nearby subsurface
investigations indicated that the depth to water is shallow (approximately 40 feet below ground surface)
and the groundwater flow direction is estimated to be southeastern toward Parachute Creek.
The well search conducted by EDR identified ten monitoring wells depths ranging from 35 to 55 feet and
three abandoned monitoring wells within the Subject Property boundaries. Fifty well records were
identified within 1-mile of the Subject Area.
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SITE DESCRIPTION
10
Figure 1. Project Location
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
11
O overview
Figure 2. Project Detail
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
USER-PROVIDED INFORMATION
12
3.0 User-Provided Information
Mr. Jason Eckman, on behalf of the User, Caerus Oil and Gas LLC, responded to requests for information
on the Subject Property on December 5, 2022, and December 31, 2022. The User of the report stated:
• The User found no identification of any environmental against the Subject Property based on the
title commitments.
• The User has knowledge of an environmental cleanup that occurred on the Subject Property
described below:
• One holding pond and aeration/settling basins were located on the Subject Property from
1987 to 1993. The holding pond was taken out of service in November 1993, and soils in the
bottom of the pond were tested and shown to exceed the arsenic background levels. Soils
exceeding the CDPHE-approved performance standard were excavated and placed in a soil
repository parcel created out of the former aeration/settling basins immediately north of the
holding pond. The CDPHE granted closure of the soil repository parcel in 1998. The parcel
containing the repository will be excluded from the Wheeler Gulch Solar Project.
• The User provided HDR with a Deed Restriction and Notification, dated November 1998, for the
soil repository discussed above.
• The User has specialized knowledge related to the Subject Property summarized below:
• Two (2) privately owned producing oil/gas wells are located on the northwest and southeast
areas of the Subject Property and will be excluded from the Wheeler Gulch Solar Project.
• The User was unable to locate any lease or contractual agreements between the Landowner and
the oil/gas pad Leasee(s).
• Other than the arsenic-contaminated soils contained in the on-site repository discussed in the
previous bullet, the User has no knowledge of the presence of contamination on the Subject
Property.
• The User has no knowledge of any spills or chemical releases on the Subject Property
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
RECORDS REVIEW
13
4.0 Records Review
4.1 Environmental Records Review
EDR was contracted by HDR to complete a database search of federal, state, local, and tribal
environmental records (as required by ASTM) for the Subject Property. A computerized environmental
information database search was performed for the Subject Property by EDR on October 13, 2022. The
databases searched included federal, state, local, tribal, and EDR proprietary databases for listings within
the Subject Property, and a one-mile search buffer zone. The results of the Governmental database search
are summarized in the following paragraphs. A complete copy of the Governmental database report and
detailed map is included in Appendix A.
Table 2. Summary of Environmental Database Search Results
Database Description Subject
Property
ASTM
Search
Radius
Standard Environmental Records
CORRACTS Lists of Federal RCRA facilities undergoing Corrective Action. 0 1
LTANKS Active and Closed OPS Petroleum Release Events in Colorado. 0 1
LUST The Leaking Underground Storage Tank Incident Reports contain an inventory of
reported leaking underground storage tank incidents.
0 1
TOTAL 0 3
Orphan Sites 1
The database search revealed no listings for the Subject Property and three listings within the ASTM-
designated search buffer (up to 1-mile). One orphan site was also found in the search, but further
investigation showed it was located over one-mile from the Subject Property. Figure 3 shows the Subject
Property and search buffer used by EDR for the database search.
Search Buffer Sites of Concern
• UNOCAL CORP (2717 GARFIELD CR 215, MAP ID 1). This property is located 0.46 miles
downgradient of the Subject Property.
o LTANKS/LUST– Records were found for a release on 5/10/1994. Limited details on the
tank contents or capacity were provided. A NFA letter was issued on 8/18/1994.
o UST – One 4,018-gallon diesel UST and one 4,018-gallon gasoline UST were reported
as permanently closed on 12/31/1993.
• UNOCAL SHALE OIL FACILITY (2717 CNTY RD 215, MAP ID 2). This property is located 0.5 miles
upgradient of the Subject Property.
o CORRACTS – This property was ranked as a medium CA priority facility in 1993. An
investigation began in 1995 to due to groundwater contamination at active/inactive
basins, presence of oil in sewer water upstream of the API Separator and a need to
upgrade the drum storage area. The investigation workplan was approved in 1997,
remediation construction began in 2000 and the corrective action was terminated,
and remedial activities were complete as of 4/17/2000. This property was deferred
to RCRA Subtitle C for storage of benzene and was not listed on the NPL.
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14
Figure 3 Government Database Map
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
RECORDS REVIEW
15
4.2 Additional Regulatory Information
4.2.1 Online Sources
COLORADO DEPARMTENT OF NATURAL RESOURCES
Colorado Oil and Gas Conservation Commission (COGCC)
A search for well records for the Subject Property and adjacent properties was conducted. No new listings
in addition to those in the EDR database report were found.
COLORADO PIPELINE AWARENESS
National Pipeline Mapping System (NPMS)
A search for gas and oil pipelines within the vicinity of the Subject Property and adjacent properties was
conducted. The following information was collected:
• Two high-pressure natural gas pipelines are located parallel to the south side of County Road 214,
which runs through the northwest corner of the Subject Property. A second high-pressure natural
gas pipeline was located 300 feet south of the Subject Property.
• One hazardous liquid pipeline was located 500 feet west of the Subject Property. A release of 3.60
BBLs of flammable/toxic fluid occurred on 5/14/2020 as a result of equipment failure. 1.60 BBL
were recovered. The area where the release occurred was on a concrete pad, adjacent to the east
side of four ASTs, and surrounded by a soil berm. No records of the release flowing outside of the
bermed area was reported.
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Cleanups In My Community
A search for cleanup sites was conducted for the Subject Property and surrounding properties. No new
listings in addition to those in the EDR database report were found.
4.2.2 Agency File Reviews
No FOIA requests were made for listings identified in Section 4.1, due to: 1) the detailed information
already provided in the EDR report, 2) the availability of additional information online (i.e., COGCC, NPMS),
or 3) the relevant records being unavailable through this process.
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HISTORICAL USE INFORMATION
16
5.0 Historical Use Information
The objective of reviewing historical use information is to develop a history of previous land uses at, and
in the vicinity of, the Subject Property, and to assess these uses for potential hazardous materials impacts
that may affect the Subject Property. HDR reviewed those historical sources that were reasonably
ascertainable and likely to provide useful information, as defined by the ASTM standard.
5.1 Fire Insurance Maps
Fire insurance maps are produced by private fire insurance companies to indicate uses of properties within
the Subject Property, originally to develop fire ratings for insurance companies. Sanborn fire insurance
map coverage for the Subject Property was not available.
5.2 City Directory
Historical City Directories were reviewed back to 1995 for the Subject Property address. No business has
been listed at the Subject Property address (3477 County Road 215). The earliest record of a business
adjacent to the Subject Property occurred in 1992. Additional coverage years included 1995, 2000, 2005,
2010, 2014 and 2017.
The following were businesses adjacent to the Subject Property:
• 3696 County Road 215 – Unocal Ranch (1992, 1995)
• 4289 County Road 215
o 2000: Haystack Ranch/Parachute Creek Ranch
o 2014: Williams Companies/ Williams Production P3 Gas Plant
o 2017: Terra Energy Partners/ Williams Companies/ Williams Production P3 Gas Plant
• 3555 County Road 215 – Williams Production RMT /National Oilwell Varco (2005, 2014, 2017)
• 2717 County Road 215
o 1992: Texaco Trucking/Union Oil of California
o 2000: Kvaerner Metals
o 2005: America Soda Ash/Solvay Chemicals Inc
o 2010: En Cana Oil & Gas USA Inc/Solvay Chemicals Inc
o 2017: Solvay Chemicals Inc
5.3 Historical Aerial Photographs
Historical aerial photographs are valuable for the environmental assessor to review features of the Subject
Property and surrounding properties over a long period of time. HDR reviewed historical aerial
photographs for the following years: 1945, 1955, 1960, 1979, 1983, 1993, 1999, 2006, 2009, 2017, and
2021. Copies of the historical aerial photographs are included in Appendix B.
Table 3. Historical Aerial Summary
Year Source Notable Feature or Change
1949 EDR The Subject Property was undeveloped. What appears to be a tree farm was located in
the southeast corner. Several gravel roads were present in the western half of the
Subject Property. County Road 215 and Garden Gulch Road were present in the
northeast corner. A farmstead was present adjacent to the northeast corner of the
Subject Property, east of Garden Gulch Road. Surrounding properties consisted of rural
residential and agricultural land.
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HISTORICAL USE INFORMATION
17
1955
and
1960
EDR The 1955 aerial image is incorrectly shifted south, but there were no significant
changes to the Subject Property or adjacent properties.
1979 EDR The aerial image was not clear enough to observe any notable features or changes
within the Subject Property.
1983 EDR The aerial image is incorrectly shifted north. A holding pond facility was present in the
northern portion of the Subject Property by 1983 which included a main holding pond
and three aeration/settling basins. Four buildings were present southeast of the
Subject Property. Industrial development was present to the southeast.
1993 EDR A large holding pond was present east of the existing holding pond facility in 1993. The
surrounding properties remained in industrial land use.
1999 EDR By 1999, only the large east holding pond was present within the Subject Property.
2006 EDR By 2006, the large east holding pond had been partially filled in. The rectangularly-
shaped soil repository is slightly visible in the west central portion of the Subject
Property in the footprint of the former aeration/settling basins. One oil/gas well pad
was present in the northwest corner and one well pad was present in the southeast
portion of the Subject Property. Industrial and oil and gas infrastructure including
holding ponds, ASTs, oil/gas well pads and warehouses were present adjacent to the
northwest and southeast boundary of the Subject Property by 2006.
2009 EDR By 2009, the well pad adjacent to the north boundary of the Subject Property had
expanded in size. Three ASTs and four generators were clearly visible in the southeast
corner of the Subject Property.
2017 EDR No significant changes within the Subject Property.
2021 Google Earth By 2021, what appears to be machinery and storage containers are stored in the
southern portion of the Subject Property.
5.4 Historical Topographic Maps
Historical topographic maps provide an overview of the area relative to potential previous land uses. HDR
reviewed USGS 7.5-minute historical topographic maps of the Subject Property provided by EDR. The
USGS 7.5-minute series topographic maps were reviewed for Parachute, Red Pinnacle, and Grand Valley
for 1962, and Parachute, Red Pinnacle, Forked Gulch and Circle Dot Gulch for the years 2013, 2016 and
2019. These maps served to augment information that was gathered in the historic aerial photograph
review.
A review of the topographic maps concluded that the Subject Property had historically been vacant up
the late 1970s/early 1980s when holding ponds used to support adjacent industrial facilities, and gas and
oil infrastructure were present within the Subject Property.
Copies of the historical topographic maps are included in Appendix B.
5.5 Environmental Liens, AULs, and Additional Information
The User indicated that no Environmental Liens were found for the Subject Property.
An AUL, in the form of a Deed Restriction and Notification, is present on the Subject Property for the
parcel where the soil repository containing arsenic contaminated soils is located. The deed restriction was
executed in November 1998 by Unocal, the owner of the real property at the time. The deed restriction
provided a brief summary of the construction and closure of Unocal’s Construction Camp Holding Pond in
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
HISTORICAL USE INFORMATION
18
the northwest corner of the Subject Property. The Holding Pond, constructed in 1981, was originally
designed for use as a polishing basin for a sewage treatment system but in 1987, Unocal was given
permission by CDPHE to store treated process water in the Holding Pond until 1993 when it was taken out
of service. Arsenic was present in the holding pond above background and 12,000 cubic yards of soil were
excavated and consolidated in an on-site soil repository located in the footprint of the aeration/settling
ponds. Refer to Figure 2 for the location of the soil repository and the former Holding Pond.
The deed restriction and notice (Appendix C) limits uses of the repository as follows:
“future use of the land contained in the Parcel must not disturb the soil repository controls
implemented by Unocal. The controls are the graded and compressed cap and liner. Any future
owner of the Parcel must notify CDPHE before any modification or disturbance to the existing
control commences”
5.6 Summary of Previous Environmental Investigations
The deed restriction and notice discussed in Section 5.5 described an investigation and closure plan for
the former holding pond facility. HDR was unable to locate these reports to summarize the investigations.
HDR was unaware of any other previous environmental investigations on the Subject Property at the time
of this report.
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INTERVIEWS
19
6.0 Interviews
6.1 Landowner Interview
A Landowner Questionnaire was completed on December 5, 2022, by Mr. Jason Eckman, the Regulatory
and Community Relations Lead for the current landowner, Caerus Operating LLC, who stated that the
property has been owned by Caerus Operating LLC for five years. Mr. Eckman sated the prior owners of
the Subject Property used it to support oil shale development. He was aware of two producing oil/gas
wells owned by Terra Energy Partners in the northwest and southeast portion of the Subject Property and
a soil repository containing excavated soil contaminated with arsenic from a holding pond in the
northwest portion of the Subject Property. Mr. Eckman stated that the soil repository and two producing
oil/gas well pads were excluded from the Wheeler Gulch Solar Project.
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
SITE RECONNAISSANCE
20
7.0 Site Reconnaissance
HDR conducted the site reconnaissance on October 18, 2022. The site reconnaissance activities included
a review of the Subject Property and surrounding area.
The Subject Property was primarily vacant, undeveloped parcel with mostly short herbaceous plants and
scrubby grasses, areas of tall grasses and shrubs, and some trees surrounding the location of a former
drainage basin and near the banks of Parachute Creek. A barbed wire fence was present around the
majority of the Subject Property. Agricultural fields were present northeast of Highway 215.
Minor amounts of discarded trash were also present throughout the Subject Property. Larger pieces of
trash were found in a ditch near the southwestern edge of the Subject Property. These items included: an
old automobile, debris from a wooden structure, and scrap metal.
A well-maintained access road was present in the south-central area of the Subject Property which led to
an unfenced equipment storage yard. The equipment yard contained a small shed and conex box, as well
as generators, trailers, and other construction equipment. Two producing gas wells were present in the
northwest and southeast portions of the Subject Property.
The surrounding properties were industrial oil and gas businesses to the northwest, southeast, and north.
These businesses included large oil and gas processing buildings and equipment, and unpaved storage
yards with large amounts of vehicles. Parachute Creek traversed the Subject Property in the westernmost
section of the Subject Property. The creek was surrounded by dense vegetation and the water was high
in silt content.
Photographs taken during the site reconnaissance are provided in Appendix D.
7.1 Utilities and PCBs
High voltage power lines transect the eastern portion of the Subject Property from north to south, crossing
over the access road to the equipment yard. Abandoned power infrastructure is scattered through the
western portion of the Subject Property with some active infrastructure along the western edge. Several
mounted transformers were present on power poles throughout the Subject Property, and one
abandoned transformer was present in the northwest corner of the Subject Property. No obvious signs
of leaks were noted in association with any of the transformers.
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
DATA GAP ANALYSIS
21
8.0 Data Gap Analysis
The ASTM E1527-21 standards require a listing of “data gaps,” including data failure, encountered during
the investigative process that may affect the validity of the conclusions drawn by the environmental
professional. The ASTM E1527-21: 12.7 standard also requires that the environmental professional
estimate the relative importance of the data gaps. Generally, gaps in available data are related to the
availability of historical data sources for specific sites of concern. The environmental professional uses
multiple historical data sources as a method to provide coverage for data gaps. Historical information is
collected on a recurring basis, and the passage of time between data sets may or may not constitute a
significant gap in data coverage.
For this project, the following significant data gaps, as defined by ASTM E1527-21, were identified:
• The former Holding Pond and aeration basin/settling ponds were closed in 1998. The Deed
Restriction and Notification indicated that the Pond closure was completed in accordance with a
CDPHE-approved Closure Plan. HDR was unable to locate the Closure Plan and associated
regulatory approval documents. Without these documents, it cannot be verified that this facility
closure was completed in accordance with the plan, met the soil performance standards
established for the closure, or was approved by CDPHE.
• A second large holding pond was located east of the Holding Pond discussed in the previous bullet.
This East Holding Pond (refer to Figure 2) was present in the 1993 historic aerial and remained on
site in 1999, undergoing closure, after the adjacent Holding Pond facility had been closed. HDR
was unable to locate documentation to identify the type of liquids managed in the East Holding
Pond or any regulatory documentation supporting its closure. Without this information, HDR is
unable to determine the potential hazardous materials impacts in this area of the Subject
Property.
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
FINDINGS, OPINIONS, AND CONCLUSIONS
22
9.0 Findings, Opinions, and Conclusions
HDR has completed a Phase I ESA of an 88-acre parcel located in Garfield County, Colorado, for a proposed
10 MW solar energy system. Caerus Oil and Gas LLC (“User”) has requested a Phase I ESA for permitting
support to develop the Wheeler Gulch Solar Project.
The purpose of this Phase I ESA is to identify Recognized Environmental Conditions (RECs) that may
adversely affect the Subject Property. This Phase I ESA was conducted in accordance with the scope and
limitations of ASTM International (ASTM) Standard Practice E1527-21. This report includes a summary of
the site reconnaissance conducted on October 18, 2022, landowner interview, a review of environmental
databases, and a review of historical data sources. Any exceptions to or deletions from these ASTM
practices are described later in this report.
9.1 Findings
General findings of this assessment include the following:
• The Subject Property is situated on the western flank of the Colorado Rocky Mountains within a
river eroded basin. The local geology consists of Fluvial Deposits overlain by unconsolidated
alluvial materials. The surficial geology of the Subject Property consists of deposits from the
Wasatch Formation as well as the presence of deposits from intermountain lakes and related
deposits of marlstone. Bedrock thickness at the Subject Property is approximately 1500 feet and
soil at the site (Halaquepts) is classified as a clay loam with a very slow infiltration rate and is
considered poorly drained.
• Groundwater elevation data is not available for the Subject Property. However, nearby subsurface
investigations indicated that the depth to water is shallow (approximately 40 feet below ground
surface) and the groundwater flow direction is estimated to be southeastern toward Parachute
Creek. The computerized environmental database search conducted by EDR identified 13
monitoring wells at depths ranging from 35 to 55 feet within the Subject Property. Three out of
the ten wells were abandoned. Fifty well records were identified within 1-mile.
• The environmental database search conducted by EDR revealed no listings for the Subject
Property and three listings within the ASTM-designated search buffer (up to 1-mile). One orphan
site was also found in the search. The following listings of potential concern were identified within
the search buffer:
o UNOCAL CORP (2717 GARFIELD CR 215, MAP ID 1). This property is located 0.46 miles
downgradient of the Subject Property.
LTANKS/LUST– Records were found for a release on 5/10/1994. Limited details
on the tank contents or capacity were provided. A No Further Action (NFA) letter
was issued on 8/18/1994.
UST – One 4,018-gallon diesel underground storage tank (UST) and one 4,018-
gallon gasoline UST were reported as permanently closed on 12/31/1993.
o UNOCAL SHALE OIL FACILITY (2717 CNTY RD 215, MAP ID 2). This property is located 0.5
miles upgradient of the Subject Property.
CORRACTS – This property was ranked as a medium corrective action (CA) priority
facility in 1993. An investigation began in 1995 to due to groundwater
contamination at active/inactive holding ponds, presence of oil in sewer water
upstream of the API Separator and a need to upgrade the drum storage area. The
investigation workplan was approved in 1997, remediation construction began in
2000 were complete as of 4/17/2000. This property was deferred to Resource
Conservation and Recovery (RCRA) Subtitle C for storage of benzene and was not
listed on the National Priorities List (NPL).
• A review of historical aerials, topographic maps, and other information concluded that the Subject
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
FINDINGS, OPINIONS, AND CONCLUSIONS
23
Property had historically been vacant up the late 1970s, early 1980s when two holding ponds and
associated infrastructure, referred to as the Holding Pond and East Holding Pond, were used to
support adjacent industrial facilities.
o The Holding Pond was constructed in 1983 and closed in 1993. Arsenic contaminated soils
exceeding natural background standards were identified. These soils were excavated and
placed in an on-site repository north of the main holding pond. HDR was unable to locate
the Closure Plan and associated regulatory approval documents.
o The East Holding Pond was present in the 1993 historic aerial and was undergoing closure
in the 1999 historic aerial. HDR was unable to locate documentation to identify the type
of liquids managed in the East Holding Pond or any regulatory documentation supporting
its closure.
• A review of historical aerials and topographic maps identified gas and oil infrastructure have been
present within the Subject Property, in the northwest and southeast corners, beginning in 2006.
• An AUL, in the form of a Deed Restriction and Notification executed in November 1998, was
identified on the site for the parcel where the soil repository containing arsenic contaminated
soils is located. The Deed Restriction and Notification limits uses of the repository parcel and
requires Colorado Department of Public Health and the Environment (CDPHE) notification before
any modification or disturbance to the repository commences.
• No lease documents or other contractual agreements were identified between the current
Landowner and the Leasee(s) for the two oil/gas well pads. A Landowner Questionnaire was
completed on December 5, 2022, by Mr. Jason Eckman, the Regulatory and Community Relations
Lead for the current landowner, Caerus Oil and Gas LLC. Mr. Eckman stated that the property has
been owned by Caerus Oil and Gas LLC for five years. Mr. Eckman sated the prior owners of the
Subject Property used it to support oil shale development. He was aware of two producing oil/gas
wells owned by Terra Energy Partners in the northwest and southeast portion of the Subject
Property and a soil repository parcel containing excavated soil contaminated with arsenic from a
holding pond in the northwest portion of the Subject Property. Mr. Eckman stated that the soil
repository and two producing oil/gas well pads are excluded from the Wheeler Gulch Solar
Project.
• HDR conducted the site reconnaissance on October 18, 2022. The Subject Property is a primarily
vacant, undeveloped parcel with mostly short herbaceous plants and some trees surrounding the
location of a former holding pond and near the banks of Parachute Creek. A barbed wire fence
was present around the majority of the Subject Property. Agricultural fields were present in the
northeast portion of the Subject Property, northeast of Highway 215. Trash was present in the
southwestern edge of the Subject Property including an old automobile, debris from a wooden
structure, and scrap metal. A well-maintained access road was present in the south-central area
of the Subject Property which led to an unfenced equipment storage yard containing a small shed
and conex box, as well as generators, trailers, and other construction equipment. Other small
areas of the property appeared to be leased to oil and gas businesses including some buildings on
the southeast corner of the property and an access road on the eastern side of the property.
• High voltage power lines transect the eastern portion of the Subject Property from north to south,
crossing over the access road to the equipment yard. Abandoned power infrastructure is
scattered through the western portion of the parcel with some active infrastructure at the very
western edge.
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
FINDINGS, OPINIONS, AND CONCLUSIONS
24
9.2 Opinions
HDR has reviewed the stated data sources, which are part of the ASTM E1527-21 assessment protocol.
Based upon the review of the data, HDR has developed the following professional opinions:
• An equipment storage yard is present in the southern portion of the Subject Property. The
equipment storage yard contains a small shed and conex box, as well as generators, trailers, and
other construction equipment. Petroleum products for the generators may exist on site, but not
likely in significant quantities. This site is not considered to be a REC.
• A Holding Pond and settling ponds/aeration basins were located on the northeast Subject
Property from 1981 to 1993. The holding pond was taken out of service in November 1993 and
soils in the bottom of the holding pond were tested and shown to exceed the natural background
arsenic levels. Soils exceeding a CDPHE established performance standard were excavated and
placed in a soil repository parcel created out of the former aeration/settling basins immediately
north of the holding pond. HDR was unable to locate the Closure Plan and associated regulatory
approval documents. The soil repository is subject to a AUL that references the closure documents
with CDPHE in the form of a November 1998 Deed Restriction and Notification. Based on this
analysis, the soil repository parcel is considered a CREC and the footprint of the former holding
pond is considered a REC.
• The larger East Holding Pond was present in the 1993 historic aerial and remained on site in 1999,
undergoing closure, after the adjacent Holding Pond facility had been closed. HDR was unable to
locate documentation to identify the type of liquids managed in the East Holding Pond or any
regulatory documentation supporting its closure. The East Holding Pond is considered a REC.
• Oil and gas production in the northwest and southeast corners of the Subject Property has been
present since at least the early 2000s. The lease agreements for the two oil/gas well pads were
not available. No information was found regarding historical releases; however, a lack of an
agreement between the two parties opens up the User to liability should a release occur. The
oil/gas well pads are considered a business environmental risk due to a lack of documented
agreement between the User and the leasing party.
9.3 Conclusions
Based upon the above-detailed Findings and Opinions, HDR concludes that RECs have not been identified
in association with the Wheeler Gulch Solar Project, as summarized in the Opinions section above. The
following statement is required by ASTM E1527-21 as a declaration that RECs were found:
HDR has performed a Phase I ESA in conformance with the scope and limitations of ASTM E1527-21 of
the proposed Wheeler Gulch Solar Project located at 3477 County Road 215 Parachute, CO 81652. Any
exceptions to or deletions from these practices are described in following sections of this report. This
report has revealed no indications of RECs in connection with the Subject Property.
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
RECOMMENDATIONS
25
10.0 Recommendations
Recommendations included in this report were developed through the investigative procedures described
in the Scope of Services, Significant Assumptions, and Limitations sections of this report (See Section 2.3).
These findings should be reviewed within the context of the limitations provided in the Limitations
section.
Based upon the identification of RECs in the Subject Property, HDR makes the following recommendation:
Recommendation 1
HDR recommends a Phase II evaluation for soils in the footprint of the former Holding Pond and East
Holding Pond focused on areas where disturbance is anticipated. The evaluation will potentially
hazardous waste impacts and inform soil management needs during construction.
Recommendation 2
HDR recommends that the Wheeler Gulch Solar Project avoid construction in the location of the
arsenic soil repository and the operating oil and gas pads identified in Figure 2. If construction is
anticipated in the location of the arsenic soil repository, per the Deed Restriction and Notification, the
User must notify CDPHE before construction commences.
Recommendation 3
HDR recommends that the User complete and maintain lease agreements (or other appropriate legal
mechanism) with the operator(s) of the oil and gas pads to determine environmental liability should
a release occur due to Leasee operations.
Recommendation 4
HDR recommends that the User consider the “shelf life” of Phase I documents in determining risk.
ASTM E 1527-21 states that a conforming “Phase I” report is valid for a period of 180 days and may
be updated during the 180 days to 1-year timeframe. The report is valid for use in any of the CERCLA
defenses ONLY if it is updated within this time frame. If greater than one year passes from the final
report date, the Phase I effort would need to be repeated to remain in compliance with ASTM and
the “All Appropriate Inquiry” protections.
Report Viability Dates
Phase I ESA Component Date Collected
Database Search October 13, 2022
Interview(s) December 5, 2022
Site Reconnaissance October 18, 2022
Environmental Professional Declaration Report Date
AUL and Environmental Lien Search December 5, 2022
Report Expiration
*calculated from earliest collection date
April 11, 2023
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
QUALIFICATIONS OF ENVIRONMENTAL PROFESSIONALS
26
11.0 Qualifications of Environmental
Professionals
11.1 Signatures and Qualifications
We declare that, to the best of our professional knowledge and belief, we meet the definition of
environmental professional as defined in Section 312.10 of 40 Code of Federal Regulations [C.F.R.]
Part 312.
We have the specific qualifications based on education, training, and experience to assess a property of
the nature, history, and setting of the Subject Property. We have developed and performed the all
appropriate inquires in conformance with standards and practices set forth in 40 CFR Part 312.
Qualified Environmental Professional Qualified Environmental Professional
Nicole Pahl Kate Garufi
11.1.1 Qualifications of Environmental Professionals
This Phase I ESA was performed by the following HDR personnel:
Mrs. Nicole Pahl is an Environmental Scientist with over 7 years of experience with environmental review
documents and field reports. Over the last 5 years with HDR, Nicole has assisted qualified environmental
professionals with Phase IESA reports and site reconnaissance for a variety of energy, water resources,
and transportation development projects.
Ms. Kate Garufi, PMP, has more than 17 years of experience in the assessment and remediation of
impacted properties and compliance with environmental regulations. She has a B.S. in Chemical
Engineering from Virginia Polytechnic Institute and State University and a Masters in Environmental
Engineering from Johns Hopkins University. Ms. Garufi specializes in site investigation and remediation of
hazardous waste sites and properties for public and private sector clients across the United States. As a
former CERCLA regulator for the Environmental Protection Agency for 15 years, she is highly
knowledgeable of federal and state regulations and standards.
Wheeler Gulch Solar Project | Phase I Environmental Site Assessment
REFERENCES
27
12.0 References
ASTM Practice E 1527-21, 2021, Standard Practice for Environmental Site Assessments: Phase I
Environmental Site Assessment Process.
COGCC. 2022. Colorado Oil and Gas Information System (COGIS). Accessed October 27, 2022.
https://cogcc.state.co.us/data.html.
Donnell, J.R., Yeend, W.E., and Smith, M.C., 1986, Preliminary geologic map of the Grand Valley
quadrangle, Garfield County, Colorado, U.S. Geological Survey, Miscellaneous Field Studies Map
MF-1883, 1:24,000.
EDR. 2022a. The EDR Aerial Photo Decade Package. Wheeler Gulch Solar, 3477 County Road 215
Parachute, CO 81635. Inquiry number 7146432.8. Dated October 17, 2022.
EDR. 2022b. The EDR City Directory Image Report. Wheeler Gulch Solar, 3477 County Road 215
Parachute, CO 81635. Inquiry number 7146432.5. Dated October 17, 2022.
EDR. 2022c. The EDR Historical Topo Map Report. Wheeler Gulch Solar, 3477 County Road 215
Parachute, CO 81635. Inquiry number 7146432.4. Dated October 13, 2022
EDR. 2022d. The EDR Radius Map Report with GeoCheck. Wheeler Gulch Solar, 3477 County Road 215
Parachute, CO 81635. Inquiry number 7146432.2s. Dated October 13, 2022.
NPMS. 2022. Public Viewer. Accessed November 1, 2022. https://co.pipeline-
awareness.com/national_pipeline_mapping/.
Tweto, O. (1979) Geologic Map of Colorado. United States Geological Survey Map (Scale 1:500,000).
A
Environmental Database
Search Results
FORM-LBC-SPM
®kcehCoeG htiw tropeR ™paM suidaR RDE ehT
6 Armstrong Road, 4th floor
Shelton, CT 06484
Toll Free: 800.352.0050
www.edrnet.com
Wheeler Gulch Solar
3477 County Road 215
Parachute, CO 81635
Inquiry Number: 7146432.2s
October 13, 2022
TABLE OF CONTENTS
SECTION PAGE
Executive Summary ES1
Overview Map 2
Detail Map 3
Map Findings Summary 4
Map Findings 8
Orphan Summary 129
Government Records Searched/Data Currency Tracking GR-1
GEOCHECK ADDENDUM
Physical Setting Source Addendum A-1
Physical Setting Source Summary A-2
Physical Setting SSURGO Soil Map A-5
Physical Setting Source Map A-18
Physical Setting Source Map Findings A-20
Physical Setting Source Records Searched PSGR-1
Thank you for your business.
Please contact EDR at 1-800-352-0050
with any questions or comments.
Disclaimer - Copyright and Trademark Notice
This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data
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provide, nor should they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property.
Only an assessment performed by a qualified environmental professional can provide findings, opinions or conclusions regarding the
environmental risk or conditions in, on or at any property.
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TC7146432.2s Page 1
EXECUTIVE SUMMARY
TC7146432.2s EXECUTIVE SUMMARY 1
A search of available environmental records was conducted by Environmental Data Resources, Inc (EDR).
The report was designed to assist parties seeking to meet the search requirements of EPA’s Standards
and Practices for All Appropriate Inquiries (40 CFR Part 312), the ASTM Standard Practice for
Environmental Site Assessments (E1527-21), the ASTM Standard Practice for Environmental Site
Assessments for Forestland or Rural Property (E 2247-16), the ASTM Standard Practice for Limited
Environmental Due Diligence: Transaction Screen Process (E 1528-14) or custom requirements developed
for the evaluation of environmental risk associated with a parcel of real estate.
TARGET PROPERTY INFORMATION
ADDRESS
3477 COUNTY ROAD 215
PARACHUTE, CO 81635
COORDINATES
39.4808000 - 39ˆ 28’ 50.88’’Latitude (North):
108.1032580 - 108ˆ 6’ 11.72’’Longitude (West):
Zone 12Universal Tranverse Mercator:
749154.6UTM X (Meters):
4373931.0UTM Y (Meters):
5387 ft. above sea levelElevation:
USGS TOPOGRAPHIC MAP ASSOCIATED WITH TARGET PROPERTY
14202419 PARACHUTE, COTarget Property Map:
2019Version Date:
14202333 FORKED GULCH, CONorth Map:
2019Version Date:
14202379 RED PINNACLE, COSouthwest Map:
2019Version Date:
14202313 CIRCLE DOT GULCH, CONorthwest Map:
2019Version Date:
AERIAL PHOTOGRAPHY IN THIS REPORT
20150909, 20150828Portions of Photo from:
USDASource:
7146432.2s Page 2
2 UNOCAL SHALE OIL FAC 2717 CNTY RD 215 SEMS-ARCHIVE, CORRACTS, RCRA-TSDF, RCRA-VSQG Higher 2889, 0.547, NNW
1 UNOCAL CORP 2717 GARFIELD CR 215 LTANKS, LUST, UST Lower 2477, 0.469, ESE
MAPPED SITES SUMMARY
Target Property Address:
3477 COUNTY ROAD 215
PARACHUTE, CO 81635
Click on Map ID to see full detail.
MAP RELATIVE DIST (ft. & mi.)
ID DATABASE ACRONYMS ELEVATION DIRECTIONSITE NAME ADDRESS
EXECUTIVE SUMMARY
TC7146432.2s EXECUTIVE SUMMARY 3
TARGET PROPERTY SEARCH RESULTS
The target property was not listed in any of the databases searched by EDR.
DATABASES WITH NO MAPPED SITES
No mapped sites were found in EDR’s search of available ("reasonably ascertainable ") government
records either on the target property or within the search radius around the target property for the
following databases:
STANDARD ENVIRONMENTAL RECORDS
Lists of Federal NPL (Superfund) sites
NPL National Priority List
Proposed NPL Proposed National Priority List Sites
NPL LIENS Federal Superfund Liens
Lists of Federal Delisted NPL sites
Delisted NPL National Priority List Deletions
Lists of Federal sites subject to CERCLA removals and CERCLA orders
FEDERAL FACILITY Federal Facility Site Information listing
SEMS Superfund Enterprise Management System
Lists of Federal CERCLA sites with NFRAP
SEMS-ARCHIVE Superfund Enterprise Management System Archive
Lists of Federal RCRA TSD facilities
RCRA-TSDF RCRA - Treatment, Storage and Disposal
Lists of Federal RCRA generators
RCRA-LQG RCRA - Large Quantity Generators
RCRA-SQG RCRA - Small Quantity Generators
RCRA-VSQG RCRA - Very Small Quantity Generators (Formerly Conditionally Exempt Small Quantity
Generators)
Federal institutional controls / engineering controls registries
LUCIS Land Use Control Information System
US ENG CONTROLS Engineering Controls Sites List
US INST CONTROLS Institutional Controls Sites List
Federal ERNS list
ERNS Emergency Response Notification System
EXECUTIVE SUMMARY
TC7146432.2s EXECUTIVE SUMMARY 4
Lists of state- and tribal hazardous waste facilities
SHWS This state does not maintain a SHWS list. See the Federal CERCLIS list and Federal
NPL list.
Lists of state and tribal landfills and solid waste disposal facilities
SWF/LF Solid Waste Sites & Facilities
SHWF Solid Waste Information System Listing
Lists of state and tribal leaking storage tanks
LAST Leaking Aboveground Storage Tank Listing
INDIAN LUST Leaking Underground Storage Tanks on Indian Land
LUST TRUST RAP Site Listing
Lists of state and tribal registered storage tanks
FEMA UST Underground Storage Tank Listing
UST Underground Storage Tank Database
AST Aboveground Tank List
INDIAN UST Underground Storage Tanks on Indian Land
State and tribal institutional control / engineering control registries
AUL Environmental Covenants and Environmental Use Restrictions List
Lists of state and tribal voluntary cleanup sites
INDIAN VCP Voluntary Cleanup Priority Listing
VCP Voluntary Cleanup & Redevelopment Act Application Tracking Report
Lists of state and tribal brownfield sites
BROWNFIELDS Brownfields Sites Listing
ADDITIONAL ENVIRONMENTAL RECORDS
Local Brownfield lists
US BROWNFIELDS A Listing of Brownfields Sites
Local Lists of Landfill / Solid Waste Disposal Sites
SWRCY Registered Recyclers Listing
HIST LF Historical Landfill List
INDIAN ODI Report on the Status of Open Dumps on Indian Lands
ODI Open Dump Inventory
DEBRIS REGION 9 Torres Martinez Reservation Illegal Dump Site Locations
IHS OPEN DUMPS Open Dumps on Indian Land
DENVER CO HISTORIC FILL Denver City & County Historic Fill Areas
Local Lists of Hazardous waste / Contaminated Sites
US HIST CDL Delisted National Clandestine Laboratory Register
EXECUTIVE SUMMARY
TC7146432.2s EXECUTIVE SUMMARY 5
CDL Meth Lab Locations
US CDL National Clandestine Laboratory Register
PFAS PFAS Information Listing
AQUEOUS FOAM Class B Firefighting Foam Contaminating PFAS Listing
Local Land Records
LIENS 2 CERCLA Lien Information
Records of Emergency Release Reports
HMIRS Hazardous Materials Information Reporting System
SPILLS Spills Database
SPILLS 90 SPILLS 90 data from FirstSearch
Other Ascertainable Records
RCRA NonGen / NLR RCRA - Non Generators / No Longer Regulated
FUDS Formerly Used Defense Sites
DOD Department of Defense Sites
SCRD DRYCLEANERS State Coalition for Remediation of Drycleaners Listing
US FIN ASSUR Financial Assurance Information
EPA WATCH LIST EPA WATCH LIST
2020 COR ACTION 2020 Corrective Action Program List
TSCA Toxic Substances Control Act
TRIS Toxic Chemical Release Inventory System
SSTS Section 7 Tracking Systems
ROD Records Of Decision
RMP Risk Management Plans
RAATS RCRA Administrative Action Tracking System
PRP Potentially Responsible Parties
PADS PCB Activity Database System
ICIS Integrated Compliance Information System
FTTS FIFRA/ TSCA Tracking System - FIFRA (Federal Insecticide, Fungicide, & Rodenticide
Act)/TSCA (Toxic Substances Control Act)
MLTS Material Licensing Tracking System
COAL ASH DOE Steam-Electric Plant Operation Data
COAL ASH EPA Coal Combustion Residues Surface Impoundments List
PCB TRANSFORMER PCB Transformer Registration Database
RADINFO Radiation Information Database
HIST FTTS FIFRA/TSCA Tracking System Administrative Case Listing
DOT OPS Incident and Accident Data
CONSENT Superfund (CERCLA) Consent Decrees
INDIAN RESERV Indian Reservations
FUSRAP Formerly Utilized Sites Remedial Action Program
UMTRA Uranium Mill Tailings Sites
LEAD SMELTERS Lead Smelter Sites
US AIRS Aerometric Information Retrieval System Facility Subsystem
US MINES Mines Master Index File
ABANDONED MINES Abandoned Mines
FINDS Facility Index System/Facility Registry System
UXO Unexploded Ordnance Sites
DOCKET HWC Hazardous Waste Compliance Docket Listing
ECHO Enforcement & Compliance History Information
FUELS PROGRAM EPA Fuels Program Registered Listing
EXECUTIVE SUMMARY
TC7146432.2s EXECUTIVE SUMMARY 6
AIRS Permitted Facility & Emissions Listing
ASBESTOS Asbestos Abatement & Demolition Projects
METHANE SITE Methane Site Investigations - Jefferson County 1980
Methane Investigation Methane Gas & Swamp Findings
DRYCLEANERS Drycleaner Facilities
Financial Assurance Financial Assurance Information Listing
LEAD LEAD
MINES Permitted Mines Listing
NPDES Permitted Facility Listing
UIC Underground Injection Control
UMTRA Uranium Mill Tailings Sites
MINES MRDS Mineral Resources Data System
EDR HIGH RISK HISTORICAL RECORDS
EDR Exclusive Records
EDR MGP EDR Proprietary Manufactured Gas Plants
EDR Hist Auto EDR Exclusive Historical Auto Stations
EDR Hist Cleaner EDR Exclusive Historical Cleaners
EDR RECOVERED GOVERNMENT ARCHIVES
Exclusive Recovered Govt. Archives
RGA LF Recovered Government Archive Solid Waste Facilities List
RGA LUST Recovered Government Archive Leaking Underground Storage Tank
SURROUNDING SITES: SEARCH RESULTS
Surrounding sites were identified in the following databases.
Elevations have been determined from the USGS Digital Elevation Model and should be evaluated on
a relative (not an absolute) basis. Relative elevation information between sites of close proximity
should be field verified. Sites with an elevation equal to or higher than the target property have been
differentiated below from sites with an elevation lower than the target property.
Page numbers and map identification numbers refer to the EDR Radius Map report where detailed
data on individual sites can be reviewed.
Sites listed in bold italics are in multiple databases.
Unmappable (orphan) sites are not considered in the foregoing analysis.
STANDARD ENVIRONMENTAL RECORDS
Lists of Federal RCRA facilities undergoing Corrective Action
CORRACTS: CORRACTS is a list of handlers with RCRA Corrective Action Activity. This report shows
which nationally-defined corrective action core events have occurred for every handler that has had corrective
action activity.
A review of the CORRACTS list, as provided by EDR, and dated 06/20/2022 has revealed that there is 1
EXECUTIVE SUMMARY
TC7146432.2s EXECUTIVE SUMMARY 7
CORRACTS site within approximately 1 mile of the target property.
PageMap IDDirection / Distance Address Equal/Higher Elevation ____________________ ________ ___________________ _____ _____
UNOCAL SHALE OIL FAC 2717 CNTY RD 215 NNW 1/2 - 1 (0.547 mi.) 2 9
EPA ID:: COD980718902
Lists of state and tribal leaking storage tanks
LUST: The Leaking Underground Storage Tank Incident Reports contain an inventory of reported
leaking underground storage tank incidents. The data come from the Department of Health’s Leaking Underground
Storage Tank List.
A review of the LUST list, as provided by EDR, and dated 03/01/2018 has revealed that there is 1 LUST
site within approximately 0.5 miles of the target property.
PageMap IDDirection / Distance Address Lower Elevation ____________________ ________ ___________________ _____ _____
UNOCAL CORP 2717 GARFIELD CR 215 ESE 1/4 - 1/2 (0.469 mi.) 1 8
Facility Id: 1329
Status: Closed
LTANKS: Active and Closed OPS Petroleum Release Events in Colorado. Includes the OPS Open Event
locations, but also shows locations of closed events (releases that have been issued a No Further Action
determination).
A review of the LTANKS list, as provided by EDR, and dated 05/03/2022 has revealed that there is 1
LTANKS site within approximately 0.5 miles of the target property.
PageMap IDDirection / Distance Address Lower Elevation ____________________ ________ ___________________ _____ _____
UNOCAL CORP 2717 GARFIELD CR 215 ESE 1/4 - 1/2 (0.469 mi.) 1 8
EXECUTIVE SUMMARY
TC7146432.2s EXECUTIVE SUMMARY 8
Due to poor or inadequate address information, the following sites were not mapped. Count: 1 records.
Site Name Database(s)____________ ____________
MIDDLE FORK COMPRESSOR STATION SHWF